Standard Practice for Sampling of Coating Films

SIGNIFICANCE AND USE
Specimens for analysis must be adequately sampled, packaged, and documented to obtain meaningful information from the laboratory. The sampling procedure and packaging will be dependent upon the reason for taking the sample.
SCOPE
1.1 This practice covers methods to remove samples of coating films for subsequent analysis related to identification of generic coating type and failure analysis or other reasons. These techniques can be used in the field, the fabricating shop, or laboratory.
1.2 The method for obtaining coating samples for heavy metal analysis is presented in Practice D 5702.
1.3 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

General Information

Status
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Publication Date
31-Jan-2009
Current Stage
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NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
Designation: D6206 − 09
StandardPractice for
1
Sampling of Coating Films
This standard is issued under the fixed designation D6206; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope latex gloves. Contact the laboratory that will perform the
analysis to determine if any other precautions are needed.
1.1 This practice covers methods to remove samples of
Clean blades or knife between each sample with a rag soaked
coatingfilmsforsubsequentanalysisrelatedtoidentificationof
in solvent, or change blades between each sample.
generic coating type and failure analysis or other reasons.
4.1.2 The number and location of samples will vary depend-
These techniques can be used in the field, the fabricating shop,
ing upon the reason for sampling. Document the sampling
or laboratory.
location prior to obtaining the sample. Measure and record dry
1.2 The method for obtaining coating samples for heavy
filmthicknesses.Ifdelaminationispresent,measureandrecord
metal analysis is presented in Practice D5702.
dry film thickness of the coating remaining in the delaminated
1.3 The values stated in SI units are to be regarded as the
area as well as the intact area. Record the type of delamination,
standard. The values given in parentheses are for information
that is, adhesive or cohesive, and the color of the coating
only.
layer(s) where the delamination occurred. Document any other
visual defects such as alligatoring, mudcracking, checking,
1.4 This standard does not purport to address all of the
blistering, non-uniform appearance, or chalking.
safety concerns, if any, associated with its use. It is the
responsibility of the user of this standard to establish appro- 4.1.3 Obtain any history of the coating system available.
This should include when the coating was applied, the type of
priate safety and health practices and determine the applica-
bility of regulatory limitations prior to use. coating,andintendeddryfilmthicknesses.Obtainacopyofthe
painting specification, if possible, to verify the information.
2. Referenced Documents
4.1.4 Photograph the sample area before and after obtaining
2
2.1 ASTM Standards: the sample.
D4840 Guide for Sample Chain-of-Custody Procedures
4.1.5 Samples should be sent to the laboratory with a
D5702 Practice for Field Sampling of Coating Films for
chain-of-custody form, especially if there are existing or
Analysis for Heavy Metals
potential legal ramifications to the results of the laboratory
analysis. Guide D4840 presents the minimum requirements for
3. Significance and Use
sample chain-of-custody procedures.
3.1 Specimens for analysis must be adequately sampled,
4.2 Peeling Paint or Paint with Poor Adhesion:
packaged, and documented to obtain meaningful information
4.2.1 Samples should be taken that have not had both sides
from the laboratory. The sampling procedure and packaging
exposed to the elements. Make an incision approximately 5 cm
will be dependent upon the reason for taking the sample.
(2-in.) long in the coating using a sharp knife blade (such as a
utility knife). Hold the blade at a low angle to the surface and
4. Procedure
probe the incision by pushing forward on the knife.
4.1 General:
Alternatively, it may be possible to remove the sample by
4.1.1 Contaminating samples must be avoided. Hands must
cuttinga5cm (2-in.) square in the coating and peeling a
be kept clean by washing or wearing protective covers such as
sample by inserting the knife blade held at a low angle to the
surface at one of the edges of the incision. For brittle coatings,
1
masking tape may be used to hold the film together during
This practice is under the jurisdiction of ASTM Committee D01 on Paint and
Related Coatings, Materials, and Applications and is the direct responsibility of
removal.
Subcommittee D01.46 on Industrial Protective Coatings.
4.2.2 Obtain at least three samples, each sample being at
Current edition approved Feb. 1, 2009. Published February 2009. Originally
least 5 cm (2-in.) square. Smaller samples are allowed ifa5cm
approved in 1997. Last previous edition approved in 2003 as D6206 - 03. DOI:
10.1520/D6206-09.
(2-in.) square piece cannot be removed. Ensure that the three
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or
samples represent the same system. Place the samples in a
contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
plastic bag, aluminum foil, or envelope. Mark the outside of
Standards volume information, refer to the standard’s Document Summary page on
the ASTM website. the bag or envelope with the identity of the sample, includin
...

This document is not an ASTM standard and is intended only to provide the user of an ASTM standard an indication of what changes have been made to the previous version. Because
it may not be technically possible to adequately depict all changes accurately, ASTM recommends that users consult prior editions as appropriate. In all cases only the current version
of the standard as published by ASTM is to be considered the official document.
Designation:D6206–03 Designation: D 6206 – 09
Standard Practice for
1
Sampling of Coating Films
This standard is issued under the fixed designation D 6206; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope
1.1 This practice covers methods to remove samples of coating films for subsequent analysis related to identification of generic
coating type and failure analysis or other reasons. These techniques can be used in the field, the fabricating shop, or laboratory.
1.2 The method for obtaining coating samples for heavy metal analysis is presented in Practice D 5702.
1.3 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility
of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory
limitations prior to use.
2. Referenced Documents
2
2.1 ASTM Standards:
D 4840 Guide for Sampling Chain–of–Custody Procedures Guide for Sample Chain-of-Custody Procedures
D 5702 Practice for Field Sampling of Coating Films for Analysis for Heavy Metals
3. Significance and Use
3.1 Specimens for analysis must be adequately sampled, packaged, and documented to obtain meaningful information from the
laboratory. The sampling procedure and packaging will be dependent upon the reason for taking the sample.
4. Procedure
4.1 General:
4.1.1 Contaminating samples must be avoided. Hands must be kept clean by washing or wearing protective covers such as latex
gloves.Contactthelaboratorythatwillperformtheanalysistodetermineifanyotherprecautionsareneeded.Cleanbladesorknife
between each sample with a rag soaked in solvent, or change blades between each sample.
4.1.2 The number and location of samples will vary depending upon the reason for sampling. Document the sampling location
prior to obtaining the sample. Measure and record dry film thicknesses. If delamination is present, measure and record dry film
thickness of the coating remaining in the delaminated area as well as the intact area. Record the type of delamination, that is,
adhesive or cohesive, and the color of the coating layer(s) where the delamination occurred. Document any other visual defects
such as alligatoring, mudcracking, checking, blistering, non–-uniform appearance, or chalking.
4.1.3 Obtain any history of the coating system available. This should include when the coating was applied, the type of coating,
and intended dry film thicknesses. Obtain a copy of the painting specification, if possible, to verify the information.
4.1.4 Photograph the sample area before and after obtaining the sample.
4.1.5 Samples should be sent to the laboratory with a chain–of–custodychain-of-custody form, especially if there are existing
or potential legal ramifications to the results of the laboratory analysis. Guide D 4840 presents the minimum requirements for
sample chain–of–custodychain-of-custody procedures.
4.2 Peeling Paint or Paint with Poor Adhesion:
4.2.1 Samples should be taken that have not had both sides exposed to the elements. Make an incision approximately 5 cm
(2-in.) long in the coating using a sharp knife blade (such as a utility knife). Hold the blade at a low angle to the surface and probe
theincisionbypushingforwardontheknife.Alternatively,itmaybepossibletoremovethesamplebycuttinga5cm(2-in.)square
inthecoatingandpeelingasamplebyinsertingtheknifebladeheldat alowangletothesurfaceatoneoftheedgesoftheincision.
For brittle coatings, masking tape may be used to hold the film together during removal.
1
This practice is under the jurisdiction of ASTM Committee D01 on Paint and Related Coatings, Materials, and Applications and is the direct responsibility of
Subcommittee D01.46 on Industrial Protective Coatings.
Current edition approved Jan. 10, 2003. Published May 2003. Originally approved in 1997. Last previous edition approved in 1997 as D6206-97.
Current edition approved Feb. 1, 2009. Published February 2009. Originally approved in 1997. Last previous edition approved in 2003 as D 6206 - 03.
2
For referencedASTM standards, visit theASTM website, www.astm.org, or contactASTM Customer Service at service@astm.org. For Annual Book ofASTM Sta
...

This document is not an ASTM standard and is intended only to provide the user of an ASTM standard an indication of what changes have been made to the previous version. Because
it may not be technically possible to adequately depict all changes accurately, ASTM recommends that users consult prior editions as appropriate. In all cases only the current version
of the standard as published by ASTM is to be considered the official document.
Designation:D6206–03 Designation: D 6206 – 09
Standard Practice for
1
Sampling of Coating Films
This standard is issued under the fixed designation D 6206; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope
1.1 This practice covers methods to remove samples of coating films for subsequent analysis related to identification of generic
coating type and failure analysis or other reasons. These techniques can be used in the field, the fabricating shop, or laboratory.
1.2 The method for obtaining coating samples for heavy metal analysis is presented in Practice D 5702.
1.3 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility
of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory
limitations prior to use.
2. Referenced Documents
2
2.1 ASTM Standards:
D 4840 Guide for Sampling Chain–of–Custody Procedures Guide for Sample Chain-of-Custody Procedures
D 5702 Practice for Field Sampling of Coating Films for Analysis for Heavy Metals
3. Significance and Use
3.1 Specimens for analysis must be adequately sampled, packaged, and documented to obtain meaningful information from the
laboratory. The sampling procedure and packaging will be dependent upon the reason for taking the sample.
4. Procedure
4.1 General:
4.1.1 Contaminating samples must be avoided. Hands must be kept clean by washing or wearing protective covers such as latex
gloves.Contactthelaboratorythatwillperformtheanalysistodetermineifanyotherprecautionsareneeded.Cleanbladesorknife
between each sample with a rag soaked in solvent, or change blades between each sample.
4.1.2 The number and location of samples will vary depending upon the reason for sampling. Document the sampling location
prior to obtaining the sample. Measure and record dry film thicknesses. If delamination is present, measure and record dry film
thickness of the coating remaining in the delaminated area as well as the intact area. Record the type of delamination, that is,
adhesive or cohesive, and the color of the coating layer(s) where the delamination occurred. Document any other visual defects
such as alligatoring, mudcracking, checking, blistering, non–-uniform appearance, or chalking.
4.1.3 Obtain any history of the coating system available. This should include when the coating was applied, the type of coating,
and intended dry film thicknesses. Obtain a copy of the painting specification, if possible, to verify the information.
4.1.4 Photograph the sample area before and after obtaining the sample.
4.1.5 Samples should be sent to the laboratory with a chain–of–custodychain-of-custody form, especially if there are existing
or potential legal ramifications to the results of the laboratory analysis. Guide D 4840 presents the minimum requirements for
sample chain–of–custodychain-of-custody procedures.
4.2 Peeling Paint or Paint with Poor Adhesion:
4.2.1 Samples should be taken that have not had both sides exposed to the elements. Make an incision approximately 5 cm
(2-in.) long in the coating using a sharp knife blade (such as a utility knife). Hold the blade at a low angle to the surface and probe
theincisionbypushingforwardontheknife.Alternatively,itmaybepossibletoremovethesamplebycuttinga5cm(2-in.)square
inthecoatingandpeelingasamplebyinsertingtheknifebladeheldat alowangletothesurfaceatoneoftheedgesoftheincision.
For brittle coatings, masking tape may be used to hold the film together during removal.
1
This practice is under the jurisdiction of ASTM Committee D01 on Paint and Related Coatings, Materials, and Applications and is the direct responsibility of
Subcommittee D01.46 on Industrial Protective Coatings.
Current edition approved Jan. 10, 2003. Published May 2003. Originally approved in 1997. Last previous edition approved in 1997 as D6206-97.
Current edition approved Feb. 1, 2009. Published February 2009. Originally approved in 1997. Last previous edition approved in 2003 as D 6206 - 03.
2
For referencedASTM standards, visit theASTM website, www.astm.org, or contactASTM Customer Service at service@astm.org. For Annual Book ofASTM Sta
...

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