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ASTM

ASTM D5616-04

(Specification)

Standard Specification for Reclaimed Trichloroethylene

Standard Specification for Reclaimed Trichloroethylene

ABSTRACT
This specification covers the grades of trichloroethylene typically needed in various industries for noncritical applications such as in metal cleaning formulations. It may also be used as a reference document by purchasers or persons establishing in-house trichloroethylene recovery programs. The specimens are classified into three types: Type I— generally recognized for use in precision applications; Type II— for use in less-demanding precision applications; and Type III— may not be suitable for all applications. The three types of reclaimed trichloroethylene shall meet the specific gravity, nonvolatile residue, water content, assay percentage, 1,1,1 trichloroethane content, color in platinum-cobalt scale, appearance, acid acceptance, and acidity requirements.
SCOPE
1.1 This specification covers the grades of trichloroethylene typically needed in various industries for noncritical applications such as in metal cleaning formulations. It may be used as a reference document by purchasers or persons establishing in-house trichloroethylene recovery programs.

General Information

Status
Historical
Publication Date
31-Dec-2003
ICS
71.080.20 - Halogenated hydrocarbons
Technical Committee
D26 - Halogenated Organic Solvents and Fire Extinguishing Agents
Drafting Committee
D26.02 - Vapor Degreasing
Current Stage
Ref Project

Relations

Replaces
ASTM D5616-00 - Standard Specification for Reclaimed Trichloroethylene
Effective Date
01-Jan-2004
Replaced By
ASTM D5616-04(2010) - Standard Specification for Reclaimed Trichloroethylene
Effective Date
01-Feb-2010

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ASTM D5616-04 - Standard Specification for Reclaimed TrichloroethyleneASTM D5616-04 - Standard Specification for Reclaimed Trichloroethylene
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ASTM D5616-04 - Standard Specification for Reclaimed Trichloroethylene
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Standards Content (Sample)

NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information.
Designation: D5616 – 04
Standard Specification for
1
Reclaimed Trichloroethylene
This standard is issued under the fixed designation D5616; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope taining Halogenated Organic Solvents
D6806 Practice for Analysis of Halogenated Organic Sol-
1.1 This specification covers the grades of trichloroethyl-
2
vents and Their Admixtures by Gas Chromatography
ene typically needed in various industries for noncritical
5
2.2 Code of Federal Regulations:
applications such as in metal cleaning formulations. It may be
29 CFR 1910.1200 Department of Labor, OSHA Regula-
used as a reference document by purchasers or persons
tions, Hazard Communication
establishing in-house trichloroethylene recovery programs.
49 CFR Parts 100 to 199 Department of Transportation
2. Referenced Documents Hazardous Materials Regulations
3
2.1 ASTM Standards:
3. Classification
D1064 Test Methods for Iron in Rosin Tall Oil Fatty Acids
4 3.1 Type I—Generally recognized for use in precision ap-
and Other Related Products
plications.
D2108 Test Method for Color of Halogenated Organic
3.2 Type II—Use for less-demanding precision applications.
Solvents and Their Admixtures (Platinum-Cobalt Scale)
3.3 Type III—May not be suitable for all applications.
D2109 Test Methods for Nonvolatile Matter in Halogenated
Organic Solvents and Their Admixtures
4. Properties
D2111 Test Methods for Specific Gravity and Density of
4.1 Type I reclaimed trichloroethylene shall meet the re-
Halogenated Organic Solvents and Their Admixtures
quirements of Table 1.
D2942 Test Method for Total Acid Acceptance of Haloge-
4.2 Type II reclaimed trichloroethylene shall meet the re-
nated Organic Solvents (Nonreflux Methods)
quirements of Table 1.
D2989 Test Method for Acidity-Alkalinity of Halogenated
4.3 Type III reclaimed trichloroethylene shall meet the
Organic Solvents and Their Admixtures
requirements of Table 1.
D3401 Test Methods for Water in Halogenated Organic
Solvents and Their Admixtures
5. Packaging
D3741 Test Methods for Appearance of Admixtures Con-
5.1 Industrial or commercial quantities shall be packaged
and labeled in accordance with DOTregulations as found in 49
CFR100to199,inaccordancewithstateandlocalregulations,
1
This specification is under the jurisdiction of ASTM Committee D26 on
and in accordance with OSHA regulations found in 29 CFR
Halogenated Organic Solvents and Fire Extinguishing Agents and is the direct
1919.1200.
responsibility of Subcommittee D26.02 on
...

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4.1 High water concentrations can have a detrimental effect on many uses of halogenated solvents.  
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SCOPE
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1.1.2 Test Method B, Water Determination Using a Volumetric KF Titrator—The volumetric test method is a more traditional approach to KF water determinations. Although titrators are specifically designed for KF volumetric determinations, many automatic titrators on the market can be adapted to perform KF titrations.  
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