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ASTM C183/C183M-15

(Practice)

Standard Practice for Sampling and the Amount of Testing of Hydraulic Cement

Standard Practice for Sampling and the Amount of Testing of Hydraulic Cement

SIGNIFICANCE AND USE
4.1 The sampling procedures described are intended for use in the procurement of samples of hydraulic cement after it has been manufactured and is ready to be offered for sale. They are not intended as sampling procedures for quality control purposes during manufacturing. The testing procedures outlined cover the amount of testing to be done and provide guidance for reporting on conformance or non-conformance of cements with requirements of purchase specifications.  
4.2 This practice is referenced as the procedure for sampling natural cement (Specification C10/C10M), masonry cement (Specification C91/C91M), portland cement (Specification C150/C150M), blended hydraulic cement (Specification C595/C595M), expansive hydraulic cement (Specification C845/C845M), hydraulic cement based on a performance specification (Specification C1157/C1157M), plastic stucco cement (Specification C1328/C1328M), and mortar cement (Specification C1329/C1329M), and  
4.3 Most building codes and construction specifications require that hydraulic cement to be used in the work meet the applicable requirements of the relevant purchase specifications, such as Specifications C10/C10M, C91/C91M, C150/C150M, C595/C595M, C1157/C1157M, C1328/C1328M, C1329/C1329M, or C845/C845M. If the code or specification requires sampling of the manufactured cement, the provisions given in 4.4 are applicable. Not much cement is sold on the basis of such sampling and testing. A useful discussion of sampling and testing cement is contained in ACI 225.1R.  
4.4 The procedures covered in this practice should be done by or for purchasers of hydraulic cement who are using a code or specification that requires sampling and testing to determine if the samples conform to the relevant acceptance specifications. The testing is done using specified methods to determine whether the samples yield test results that conform to the specification, and the tests serve as a basis for acceptance or rejection of the lot of material ...
SCOPE
1.1 This practice covers procedures for sampling and for the amount of testing of hydraulic cement after it has been manufactured and is ready to be offered for sale.  
1.2 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the two systems may result in non-conformance with the standard. Values in SI units [or inch-pound units] shall be obtained by measurement in SI units [or inch-pound units] or by appropriate conversion, using the Rules for Conversion and Rounding given in Standard IEEE/ASTM SI 10, Values are stated in only SI units when inch-pound units are not used in practice  
1.3 The text of this standard references notes and footnotes which provide explanatory material. These notes and footnotes (excluding those in tables and figures) shall not be considered requirements of the standard.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

General Information

Status
Historical
Publication Date
31-Mar-2015
ICS
91.100.10 - Cement. Gypsum. Lime. Mortar
Technical Committee
C01 - Cement
Drafting Committee
C01.95 - Coordination of Standards
Current Stage
Ref Project

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ASTM C183/C183M-15 - Standard Practice for Sampling and the Amount of Testing of Hydraulic CementASTM C183/C183M-15 - Standard Practice for Sampling and the Amount of Testing of Hydraulic Cement
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NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
Designation: C183/C183M − 15
StandardPractice for
1
Sampling and the Amount of Testing of Hydraulic Cement
This standard is issued under the fixed designation C183/C183M; the number immediately following the designation indicates the year
of original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval.
A superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
This standard has been approved for use by agencies of the U.S. Department of Defense.
1. Scope C114 Test Methods for Chemical Analysis of Hydraulic
Cement
1.1 Thispracticecoversproceduresforsamplingandforthe
C115 Test Method for Fineness of Portland Cement by the
amount of testing of hydraulic cement after it has been
Turbidimeter
manufactured and is ready to be offered for sale.
C150/C150M Specification for Portland Cement
1.2 The values stated in either SI units or inch-pound units
C151/C151M Test Method for Autoclave Expansion of Hy-
are to be regarded separately as standard. The values stated in
draulic Cement
each system may not be exact equivalents; therefore, each
C157/C157M Test Method for Length Change of Hardened
system shall be used independently of the other. Combining
Hydraulic-Cement Mortar and Concrete
values from the two systems may result in non-conformance
C185 Test Method for Air Content of Hydraulic Cement
with the standard.Values in SI units [or inch-pound units] shall
Mortar
be obtained by measurement in SI units [or inch-pound units]
C186 Test Method for Heat of Hydration of Hydraulic
or by appropriate conversion, using the Rules for Conversion
Cement
andRoundinggiveninStandardIEEE/ASTMSI10,Valuesare
C191 TestMethodsforTimeofSettingofHydraulicCement
stated in only SI units when inch-pound units are not used in
by Vicat Needle
practice
C204 Test Methods for Fineness of Hydraulic Cement by
1.3 The text of this standard references notes and footnotes Air-Permeability Apparatus
C227 Test Method for Potential Alkali Reactivity of
which provide explanatory material. These notes and footnotes
(excluding those in tables and figures) shall not be considered Cement-Aggregate Combinations (Mortar-Bar Method)
C266 Test Method for Time of Setting of Hydraulic-Cement
requirements of the standard.
Paste by Gillmore Needles
1.4 This standard does not purport to address all of the
C430 Test Method for Fineness of Hydraulic Cement by the
safety concerns, if any, associated with its use. It is the
45-µm (No. 325) Sieve
responsibility of the user of this standard to establish appro-
C451 Test Method for Early Stiffening of Hydraulic Cement
priate safety and health practices and determine the applica-
(Paste Method)
bility of regulatory limitations prior to use.
C452/C452M Test Method for Potential Expansion of
Portland-Cement Mortars Exposed to Sulfate
2. Referenced Documents
C595/C595M Specification for Blended Hydraulic Cements
2
2.1 ASTM Standards:
C806 Test Method for Restrained Expansion of Expansive
C10/C10M Specification for Natural Cement
Cement Mortar
C91/C91M Specification for Masonry Cement
C807 Test Method for Time of Setting of Hydraulic Cement
C109/C109M Test Method for Compressive Strength of
Mortar by Modified Vicat Needle
Hydraulic Cement Mortars (Using 2-in. or [50-mm] Cube
C845/C845M Specification for Expansive Hydraulic Ce-
Specimens)
ment
C1012/C1012M Test Method for Length Change of
Hydraulic-Cement Mortars Exposed to a Sulfate Solution
1
ThispracticeisunderthejurisdictionofASTMCommitteeC01onCementand
C1038/C1038M Test Method for Expansion of Hydraulic
is the direct responsibility of Subcommittee C01.95 on Coordination of Standards.
Cement Mortar Bars Stored in Water
Current edition approved April 1, 2015. Published April 2015. Originally
C1157/C1157M Performance Specification for Hydraulic
approved in 1944. Last previous edition approved in 2013 as C183 – 13. DOI:
10.1520/C0183_C0183M-15.
Cement
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or
C1328/C1328M Specification for Plastic (Stucco) Cement
contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
C1329/C1329M Specification for Mortar Cement
Standards volume information, refer to the standard’s Document Summary page on
the ASTM website. C1357 Test Methods for Evaluating Masonry Bond Strength
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
1

---------------------- Page: 1 ----------------------
C183/C183M − 15
C1506 Test Method for Water Retention of Hydraulic 4.4 The procedures covered in this practice should be done
Cement-Based Mortars and Plasters by or for purchasers of hydraulic cement who are using a code
E11 Specification for Woven Wire Test Sieve Cloth and Test or specification that requires
...

This document is not an ASTM standard and is intended only to provide the user of an ASTM standard an indication of what changes have been made to the previous version. Because
it may not be technically possible to adequately depict all changes accurately, ASTM recommends that users consult prior editions as appropriate. In all cases only the current version
of the standard as published by ASTM is to be considered the official document.
Designation: C183 − 13 C183/C183M − 15
Standard Practice for
1
Sampling and the Amount of Testing of Hydraulic Cement
This standard is issued under the fixed designation C183;C183/C183M; the number immediately following the designation indicates the
year of original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last
reapproval. A superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
This standard has been approved for use by agencies of the U.S. Department of Defense.
1. Scope
1.1 This practice covers procedures for sampling and for the amount of testing of hydraulic cement after it has been
manufactured and is ready to be offered for sale.
1.2 The values stated in either SI units or inch-pound units are to be regarded separately as the standard. The inch-pound units
in parentheses are for information purposes only.standard. The values stated in each system may not be exact equivalents;
therefore, each system shall be used independently of the other. Combining values from the two systems may result in
non-conformance with the standard. Values in SI units [or inch-pound units] shall be obtained by measurement in SI units [or
inch-pound units] or by appropriate conversion, using the Rules for Conversion and Rounding given in Standard IEEE/ASTM SI
10, Values are stated in only SI units when inch-pound units are not used in practice
1.2.1 A ton as used in this practice is 907 kg (2000 lb).
1.2.2 Values in SI units shall be obtained by measurement in SI units or by appropriate conversion, using the Rules for
Conversion and Rounding given in Standard IEEE/ASTM SI 10, of measurement made in other units.
1.3 The text of this standard references notes and footnotes which provide explanatory material. These notes and footnotes
(excluding those in tables and figures) shall not be considered requirements of the standard.
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility
of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory
limitations prior to use.
2. Referenced Documents
2
2.1 ASTM Standards:
C10/C10M Specification for Natural Cement
C91C91/C91M Specification for Masonry Cement
C109/C109M Test Method for Compressive Strength of Hydraulic Cement Mortars (Using 2-in. or [50-mm] Cube Specimens)
C114 Test Methods for Chemical Analysis of Hydraulic Cement
C115 Test Method for Fineness of Portland Cement by the Turbidimeter
C150C150/C150M Specification for Portland Cement
C151C151/C151M Test Method for Autoclave Expansion of Hydraulic Cement
C157/C157M Test Method for Length Change of Hardened Hydraulic-Cement Mortar and Concrete
C185 Test Method for Air Content of Hydraulic Cement Mortar
C186 Test Method for Heat of Hydration of Hydraulic Cement
C191 Test Methods for Time of Setting of Hydraulic Cement by Vicat Needle
C204 Test Methods for Fineness of Hydraulic Cement by Air-Permeability Apparatus
C227 Test Method for Potential Alkali Reactivity of Cement-Aggregate Combinations (Mortar-Bar Method)
C265 Test Method for Water-Extractable Sulfate in Hydrated Hydraulic Cement Mortar
C266 Test Method for Time of Setting of Hydraulic-Cement Paste by Gillmore Needles
C430 Test Method for Fineness of Hydraulic Cement by the 45-μm (No. 325) Sieve
C451 Test Method for Early Stiffening of Hydraulic Cement (Paste Method)
1
This practice is under the jurisdiction of ASTM Committee C01 on Cement and is the direct responsibility of Subcommittee C01.95 on Coordination of Standards.
Current edition approved Aug. 1, 2013April 1, 2015. Published September 2013April 2015. Originally approved in 1944. Last previous edition approved in 20082013 as
C183 – 08.C183 – 13. DOI: 10.1520/C0183-13.10.1520/C0183_C0183M-15.
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM Standards
volume information, refer to the standard’s Document Summary page on the ASTM website.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
1

---------------------- Page: 1 ----------------------
C183/C183M − 15
C452C452/C452M Test Method for Potential Expansion of Portland-Cement Mortars Exposed to Sulfate
C595/C595M Specification for Blended Hydraulic Cements
C563C806 Test Method for Approximation of Optimum SORestrained Expansi
...

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Standard Test Method for Drying Shrinkage of Mortar Containing Hydraulic Cement

SIGNIFICANCE AND USE
4.1 This test method establishes a selected set of conditions of temperature, relative humidity and rate of evaporation of the environment to which a mortar specimen of stated composition shall be subjected for a specified period of time during which its change in length is determined and designated “drying shrinkage.”  
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1.1 This test method determines the change in length on drying of mortar bars containing hydraulic cement and graded standard sand.  
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These test methods cover the chemical analyses of hydraulic cements. Specific chemical test methods are grouped as reference test methods and alternative test methods. The reference test methods are long accepted classical chemical test methods which provide a reasonably well-integrated basic scheme of analysis for hydraulic cements and are also required for referee analysis in those cases where conformance to chemical specification requirements are questioned. Apparatus and materials for the test method include balance, weights, glassware and laboratory containers, desiccators, filter paper, crucibles, and muffle furnace. Standard reagents for the test method shall be used within the limits of the specification. These reagents shall include purity agents, water, repackaged reagents, concentrated acids and ammonium hydroxide, nonstandardized solutions, and indicator solutions. Sample preparation and general test procedures shall be followed according to the specification. General procedures include sample weighing, taring of crucibles, weighing of ignited residues, volatilization of platinum, chemical analyses, and calculation. Reporting of analyses shall be of the following order: major components, minor components, and separate determinations. Reference test methods and procedures include determination of insoluble residue, silicon dioxide, ammonium hydroxide group, ferric oxide, phosphorus pentoxide, titanium dioxide, zinc oxide, aluminum oxide, calcium oxide, magnesium oxide, sulfur, loss on ignition, sodium and potassium oxides, manganic oxide, chloride, chloroform-soluble organic substances. Alternative test methods and procedures include determination of calcium oxide, calcium dioxide, magnesium oxide, loss on ignition, titanium dioxide, phosphorus pentoxide, manganic oxide, and free calcium oxide. The standardization used for qualification and for analysis of each constituent shall be determined by valid curve-fitting procedures.
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1.1 These test methods cover the chemical analyses of hydraulic cements. Any test methods of demonstrated acceptable precision and bias may be used for analysis of hydraulic cements, including analyses for referee and certification purposes, as explained in Section 4. Specific chemical test methods are provided for ease of reference for those desiring to use them. They are grouped as Reference Test Methods and Alternative Test Methods. The reference test methods are long accepted classical chemical test methods which provide a reasonably well-integrated basic scheme of analysis for hydraulic cements. The alternative test methods generally provide individual determination of specific analytes and may be used alone or as alternates and determinations within the basic scheme at the option of the analyst and as indicated in the individual method.  
1.2 Contents:    
Section  
Subject    
2  
Referenced Documents  
4  
Description of Referee Analyses  
4.1  
Referee Analyses  
5  
Qualification for Different Analyses  
5.1  
Certified Reference Materials  
5.2  
Requirements for Qualification Testing  
5.3  
Alternative Analyses  
5.4  
Performance Requirements for Rapid Test Methods  
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General  
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Interferences and Limitations  
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Apparatus and Materials  
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Reagents  
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Sample Preparation  
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General Procedures  
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Recommended Order for Reporting Analyses    
Reference Test Methods    
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Insoluble Residue  
8  
Silicon Dioxide  
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Cements with Insoluble Residue Less Than 1 %  
8.3  
Cements with Insoluble Residue Greater Than 1 %  
9  
Ammonium Hydroxide Group  
10  
Ferric Oxide  
11  
Phosphorus Pentoxide  
12  
Titanium Dioxide  
13  
Zinc Oxide  
14  
Aluminum Oxide  
15  
Calcium Oxide  
16  
Magnesium Oxide  
17  
Sulfur  
17.1  
Sulfur Trioxide  
17.2  
Sulfide  
18  
Loss On Ignition  
18.1  
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ABSTRACT
This specification covers the criteria and tests to be used for determining whether a processing addition meets the requirement. When proposed addition is accepted for general use in Portland cement, tests shall be made on cements prepared from at least five different clinkers. These clinkers shall represent two Type I cements, one Type II cement, and two Type III cements. Processing additions shall be evaluated by comparing cements containing the addition to otherwise identical cements from the same source without the addition, or containing a processing addition. The compressive strength and flexural strength of the concrete made with cement containing the addition shall be compared with strengths obtained with the control cement at similar ages. The properties of the materials shall be determined through the following tests in accordance with the following standard: chemical analysis of the cement, compound composition, fineness of cement, normal consistency, time of setting, autoclave expansion, air content of mortar, compressive strength of mortar, and drying shrinkage of mortar.
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SIGNIFICANCE AND USE
4.1 These test methods are used to develop data for comparison with the requirements of Test Methods C1910/C1910M or other specifications for cements that require carbonation curing. These test methods are based on standardized testing in the laboratory and are not intended to simulate job conditions. All tests are performed with mortar and therefore, the results may not provide a direct correlation of how the tested cementitious material will perform in concrete.  
4.2 Compressive Strength—The test for compressive strength is used to determine whether the cement tested will develop a minimum level of strength when carbonated under laboratory conditions.  
4.3 Chemically Bound Carbon Dioxide—Determined using mortar cube specimens prepared for determining compressive strength, the test for chemically bound carbon dioxide is used as an estimate of the mass of carbon dioxide bound during the carbonation curing process and is expressed as a percent of the mass of cement in the test mixture. The actual amount of carbon dioxide bound in a manufactured product is affected by the carbonation process and the cement used, and the physical characteristics of the manufactured product.
SCOPE
1.1 These test methods cover procedures for testing cements that require carbonation curing and are intended for use in concrete.  
1.2 The procedures are organized in the following sections:    
Casting and Carbonation Curing Test Specimens  
Section 8  
Compressive Strength  
Section 9  
Bound Carbon Dioxide  
Section 10  
1.3 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the two systems may result in nonconformance with this standard. Some values only have SI units because the inch-pound equivalents are not used in standard.  
1.4 If required results obtained from another standard are not reported in the same system of units as used by this standard, it is permitted to convert those results using the conversion factors found in the SI Quick Reference Guide, Annex A in Form and Style for ASTM Standards, www.astm.org/COMMIT/Blue_Book.pdf.  
1.5 The text of this standard refers to notes and footnotes that provide explanatory material. These notes and footnotes (excluding those in tables and figures) shall not be considered as requirements of the standard.  
1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. Warning—Common cementitious mixtures are caustic and may cause burns to skin and tissue upon prolonged exposure.2  
1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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ASTM
ASTM C1600/C1600M-23(Specification)
Standard Specification for Rapid Hardening Hydraulic Cement

ABSTRACT
This specification covers performance requirements for rapid hardening hydraulic cements. There are no restrictions on the compositions of the cement or its constituents. The specification classifies cements by type based on specific requirements for very early compressive strength development. The following are the four types of rapid hardening cement: (1) Type URH, ultra rapid hardening for use where high early strength is desired; (2) Type VRH, very rapid hardening for use where very high early strength is desired; (3) Type MRH, medium rapid hardening for use where mid-range hardening high early strength is desired; and (4) Type GRH, general rapid hardening for use when the higher strength properties of a Type VRH or a Type MRH cement is not required. Cement of the type specified shall conform to all of the applicable standard physical requirements for compressive strength and drying shrinkage. Cement shall be tested using the following methods: autoclave expansion; time of setting; compressive strength; drying shrinkage of mortar; heat of hydration; surface resistance; alkali silica resistivity; and expansion in water.
SCOPE
1.1 This specification is for rapid hardening hydraulic cements. This is a specification giving performance requirements. There are no restrictions on the composition of the cement or its constituents.  
1.2 The specification classifies cements by type based on specific requirements for very early compressive strength development.  
1.3 The values stated in either SI units or inch-pound units shall be regarded separately as standard. The values stated in each system are not exact equivalents; therefore, each system shall be used independently of the other. Combining values from the two systems may result in nonconformance with the standard.  
1.4 The text of this standard refers to notes and footnotes that provide explanatory material. These notes and footnotes (excluding those in tables and figures) are not requirements of the standard.  
1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. (Warning—Fresh hydraulic cementitious mixtures are caustic and may cause chemical burns to skin and tissue upon prolonged exposure.2)  
1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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ASTM
ASTM C183/C183M-23(Practice)
Standard Practice for Sampling and the Amount of Testing of Hydraulic Cement

SIGNIFICANCE AND USE
4.1 The sampling procedures described are intended for use in the procurement of samples of hydraulic cement after it has been manufactured and is ready to be offered for sale. They are not intended as sampling procedures for quality control purposes during manufacturing. The testing procedures outlined cover the amount of testing to be done and provide guidance for reporting on conformance or non-conformance of cements with requirements of purchase specifications.  
4.2 This practice is referenced as the procedure for sampling natural cement (Specification C10/C10M), masonry cement (Specification C91/C91M), portland cement (Specification C150/C150M), blended hydraulic cement (Specification C595/C595M), expansive hydraulic cement (Specification C845/C845M), hydraulic cement based on a performance specification (Specification C1157/C1157M), plastic stucco cement (Specification C1328/C1328M), and mortar cement (Specification C1329/C1329M), and  
4.3 Most building codes and construction specifications require that hydraulic cement to be used in the work meet the applicable requirements of the relevant purchase specifications, such as Specifications C10/C10M, C91/C91M, C150/C150M, C595/C595M, C1157/C1157M, C1328/C1328M, C1329/C1329M, or C845/C845M. If the code or specification requires sampling of the manufactured cement, the provisions given in 4.4 are applicable. Not much cement is sold on the basis of such sampling and testing. A useful discussion of sampling and testing cement is contained in ACI 225.1R.  
4.4 The procedures covered in this practice should be done by or for purchasers of hydraulic cement who are using a code or specification that requires sampling and testing to determine if the samples conform to the relevant acceptance specifications. The testing is done using specified methods to determine whether the samples yield test results that conform to the specification, and the tests serve as a basis for acceptance or rejection of the lot of material ...
SCOPE
1.1 This practice covers procedures for sampling and for the amount of testing of hydraulic cement after it has been manufactured and is ready to be offered for sale.  
1.2 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the two systems may result in non-conformance with the standard. Values in SI units [or inch-pound units] shall be obtained by measurement in SI units [or inch-pound units] or by appropriate conversion, using the Rules for Conversion and Rounding given in Standard IEEE/ASTM SI 10, Values are stated in only SI units when inch-pound units are not used in practice  
1.3 The text of this standard references notes and footnotes which provide explanatory material. These notes and footnotes (excluding those in tables and figures) shall not be considered requirements of the standard.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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