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ASTM D7403-09

(Test Method)

Standard Test Method for Determination of Residue of Emulsified Asphalt by Low Temperature Vacuum Distillation

Standard Test Method for Determination of Residue of Emulsified Asphalt by Low Temperature Vacuum Distillation

SIGNIFICANCE AND USE
This test method can be used for quantitative determination of residue in emulsified asphalts at a temperature of 135°C (275°F) with a 60 minute distillation test using current distillation apparatus. This method is suitable to obtain residues for service evaluation, quality control, and research. This distillation method is not intended to produce residues equivalent to the Test Method D 6997 260°C (500°F) distillation procedure.
SCOPE
1.1 This method covers the quantitative determination of residue in emulsified asphalts composed principally of a semisolid or liquid asphaltic base, water, and an emulsifying agent. The emulsified asphalts will generally contain polymeric materials. It is especially suitable for emulsified asphalt residue properties that may be altered at the high temperature 260°C (500°F) distillation. Since there is currently not a precision statement for this procedure, it is recommended to the user that this procedure not be used for buy/sell purposes at the present time.
1.2 The values stated in SI units are to be regarded as the standard. Values in parentheses in inch-pound units are provided for informational purposes only.
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

General Information

Status
Historical
Publication Date
31-May-2009
ICS
75.140 - Waxes, bituminous materials and other petroleum products
91.100.50 - Binders. Sealing materials
93.080.20 - Road construction materials
Technical Committee
D04 - Road and Paving Materials
Drafting Committee
D04.42 - Emulsified Asphalt Test
Current Stage
Ref Project

Relations

Replaced By
ASTM D7403-09(2017) - Standard Test Method for Determination of Residue of Emulsified Asphalt by Low-Temperature Vacuum Distillation
Effective Date
01-Oct-2017
Referred By
ASTM D6997-12(2020) - Standard Test Method for Distillation of Emulsified Asphalt
Effective Date
01-Jun-2009
Referred By
ASTM D244-09(2017) - Standard Test Methods and Practices for Emulsified Asphalts
Effective Date
01-Jun-2009
Referred By
ASTM D6084/D6084M-21 - Standard Test Method for Elastic Recovery of Asphalt Materials by Ductilometer
Effective Date
01-Jun-2009
Referred By
ASTM D113-17 - Standard Test Method for Ductility of Asphalt Materials
Effective Date
01-Jun-2009

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ASTM D7403-09 - Standard Test Method for Determination of Residue of Emulsified Asphalt by Low Temperature Vacuum DistillationASTM D7403-09 - Standard Test Method for Determination of Residue of Emulsified Asphalt by Low Temperature Vacuum Distillation
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ASTM D7403-09 - Standard Test Method for Determination of Residue of Emulsified Asphalt by Low Temperature Vacuum Distillation
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NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
Designation:D7403 −09
Standard Test Method for
Determination of Residue of Emulsified Asphalt by Low
Temperature Vacuum Distillation
This standard is issued under the fixed designation D7403; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope distillation method is not intended to produce residues equiva-
lent to the Test Method D6997 260°C (500°F) distillation
1.1 This method covers the quantitative determination of
procedure.
residue in emulsified asphalts composed principally of a
semisolid or liquid asphaltic base, water, and an emulsifying
4. Apparatus
agent.Theemulsifiedasphaltswillgenerallycontainpolymeric
4.1 Aluminum Alloy Still, conforming to Test Method
materials.Itisespeciallysuitableforemulsifiedasphaltresidue
D6997 except that a 13 mm ( ⁄2 in.) diameter hole is drilled
properties that may be altered at the high temperature 260°C
between the two existing 13 mm ( ⁄2 in.) thermometer holes for
(500°F) distillation. Since there is currently not a precision
the connection of a vacuum gauge (see Fig. 1). The joint
statement for this procedure, it is recommended to the user that
between the still and lid shall be air tight with the gasket in
this procedure not be used for buy/sell purposes at the present
place. Other heating devices may be used provided they
time.
employ the intended control of temperature during the distil-
1.2 The values stated in SI units are to be regarded as the
lation procedure.
standard. Values in parentheses in inch-pound units are pro-
4.2 ConnectionApparatus, Test Method D6997, with modi-
vided for informational purposes only.
fications as shown in Fig. 2. Connection tubing may be of
1.3 This standard does not purport to address all of the
suitable materials provided the intended vacuum, temperature,
safety concerns, if any, associated with its use. It is the
and method is maintained. Other forms of condensers may be
responsibility of the user of this standard to establish appro-
used provided they have an equivalent or greater interior
priate safety and health practices and determine the applica-
surface area for condensation of distillate.
bility of regulatory limitations prior to use.
NOTE 1—Silicone rubber stoppers are recommended.
4.3 Thermometric Device, ASTM 7C (7F) thermometers, or
2. Referenced Documents
thermocouple devices calibrated at 135°C (275°F). The ther-
2.1 ASTM Standards:
mocouple probe, Type T with exposed junction, should be of
D6997 Test Method for Distillation of Emulsified Asphalt
sufficient length (approximately 300 mm (12 in.)) to be
E1 Specification for ASTM Liquid-in-Glass Thermometers
positioned approximately 6 mm (0.25 in.) off the bottom of the
assembled still. Use of equivalent thermometric devices is
3. Significance and Use
permitted.
4.4 Balance, capable of weighing 3500 grams to 6 0.1
3.1 This test method can be used for quantitative determi-
gram.
nation of residue in emulsified asphalts at a temperature of
135°C (275°F) with a 60 minute distillation test using current
4.5 Vacuum Pump, rotary vane type, capable of maintaining
distillation apparatus. This method is suitable to obtain resi-
a vacuum of 88 kPa below gauge pressure or greater.
dues for service evaluation, quality control, and research. This
NOTE 2—88 kPa below gauge pressure is equal to 26 in. Hg (660 mm)
below atmospheric pressure.
4.6 Gasket, of silicone rubber, 3 mm ( ⁄8 in.) thick, cut to fit
flanged opening on still. Other gasket materials may be used
This test method is under the jurisdiction of ASTM Committee D04 on Road
and Paving Materials and is the direct responsibility of Subcommittee D04.42 on
provided they withstand the maximum temperature reached
Emulsified Asphalt Test.
during distillation and are able to maintain the specified
Current edition approved June 1, 2009. Published July 2009. DOI: 10.1520/
vacuum within the still.
D7403-09.
For referenced ASTM standards, visit the ASTM website, www.astm.org, or
4.7 Vacuum Gauges, dial type or other suitable type con-
contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
nected to vacuum tubing and/or fittings to allow attachment to
Standards volume information, refer to the standard’s Document Summary page on
the ASTM website. both vacuum pump and to still apparatus and capable of
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
D7403−09
FIG. 1Aluminum Alloy Still Lid Showing Location of the Hole for Vacuum Gauge Connection
FIG. 2Connection Apparatus Schematic
reading a minimum vacuum of 88 kPa below gauge pressure 5. Hazards
(660 mm or 26 in. Hg below atmospheric pressure).
5.1 Warning—Mercury has been designated by the United
4.8 Freezer, maintained at approximately –10°C.
States Environmental ProtectionAgency (EPA) and many state
agencies as a hazardous material that can cause central nervous
4.9 Disposable Plastic Drink Cups, of convenient size and
system,kidneyandliverdamage.Mercury,oritsvapor,maybe
make to serve as a container during freezing of emulsified
asphalt. hazardous to health and corrosive to materials. Caution should
D7403−09
be taken when handling mercury and mercury containing 5°C (275 6 10°F).This temperature should be achieved with
...

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Standard Test Method for Determination of Residue of Emulsified Asphalt by Low Temperature Vacuum Distillation

SIGNIFICANCE AND USE
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SIGNIFICANCE AND USE
3.1 Cationic emulsified asphalts are identified by the migration of the particles to a negatively charged electrode (cathode) by means of a direct current. Aggregates and sands used in conjunction with emulsified asphalts are often predominantly either negatively or positively charged. Emulsified asphalts should be selected to be compatible with the available aggregate or sand. This practice will aid in identifying a cationic type of emulsified asphalt as defined by Specification D2397.
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This specification covers coated glass mat water-resistant gypsum backing panel designed for use on ceilings and walls in bath and shower areas as a base for the application of ceramic or plastic tile. Coated glass mat water-resistant gypsum backing panel shall consist of a noncombustible water-resistant gypsum core, surfaced with glass mat, partially or completely embedded in the core, and with a water-resistant coating on one surface. The specimens shall be tested for flexural strength, humidified deflection, core hardness, end hardness, edge hardness, nail pull resistance, water resistance, and surface water absorption. Coated glass mat water-resistant gypsum backing panel shall have surfaces true and free of imperfections that render the panel unfit for its designed use.
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ASTM D2170/D2170M-24(Test Method)
Standard Test Method for Kinematic Viscosity of Asphalts

SIGNIFICANCE AND USE
5.1 The kinematic viscosity characterizes flow behavior. The method is used to determine the consistency of liquid asphalt as one element in establishing the uniformity of shipments or sources of supply. The specifications are usually at temperatures of 60 and 135 °C.
Note 3: The quality of the results produced by this standard are dependent on the competence of the personnel performing the procedure and the capability, calibration, and maintenance of the equipment used. Agencies that meet the criteria of Specification D3666 are generally considered capable of competent and objective testing, sampling, inspection, etc. Users of this standard are cautioned that compliance with Specification D3666 alone does not completely ensure reliable results. Reliable results depend on many factors; following the suggestions of Specification D3666 or some similar acceptable guideline provides a means of evaluating and controlling some of those factors.
SCOPE
1.1 This test method covers procedures for the determination of kinematic viscosity of liquid asphalts, road oils, and distillation residues of liquid asphalts all at 60 °C [140 °F] and of liquid asphalt binders at 135 °C [275 °F] (see table notes, 11.1) in the range from 6 to 100 000 mm2/s [cSt].  
1.2 Results of this test method can be used to calculate viscosity when the density of the test material at the test temperature is known or can be determined. See Annex A1 for the method of calculation.  
Note 1: This test method is suitable for use at other temperatures and at lower kinematic viscosities, but the precision is based on determinations on liquid asphalts and road oils at 60 °C [140 °F] and on asphalt binders at 135 °C [275 °F] only in the viscosity range from 30 to 6000 mm2/s [cSt].
Note 2: Modified asphalt binders or asphalt binders that have been conditioned or recovered are typically non-Newtonian under the conditions of this test. The viscosity determined from this method is under the assumption that asphalt binders behave as Newtonian fluids under the conditions of this test. When the flow is non-Newtonian in a capillary tube, the shear rate determined by this method may be invalid. The presence of non-Newtonian behavior for the test conditions can be verified by measuring the viscosity with viscometers having different-sized capillary tubes. The defined precision limits in 11.1 may not be applicable to non-Newtonian asphalt binders.  
1.3 Warning—Mercury has been designated by the United States Environmental Protection Agency (EPA) and many state agencies as a hazardous material that can cause central nervous system, kidney, and liver damage. Mercury, or its vapor, may be hazardous to health and corrosive to materials. Caution should be taken when handling mercury and mercury-containing products. See the applicable product Material Safety Data Sheet (MSDS) or Safety Data Sheet (SDS) for details and the EPA’s website—http://www.epa.gov/mercury/faq.htm—for additional information. Users should be aware that selling mercury, mercury-containing products, or both, in your state may be prohibited by state law.  
1.4 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the two systems may result in nonconformance with the standard.  
1.5 The text of this standard references notes and footnotes that provide explanatory material. These notes and footnotes (excluding those in tables and figures) shall not be considered as requirements of the standard.  
1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior ...

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