ASTM E1535-93(1998)
(Test Method)Standard Test Method for Performance Evaluation of Anaerobic Digestion Systems
Standard Test Method for Performance Evaluation of Anaerobic Digestion Systems
SCOPE
1.1 This test method is applicable to all anaerobic digestion systems.
1.2 This standard does not purport to address all of the safety problems, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.
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Designation:E1535–93 (Reapproved 1998)
Standard Test Method for
Performance Evaluation of Anaerobic Digestion Systems
This standard is issued under the fixed designation E 1535; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (e) indicates an editorial change since the last revision or reapproval.
1. Scope 5. Significance and Use
1.1 This test method is applicable to all anaerobic digestion 5.1 This test method will yield data that will form a
systems. performance profile for an anaerobic digester facility. The
1.2 This standard does not purport to address all of the significance of this profile is that it can be compared directly to
safety problems, if any, associated with its use. It is the another facility’s performance profile and yield a measurement
responsibility of the user of this standard to establish appro- of expected facility performance under field conditions.
priate safety and health practices and determine the applica- 5.2 This test method will also yield data that can be used to
bility of regulatory limitations prior to use. verify the operation of a system to a regulatory agency.
5.3 The single black box technique applied to performance
2. Referenced Documents
evaluation examines only the overall input/output relationship.
2.1 ASTM Standards:
This implies that the operation of the facility during the tests
E 1126 Terminology Relating to Biomass Fuels will be conducted to achieve design conditions in accordance
2.2 Standard Methods (SM) for Analysis of Water and
with established procedures.
Wastewater:
6. Procedure
2540 D Total Suspended Solids
2720 B Sludge Digester Gas (Volume) 6.1 Conduct the test for a predetermined period mutually
+
4500 FNH Nitrogen (Ammonia) agreed upon by all parties participating in the testing program.
4500 B Nitrogen (Organic), Total Kjeldahl Nitrogen Start the test period when the system manufacturer determines
5210 B Biochemical Oxygen Demand that the system has reached normal operating conditions.
5220 B Chemical Oxygen Demand Record the time period between the initial loading of the
5520 D Oil and Grease system with waste and the start of the test period.Aminimum
test period of 90 days is suggested.
3. Terminology
6.2 Determine the influent and effluent concentrationsofthe
3.1 Definition—see Terminology E 1126. following, using the methods recommended, total suspended
+
3.1.1 biogas—a composition of methane and carbon diox-
solids (TSS) SM 2540 D, NH nitrogen (ammonia) (AN) SM
ide and minor constituents produced by the digestion of 4500 F, nitrogen (organic)-total kjeldahl nitrogen (TKN) SM
organic substrates in the absence of oxygen.
4500 B, biochemical oxygen demand (BOD) SM 5210 B,
chemical oxygen demand (COD) SM 5220 B, and oil and
4. Summary of Test Method
grease (OG) SM 5520 D.The sampling frequency and location
4.1 This test method measures the concentration and mass
of sampling shall be mutually agreed upon by all parties
oftheinfluentandeffluentwastes,respectively,aswellasother
involved in the project. As a minimum, weekly sampling of a
operational parameters such as input energy, output gas pro-
composite sample of 24 h of influent and effluent is suggested.
duction, and waste biomass, to provide a methodology for
6.3 Measure the gas production continuously, using SM
evaluation of the operation of an aerobic digester.
2720 B, or equivalent. Analyze the gas compositions using a
gas chromatograph (GC) to determine the composition of CH .
1 The GC analysis frequency shall be mutually agreed upon by
This test method is under the jurisdiction of ASTM Committee E48 on
Biotechnology and is the direct responsibility of Subcommittee E48.05 on Biomass all parties participating in the testing program.
Conversion.
6.4 Measure the thermal energy input. The most common
Current edition approved March 15, 1993. Published May 1993.
method of thermal energy input is hot water supplied to the
For referenced ASTM standards, visit the ASTM website, www.astm.org, or
system using a heat exchanger. Monitor the energy input on a
contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
Standards volume information, refer to the standard’s Document Summary page on continuous basis by measuring the flow rate of hot water to the
the ASTM website.
system and the influent and effluent flow temperatures, using
Available from American Public Health Association, 1015 15th St. N.W.,
the reference procedures and equipment.
Washington, DC 20005.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, United States.
E1535–93 (1998)
TABLE 2 Performance Calculation Procedures
6.5 Record the horsepower of any motors connected more
than 50 % of the time during a 24 h operation.
6.6 Record the weight of any material removed from the Calculation Results
system during the test period.
(1) Influent mass calculations
TSSM = TSS 3 WF 3 WD _____lb
I I
ANM =AN 3 WF 3 WD _____lb
7. Calculation
I I
TKNM = TKN 3 WF 3 WD _____lb
I I
7.1 Data Collection—See Table 1
BODM = BOD 3 WF 3 WD _____lb
I I
CODM = COD 3 WF 3 WD _____lb
7.2 Data Calculations—SeeTable 2 I I
OGM =OG 3 WF 3 WD _____lb
I I
7.3 Data Summary—See Table 3
(2) Effluent mass calculations
TSSM = TSS 3 WF 3 WD _____lb
E E
8. Precision and Bias
ANM =AN 3 WF 3 WD _____lb
E E
TKNM = TKN 3 WF 3 WD _____lb
E E
8.1 The precision and bias of this test method are still under
BODM = BOD 3 WF 3 WD _____lb
E E
evaluation.
CODM = COD 3 WF 3 WD _____lb
E E
OGM =OG 3 WF 3 WD _____lb
E E
9. Keywords (3) Pollutant reduction
Total suspended solids
9.1 anaerobic digestion; biogas; biomass; waste treatment
reduction = (TSSM − TSSM)/TSSM _____ %
E I I
Ammonia nitrogen
reduction = (ANM − ANM)/ANM _____%
E I I
Total Kjeldahl nitrogen
reduction = (TKNM − TKNM)/TKNM _____%
E I I
Biochemical oxygen
demand reduction = (BODM − BODM)/BODM _____%
E I I
Chemical oxygen demand
reduction = (CODM − CODM)/CODM _____%
E I I
Oil and grease reduction = (OGM − OGM)/OGM ____
...
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