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ASTM D8133-18

(Test Method)

Standard Test Method for Determination of Low Level Phthalates in Poly(Vinyl Chloride) Plastics by Solvent Extraction—Gas Chromatography/Mass Spectrometry

Standard Test Method for Determination of Low Level Phthalates in Poly(Vinyl Chloride) Plastics by Solvent Extraction—Gas Chromatography/Mass Spectrometry

SIGNIFICANCE AND USE
5.1 Identification and Quantification of Phthalates—DBP, BBP, DEHP, DNOP, DINP and DIDP are representative of the phthalates either banned or being monitored by a variety of regulations. Regulations include: EU—Directive 2005/84/EC, US—Consumer Product Safety Improvement Act of 2008 – section 108, Japan—Health, Labor and Welfare Ministry guideline No. 336 (2010) and IEC 62321-8:2017. These test methods provide a procedure to identify and quantify phthalates in PVC.  
5.2 Other techniques successfully used to separate and identify phthalates in PVC include TD-GC/MS (ASTM D7823), GC/MS, HPLC/UV, HPLC/MS, FTIR, and GC/FID (flame ionization detector).
SCOPE
1.1 This test method provides a procedure to quantify six phthalates by solvent extraction of plasticized PVC articles followed by analysis of the extract by gas chromatography/mass spectrometry. Six phthalates, BBP, DBP, DEHP, DNOP, DINP, and DIDP, are used to illustrate how to implement the method.
Note 1: The method can be extended to other phthalates in a wide range of polymeric substrates.  
1.2 Within the context of this method, “low level” is defined as 1000 ppm.  
1.3 The values in SI units are to be regarded as standard.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
Note 2: There is no known ISO equivalent to this standard.  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

General Information

Status
Historical
Publication Date
31-Oct-2018
ICS
83.080.20 - Thermoplastic materials
Technical Committee
D20 - Plastics
Drafting Committee
D20.70 - Analytical Methods
Current Stage
Ref Project

Relations

Replaces
ASTM D8133-17 - Standard Test Method for Determination of Low Level, Regulated Phthalates in Poly(Vinyl Chloride) Plastics by Solvent Extraction—Gas Chromatography/Mass Spectrometry
Effective Date
01-Nov-2018
Referred By
ASTM D7176-22 - Standard Specification for Non-Reinforced Polyvinyl Chloride (PVC) Geomembranes Used in Buried Applications
Effective Date
01-Nov-2018

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ASTM D8133-18 - Standard Test Method for Determination of Low Level Phthalates in Poly(Vinyl Chloride) Plastics by Solvent Extraction—Gas Chromatography/Mass SpectrometryASTM D8133-18 - Standard Test Method for Determination of Low Level Phthalates in Poly(Vinyl Chloride) Plastics by Solvent Extraction—Gas Chromatography/Mass Spectrometry
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ASTM D8133-18 - Standard Test Method for Determination of Low Level Phthalates in Poly(Vinyl Chloride) Plastics by Solvent Extraction—Gas Chromatography/Mass Spectrometry
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REDLINE ASTM D8133-18 - Standard Test Method for Determination of Low Level Phthalates in Poly(Vinyl Chloride) Plastics by Solvent Extraction—Gas Chromatography/Mass SpectrometryREDLINE ASTM D8133-18 - Standard Test Method for Determination of Low Level Phthalates in Poly(Vinyl Chloride) Plastics by Solvent Extraction—Gas Chromatography/Mass Spectrometry
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Standards Content (Sample)

NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
Designation: D8133 − 18
Standard Test Method for
Determination of Low Level Phthalates in Poly(Vinyl
Chloride) Plastics by Solvent Extraction—Gas
1
Chromatography/Mass Spectrometry
This standard is issued under the fixed designation D8133; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope* D3465 Test Method for Purity of Monomeric Plasticizers by
Gas Chromatography
1.1 This test method provides a procedure to quantify six
D7083 Practice for Determination of Monomeric Plasticiz-
phthalates by solvent extraction of plasticized PVC articles
ers in Poly (Vinyl Chloride) (PVC) by Gas Chromatogra-
followed by analysis of the extract by gas chromatography/
phy
mass spectrometry. Six phthalates, BBP, DBP, DEHP, DNOP,
D7823 Test Method for Determination of Low Level, Regu-
DINP, and DIDP, are used to illustrate how to implement the
lated Phthalates in Poly (Vinyl Chloride) Plastics by
method.
Thermal Desorption—Gas Chromatography/Mass Spec-
NOTE 1—The method can be extended to other phthalates in a wide
trometry
range of polymeric substrates.
D7993 Guide for Analyzing Complex Phthalates
1.2 Withinthecontextofthismethod,“lowlevel”isdefined
E177 Practice for Use of the Terms Precision and Bias in
as 1000 ppm.
ASTM Test Methods
E355 Practice for Gas Chromatography Terms and Relation-
1.3 The values in SI units are to be regarded as standard.
ships
1.4 This standard does not purport to address all of the
E594 Practice for Testing Flame Ionization Detectors Used
safety concerns, if any, associated with its use. It is the
in Gas or Supercritical Fluid Chromatography
responsibility of the user of this standard to establish appro-
E691 Practice for Conducting an Interlaboratory Study to
priate safety, health, and environmental practices and deter-
Determine the Precision of a Test Method
mine the applicability of regulatory limitations prior to use.
IEEE/ASTM SI-10 Practice for Use of the International
NOTE 2—There is no known ISO equivalent to this standard.
System of Units (SI), the Modernized Metric System
2.2 ASTM Adjuncts:ADJD7823-EA
1.5 This international standard was developed in accor-
Vinyl Plasticizer Library—Total Ion Chromatograms and
dance with internationally recognized principles on standard-
Mass Spectra
ization established in the Decision on Principles for the
3
Development of International Standards, Guides and Recom-
2.3 CPSC Standard:
mendations issued by the World Trade Organization Technical
CPSC-CH-C1001–09.3 Standard Operating Procedure for
Barriers to Trade (TBT) Committee.
Determination of Phthalates
2. Referenced Documents
3. Terminology
2
2.1 ASTM Standards:
3.1 Definitions:
D883 Terminology Relating to Plastics
3.1.1 For definition of plastic terms used in this standard,
D1600 Terminology forAbbreviatedTerms Relating to Plas-
see Terminologies D883 and D1600.
tics
3.2 For units, symbols, and abbreviations used in this
standard refer to Practices E594, E355,or IEEE/ASTM SI-10.
1
This test method is under the jurisdiction ofASTM Committee D20 on Plastics
3.3 Compounds and Instrumentation:
and is the direct responsibility of Subcommittee D20.70 on Analytical Methods.
3.3.1 (DOA) Hexanedioic acid, 1,6-bis(2-ethylhexyl) ester
Current edition approved Nov. 1, 2018. Published November 2018. Originally
CAS #103-23-1
approved in 2017. Last previous edition approved in 2017 as D8133 – 17. DOI:
10.1520/D8133-18.
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or
contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
3
Standards volume information, refer to the standard’s Document Summary page on Available from U.S. Consumer Product Safety Commission (CPSC), 4330 East
the ASTM website. West Hwy., Bethesda, MD 20814, http://www.cpsc.gov.
*A Summary of Changes section appears at the end of this standard
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
1

---------------------- Page: 1 ----------------------
D8133 − 18
3.3.2 (DINCH) 1,2-Cyclohexanedicarboxylic acid, dinonyl 5. Significance and Use
ester, branched and linear CAS #474919-59-0
5.1 Identification and Quantification of Phthalates—DBP,
3.3.3 (DBP) 1,2-Benzenedicarboxylic acid, 1,2-di-n-butyl
BBP, DEHP, DNOP, DINP and DIDP are representative of the
ester CAS #84-74-2
phthalates either banned or being monitored by a variety of
3.3.4 (BBP) Benzyl butyl phthalate CAS #85-68-7
regulations. Regulations include: EU—Directive 2005/84/EC,
3.3.5 (DEHP) Bis(2-ethyhexyl) phthalate CAS #117-81-7
US—Consumer Product Safety Improvement Act of
...

This document is not an ASTM standard and is intended only to provide the user of an ASTM standard an indication of what changes have been made to the previous version. Because
it may not be technically possible to adequately depict all changes accurately, ASTM recommends that users consult prior editions as appropriate. In all cases only the current version
of the standard as published by ASTM is to be considered the official document.
Designation: D8133 − 17 D8133 − 18
Standard Test Method for
Determination of Low Level, Regulated Level Phthalates in
Poly(Vinyl Chloride) Plastics by Solvent Extraction—Gas
1
Chromatography/Mass Spectrometry
This standard is issued under the fixed designation D8133; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope Scope*
1.1 This test method provides a procedure to quantify six phthalates by solvent extraction of plasticized PVC articles followed
by analysis of the extract by gas chromatography/mass spectrometry. The phthalates which are quantified are Six phthalates, BBP,
DBP, DEHP, DNOP, DINP, and DIDP.DIDP, are used to illustrate how to implement the method.
NOTE 1—The method can be extended to other phthalates.phthalates in a wide range of polymeric substrates.
1.2 Within the context of this method, “low level” is defined as 1000 ppm.
1.3 The values in SI units are to be regarded as standard.
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility
of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of
regulatory limitations prior to use.
NOTE 2—There is no known ISO equivalent to this standard.
1.5 This international standard was developed in accordance with internationally recognized principles on standardization
established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued
by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
2. Referenced Documents
2
2.1 ASTM Standards:
D883 Terminology Relating to Plastics
D1600 Terminology for Abbreviated Terms Relating to Plastics
D3465 Test Method for Purity of Monomeric Plasticizers by Gas Chromatography
D7083 Practice for Determination of Monomeric Plasticizers in Poly (Vinyl Chloride) (PVC) by Gas Chromatography
D7823 Test Method for Determination of Low Level Phthalates in Poly (Vinyl Chloride) Plastics by Thermal Desorption—Gas
Chromatography/Mass Spectrometry
D7993 Guide for Analyzing Complex Phthalates
E177 Practice for Use of the Terms Precision and Bias in ASTM Test Methods
E355 Practice for Gas Chromatography Terms and Relationships
E594 Practice for Testing Flame Ionization Detectors Used in Gas or Supercritical Fluid Chromatography
E691 Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method
IEEE/ASTM SI-10 Practice for Use of the International System of Units (SI), the Modernized Metric System
2.2 ASTM Adjuncts:ADJD7823-EA
Vinyl Plasticizer Library—Total Ion Chromatograms and Mass Spectra
3
2.3 CPSC Standard:
CPSC-CH-C1001–09.3 Standard Operating Procedure for Determination of Phthalates
1
This test method is under the jurisdiction of ASTM Committee D20 on Plastics and is the direct responsibility of Subcommittee D20.70 on Analytical Methods.
Current edition approved Aug. 1, 2017Nov. 1, 2018. Published November 2017November 2018. Originally approved in 2017. Last previous edition approved in 2017 as
D8133 – 17. DOI: 10.1520/D8133-17.10.1520/D8133-18.
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM Standards
volume information, refer to the standard’s Document Summary page on the ASTM website.
3
Available from U.S. Consumer Product Safety Commission (CPSC), 4330 East West Hwy., Bethesda, MD 20814, http://www.cpsc.gov.
*A Summary of Changes section appears at the end of this standard
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
1

---------------------- Page: 1 ----------------------
D8133 − 18
3. Terminology
3.1 Definitions:
3.1.1 For definition of plastic terms used in this standard, see Terminologies D883 and D1600.
3.2 For units, symbols, and abbreviations used in this standard refer to Practices E594, E355, or IEEE/ASTM SI-10.
3.3 Compounds and Instrumentation:
3.3.1 (DOA) Hexanedioic acid, 1,6-bis(2-ethylhexyl) ester CAS #103-23-1
3.3.2 (DINCH) 1,2-Cyclohexanedicarboxylic acid, dinonyl ester, branched and linear CAS #474919-59-0
3.3.3 (DBP) 1,2-Benzenedicarboxylic acid, 1,2-di-n-butyl ester CAS #84-74-2
3.3.4 (BBP) B
...

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1.2 This classification system allows for the use of segmented block copolyether-ester elastomers that are recycled provided that the requirements as stated in this classification system are met. The proportions of recycled material used, as well as the nature and amount of any contaminant, however, cannot be covered practically in this specification.  
1.3 The properties included in this classification system are those required to identify the compositions covered. It is possible that there are other requirements necessary to identify particular characteristics important to specialized applications. One way of specifying them is by using the suffixes as given in Section 5.  
1.4 This classification system and subsequent line callout (specification) are intended to provide a means of calling out plastic materials used in the fabrication of end items or parts. It is not intended for the selection of materials. Material selection is best made by those having expertise in the plastic field after careful consideration of the design and the performance required of the part, the environment to which it will be exposed, the fabrication process to be employed, the costs involved, and the inherent properties of the material other than those covered by this classification system.  
1.5 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.6 The following precautionary caveat pertains only to the test methods portion, Section 11, of this classification system. This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
Note 1: This standard, ISO 20029-1, and ISO 20029-2 address the same subject matter, but differ in technical content.  
1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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ASTM
ASTM D3030-23(Test Method)
Standard Test Method for Volatile Matter (Including Water) of Vinyl Chloride Resins

SIGNIFICANCE AND USE
5.1 The quantity of volatile components in a vinyl chloride resin can be established by this test method. This test method does not identify the components.
SCOPE
1.1 This test method covers the quantitative determination of the volatile matter (including water) present in vinyl chloride resins.  
1.2 The values stated in SI units are to be regarded as standard.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
Note 1: This test method is identical ISO 1269.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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ASTM
ASTM D4878-23(Test Method)
Standard Test Methods for Polyurethane Raw Materials: Determination of Viscosity of Polyols

SIGNIFICANCE AND USE
4.1 These test methods are suitable for research or as quality control or specification tests.  
4.2 Viscosity measures the resistance of a fluid to uniformly continuous flow without turbulence or other forces.
SCOPE
1.1 These test methods (A and B) determine the viscosity of polyols in the range from 10 to 100 000 mPa·s(cP) at 25°C. Test Method A is a rotational procedure for determining dynamic viscosity. Test Method B is a general procedure for kinematic viscosity of transparent polyols. (See Note 1.)  
1.2 The values stated in SI units are to be regarded as the standard. Other equivalent units are provided because of current common usage.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
Note 1: Test Method A is equivalent to ISO 3219. Test Method B is equivalent to ISO 3104.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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ASTM
ASTM D3275-18(2023)(Classification)
Standard Classification System for E-CTFE-Fluoroplastic Molding, Extrusion, and Coating Materials

ABSTRACT
This classification system covers melt processible molding, extrusion, and coating materials of ethylene-chlorotrifluoroethylene (E-CTFE) fluoroplastics. The resin is a copolymer of ethylene and chlorotrifluoroethylene. The classification of ECTFE materials into groups in accordance with their physical appearance, and further into classes based on melt flow rate, is provided. The test specimens shall be subjected to tests to determine their melt flow rate, melting endotherm peak, specific gravity, tensile property, dielectric constant and dissipation factor, and oxygen index.
SCOPE
1.1 This classification system covers melt processible molding, extrusion, and coating materials of ethylene-chlorotrifluoroethylene (E-CTFE) fluoroplastics. The resin is a copolymer of ethylene and chlorotrifluoroethylene containing approximately 80 weight % of chlorotrifluoroethylene.  
1.2 The values stated in SI units, as detailed in IEEE/ASTM SI-10, are to be regarded as standard.  
1.3 The following precautionary statement pertains only to the test methods portion, Section 11 of this classification system. This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
Note 1: Although this classification system and ISO 20568-1 and ISO 20568-2 differ in approach or detail, data obtained using either are technically equivalent.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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