ASTM D1353-09

Standard Test Method for Nonvolatile Matter in Volatile Solvents for Use in Paint, Varnish, Lacquer, and Related Products

SIGNIFICANCE AND USE
This test method describes the analytical measurement of residual matter in solvents that are intended to be 100 % volatile at 105 ± 5°C. Volatile solvents are used in the manufacture of paint, varnish, lacquer, and other related products, and the presence of any residue may affect the product quality or efficiency of the process. This test method is useful in manufacturing control and assessing compliance with specifications.
SCOPE
1.1 This test method covers the determination of the nonvolatile matter in volatile solvents for use in paint, varnish, lacquer, and related products.
1.2 The following applies to all specified limits in this standard; for purposes of determining conformance with this standard, an observed value or a calculated value shall be rounded off “to the nearest unit” in the last right-hand digit used in expressing the specification limit, in accordance with the rounding-off method of Practice E 29.
1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.4 For hazard information and guidance, see the supplier's Material Safety Data Sheet for materials listed in this test method.
1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. For specific hazard statements, see Section 5.

General Information

• Status: Historical
• Publication Date: 31-May-2009
• ICS: 87.060.30 - Solvents
• Technical Committee: D01 - Paint and Related Coatings, Materials, and Applications
• Drafting Committee: D01.35 - Solvents, Plasticizers, and Chemical Intermediates

Relations

• Replaces: ASTM D1353-03 - Standard Test Method for Nonvolatile Matter in Volatile Solvents for Use in Paint, Varnish, Lacquer, and Related Products
• Effective Date: 01-Jun-2009
• Referred By: ASTM E3237-19 - Standard Specification for Undenatured Ethanol from Biomass for Use in Industrial Applications
• Effective Date: 01-Jun-2009
• Referred By: ASTM D331-11(2019) - Standard Specification for 2-Ethoxyethanol^,
• Effective Date: 01-Jun-2009
• Referred By: ASTM D3131-07(2021) - Standard Specification for Isopropyl Acetate (99 % Grade)
• Effective Date: 01-Jun-2009
• Referred By: ASTM D1718-09(2023) - Standard Specification for Isobutyl Acetate (95 % Grade)
• Effective Date: 01-Jun-2009
• Referred By: ASTM D2634-07(2021) - Standard Specification for Methyl Amyl Acetate (95 % Grade)
• Effective Date: 01-Jun-2009
• Referred By: ASTM D1836-07(2021) - Standard Specification for Commercial Hexanes
• Effective Date: 01-Jun-2009
• Referred By: ASTM F311-08(2020) - Standard Practice for Processing Aerospace Liquid Samples for Particulate Contamination Analysis Using Membrane Filters
• Effective Date: 01-Jun-2009
• Referred By: ASTM D770-11(2019) - Standard Specification for Isopropyl Alcohol^,
• Effective Date: 01-Jun-2009
• Referred By: ASTM D329-07(2021) - Standard Specification for Acetone
• Effective Date: 01-Jun-2009
• Referred By: ASTM D268-22 - Standard Guide for Sampling and Testing Volatile Solvents and Chemical Intermediates for Use in Paint and Related Coatings and Material
• Effective Date: 01-Jun-2009
• Referred By: ASTM D1719-11(2019) - Standard Specification for Isobutyl Alcohol^,
• Effective Date: 01-Jun-2009
• Referred By: ASTM D7670-10(2021) - Standard Practice for Processing In-service Fluid Samples for Particulate Contamination Analysis Using Membrane Filters
• Effective Date: 01-Jun-2009
• Referred By: ASTM D304-11(2019) - Standard Specification for <emph type="bdit">n</emph>-Butyl Alcohol (Butanol)
• Effective Date: 01-Jun-2009
• Referred By: ASTM D1007-11(2019) - Standard Specification for <emph type="bdit">sec</emph>-Butyl Alcohol^,
• Effective Date: 01-Jun-2009

Standards Content (Sample)

NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
Designation: D1353 − 09
StandardTest Method for
Nonvolatile Matter in Volatile Solvents for Use in Paint,
1
Varnish, Lacquer, and Related Products
This standard is issued under the fixed designation D1353; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
This standard has been approved for use by agencies of the Department of Defense.
3
1. Scope* cialty Chemicals (Withdrawn 2009)
E299 Test Method for Trace Amounts of Peroxides In
1.1 This test method covers the determination of the non-
Organic Solvents
volatile matter in volatile solvents for use in paint, varnish,
lacquer, and related products.
3. Significance and Use
1.2 The following applies to all specified limits in this
3.1 This test method describes the analytical measurement
standard; for purposes of determining conformance with this
of residual matter in solvents that are intended to be 100 %
standard, an observed value or a calculated value shall be
volatile at 105 6 5°C. Volatile solvents are used in the
rounded off “to the nearest unit” in the last right-hand digit
manufacture of paint, varnish, lacquer, and other related
used in expressing the specification limit, in accordance with
products, and the presence of any residue may affect the
the rounding-off method of Practice E29.
product quality or efficiency of the process. This test method is
1.3 The values stated in SI units are to be regarded as
useful in manufacturing control and assessing compliance with
standard. No other units of measurement are included in this
specifications.
standard.
1.4 For hazard information and guidance, see the supplier’s 4. Apparatus
Material Safety Data Sheet for materials listed in this test
4.1 Oven, thermostatically controlled at 105 6 5°C.
method.
4.2 Dish, evaporating, platinum, 125-mL. A platinum
1.5 This standard does not purport to address all of the
evaporating dish is preferred. Alternatively, an aluminum or
safety concerns, if any, associated with its use. It is the
porcelain dish may be used (see Note 1).
responsibility of the user of this standard to establish appro-
NOTE 1—Precision data were determined utilizing only platinum
priate safety and health practices and determine the applica-
dishes.
bility of regulatory limitations prior to use. For specific hazard
4.3 Cylinder, graduated, 100-mL.
statements, see Section 5.
4.4 Analytical Balance, precision to 60.1 mg.
2. Referenced Documents
2
5. Hazards
2.1 ASTM Standards:
E29 Practice for Using Significant Digits in Test Data to
5.1 Warning—Certain solvents and chemical
Determine Conformance with Specifications
intermediates, particularly, but not only ethers and unsaturated
E180 Practice for Determining the Precision of ASTM
compounds, may form peroxides during storage. These perox-
Methods for Analysis and Testing of Industrial and Spe-
ides may present a violent explosion hazard when the chemi-
calsareevaporated.Whenperoxideformationislikelybecause
of chemical type or length of storage time, analyze the material
1
for peroxides (see Test Method E299). If they exist in hazard-
This test method is under the jurisdiction of ASTM Committee D01 on Paint
and Related Coatings, Materials, andApplications and is the direct responsibility of
ous concentrations, take appropriate precautions such as de-
Subcommittee D01.35 on Solvents, Plasticizers, and Chemical Intermediates.
stroying the peroxides before evaporation, shielding, or dis-
Current edition approved June 1, 2009. Published June 2009. Originally
posal of the sample and not running the test.
approved in 1954. Last previous edition approved in 2003 as D1353 – 03. DOI:
10.1520/D1353-09.
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or
contact ASTM Customer Service at [e-mail]. For Annual Book of ASTM
3
Standards volume information, refer to the standard’s Document Summary page on The last approved version of this historical standard is referenced on
the ASTM website. www.astm.org.
*A Summary of Changes section appears at the end of this standard
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
1

---------------------- Page: 1 ----------------------
D1353 − 09
6. Procedure different laboratories analyzed one sample of methyl ethyl
ketone in duplicate on two different days. This sample was
6.1 Dry a 125-mL platinum evaporating dish in an oven at
prepared by adding 0.006 % of a nonvolatile resin to commer-
105 6 5°C, cool in a desiccator, and weigh. Repeat until the
cial methyl ethyl ketone. Platinum evaporating dishes were
weight is within 0.1 mg
...

This document is not an ASTM standard and is intended only to provide the user of an ASTM standard an indication of what changes have been made to the previous version. Because
it may not be technically possible to adequately depict all changes accurately, ASTM recommends that users consult prior editions as appropriate. In all cases only the current version
of the standard as published by ASTM is to be considered the official document.
Designation:D1353–03 Designation:D1353–09
Standard Test Method for
Nonvolatile Matter in Volatile Solvents for Use in Paint,
1
Varnish, Lacquer, and Related Products
This standard is issued under the fixed designation D 1353; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
This standard has been approved for use by agencies of the Department of Defense.
1. Scope*
1.1 This test method covers the determination of the nonvolatile matter in volatile solvents for use in paint, varnish, lacquer,
and related products.
1.2The following applies to all specified limits in this standard; for purposes of determining conformance with this standard, an
observed value or a calculated value shall be rounded off “to the nearest unit” in the last right-hand digit used in expressing the
specification limit, in accordance with the rounding-off method of Practice E29.
1.3The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.
1.4
1.2 The following applies to all specified limits in this standard; for purposes of determining conformance with this standard,
an observed value or a calculated value shall be rounded off “to the nearest unit” in the last right-hand digit used in expressing
the specification limit, in accordance with the rounding-off method of Practice E 29.
1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.4 For hazard information and guidance, see the supplier’s Material Safety Data Sheet for materials listed in this test method.
1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility
of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory
limitations prior to use. For specific hazard statements, see Section 5.
1.5For hazard information and guidance, see the supplier’s Material Safety Data Sheet for materials listed in this test method.
2. Referenced Documents
2
2.1 ASTM Standards:
E29 Practice for Using Significant Digits in Test Data to Determine Conformance with Specifications
E 180 Practice for Determining the Precision Data of ASTM Methods for Analysis and Testing of Industrial and Specialty
Chemicals
E 299 Test Method for Trace Amounts of Peroxide in Organic Solvents
E29Practice for Using Significant Digits in Test Data to Determine Conformance with Specifications Test Method for Trace
Amounts of Peroxides In Organic Solvents
3. Significance and Use
3.1 This test method describes the analytical measurement of residual matter in solvents that are intended to be 100 % volatile
at 105 6 5°C. Volatile solvents are used in the manufacture of paint, varnish, lacquer, and other related products, and the presence
of any residue may affect the product quality or efficiency of the process. This test method is useful in manufacturing control and
assessing compliance with specifications.
4. Apparatus
4.1 Oven, thermostatically controlled at 105 6 5°C.
4.2 Dish,evaporating,platinum,125-mL.Aplatinumevaporatingdishispreferred.Alternatively,analuminumorporcelaindish
may be used (see Note 1).
1
This test method is under the jurisdiction of ASTM Committee D01 on Paint and Related Coatings, Materials, and Applications and is the direct responsibility of
Subcommittee D01.35 on Solvents, Plasticizers, and Chemical Intermediates .
Current edition approved Dec.June 1, 2003.2009. Published December 2003.June 2009. Originally approved in 1954. Last previous edition approved in 20022003 as
D 1353 – 023.
2
For referencedASTM standards, visit theASTM website, www.astm.org, or contactASTM Customer Service at [e-mail]. For Annual Book ofASTM Standards
volume information, refer to the standard’s Document Summary page on the ASTM website.
*A Summary of Changes section appears at the end of this standard.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, United States.
1

---------------------- Page: 1 ----------------------
D1353–09
NOTE 1—Precision data were determined utilizing only platinum dishes.
4.3 Cylinder, graduated, 100-mL.
4.4 Analytical Balance, precision to 60.1 mg.
5. Hazards
5.1 Warning—Certain solvents
...