ASTM E2102-00
(Test Method)Standard Test Method for Measurement of Mass Loss and Ignitability for Screening Purposes Using a Conical Radiant Heater
Standard Test Method for Measurement of Mass Loss and Ignitability for Screening Purposes Using a Conical Radiant Heater
SCOPE
1.1 This fire-test-response standard provides a means of measuring mass loss and ignitability, for screening purposes, from essentially planar materials, products, or assemblies (including surface finishes), exposed to controlled levels of radiant heating, with or without an external ignitor. This test method is intended for screening purposes only.
1.2 The principal fire-test-response characteristics obtained from this test method are those associated with mass loss from the specimens tested, as a function of time. Time to sustained flaming is also determined. Heat release is, optionally, determined using thermopile measurements detailed in Annex A2.
1.2.1 The fire-test-response characteristics obtained from this test are best used for comparisons between materials with some similarities in composition or structure.
1.3 The relationship between mass loss and heat release depends on the material, product, or assembly tested, and no universal formula exists for calculation of heat release using mass loss measurements (see also additional limitations in 5.7).
1.4 The fire-test-response characteristics obtained from this test method are also obtainable with the apparatus used in Test Method E1354 (the cone calorimeter) or in an applications standards of that equipment (see also 5.4). The referenced test methods permit measurements of added fire-test-response characteristics.
1.5 The fire-test-response characteristics obtained by this test method are specific to the specimen tested, in the form and thickness tested, and are not an inherent property of the material, product, or assembly.
1.6 This fire-test-response method does not provide information on the fire performance of the test specimens under fire conditions other than those conditions specified in this test method. For additional limitations of this test method, see 5.7.
1.7 Use the SI system of units in referee decisions; see IEEE/ASTM SI-10. The units given in parentheses are for information only.
1.8 This standard is used to measure and describe the response of materials, products, or assemblies to heat and flame under controlled conditions, but does not by itself incorporate all factors required for fire hazard or fire risk assessment of the materials, products, or assemblies under actual fire conditions.
1.9 Fire testing of products and materials is inherently hazardous, and adequate safeguards for personnel and property shall be employed in conducting these tests. This test method may involve hazardous materials, operations, and equipment. See also Section 7.
1.10 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.
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An American National Standard
Designation: E 2102 – 00
Standard Test Method for
Measurement of Mass Loss and Ignitability for Screening
Purposes Using a Conical Radiant Heater
This standard is issued under the fixed designation E 2102; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (e) indicates an editorial change since the last revision or reapproval.
INTRODUCTION
The screening fire-test-response method described in this standard uses a radiant energy source
similar to that used in the cone calorimeter, Test Method E 1354. However, the test method apparatus
is much simpler, because it excludes measurements of oxygen consumption or of smoke obscuration,
which are incorporated into the cone calorimeter to measure heat and smoke release. A fire-test-
response standard describes a test method from which one or more fire-test-response characteristics
can be measured, as a result of exposure to a prescribed source of heat or flame, under controlled
conditions. There are many occasions, typically for initial research and development, when there is a
need for screening samples of materials, products, or assemblies, using a simple test. This allows the
user to verify whether certain fire-test-response characteristics of the sample fall within the expected
margins. Screening tests, as related to fire, are described in fire terminology as fire-response tests
performed to determine whether a material, product, or assembly (a) exhibits any unusual fire-related
characteristics, (b) has certain expected fire-related characteristics, or (c) is capable of being
preliminarily categorized according to the fire characteristic in question. Screening tests addressing
fire properties should be chosen so that the energy input (as heat or flame) is representative of that in
the fire test method for which screening is desired.
1. Scope universal formula exists for calculation of heat release using
mass loss measurements (see also additional limitations in 5.7).
1.1 This fire-test-response standard provides a means of
1.4 The fire-test-response characteristics obtained from this
measuring mass loss and ignitability, for screening purposes,
test method are also obtainable with the apparatus used in Test
from essentially planar materials, products, or assemblies
Method E 1354 (the cone calorimeter) or in an applications
(including surface finishes), exposed to controlled levels of
standards of that equipment (see also 5.4). The referenced test
radiant heating, with or without an external ignitor. This test
methods permit measurements of added fire-test-response char-
method is intended for screening purposes only.
acteristics.
1.2 The principal fire-test-response characteristics obtained
1.5 The fire-test-response characteristics obtained by this
from this test method are those associated with mass loss from
test method are specific to the specimen tested, in the form and
the specimens tested, as a function of time. Time to sustained
thickness tested, and are not an inherent property of the
flaming is also determined. Heat release is, optionally, deter-
material, product, or assembly.
mined using thermopile measurements detailed in Annex A2.
1.6 This fire-test-response method does not provide infor-
1.2.1 The fire-test-response characteristics obtained from
mation on the fire performance of the test specimens under fire
this test are best used for comparisons between materials with
conditions other than those conditions specified in this test
some similarities in composition or structure.
method. For additional limitations of this test method, see 5.7.
1.3 The relationship between mass loss and heat release
1.7 Use the SI system of units in referee decisions; see
depends on the material, product, or assembly tested, and no
IEEE/ASTM SI-10. The units given in parentheses are for
information only.
This test method is under the jurisdiction of ASTM Committee E05 on Fire
1.8 This standard is used to measure and describe the
Standards and is the direct responsibility of Subcommittee E05.21 on Smoke and
response of materials, products, or assemblies to heat and flame
Combustion Products.
under controlled conditions, but does not by itself incorporate
Current edition approved Nov. 10, 2000. Published March 2001.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, United States.
E2102–00
all factors required for fire hazard or fire risk assessment of the 2.2 ISO Standards:
materials, products, or assemblies under actual fire conditions.
ISO 3261 Fire Tests–Vocabulary
1.9 Fire testing of products and materials is inherently
ISO 5657 , Fire Tests–Reaction to Fire–Ignitability of
hazardous, and adequate safeguards for personnel and property
Building Products
shall be employed in conducting these tests. This test method
ISO 5660-1 Fire Tests–Reaction to Fire–Rate of Heat Re-
may involve hazardous materials, operations, and equipment.
lease from Building Products (Cone calorimeter method)
See also Section 7.
ISO 9705 Fire Tests–Full Scale Room Test for Surface
1.10 This standard does not purport to address all of the
Products
safety concerns, if any, associated with its use. It is the
ISO 13943 Fire Safety Vocabulary
responsibility of the user of this standard to establish appro-
2.3 British Standards:
priate safety and health practices and determine the applica-
BS 476, Part 15, Fire Tests– Reaction to Fire–Rate of Heat
bility of regulatory limitations prior to use.
Release from Building Products (Cone calorimeter
method)
2. Referenced Documents
BS 6809 Method of Calibration of Radiometers for Use in
2.1 ASTM Standards:
Fire Testing
D 5537 Test Method for Heat Release, Flame Spread and
Mass Loss Testing of Insulating Materials Contained in
3. Terminology
Electrical or Optical Fiber Cables When Burning in a
2 3.1 Definitions: For definitions of terms used in this test
Vertical Cable Tray Configuration
method refer to the terminology contained in Terminology
D 6113 Test Method for Using a Cone Calorimeter to
E 176, ISO 3261 and ISO 13943. In case of conflict, the
Determine Fire-Test-Response Characteristics of Insulat-
definitions given in Terminology E 176 shall prevail.
ing Materials Contained in Electrical or Optical Fiber
2 3.2 Definitions of Terms Specific to This Standard:
Cables
3.2.1 assembly, n—a unit or structure composed of a com-
E 176 Terminology of Fire Standards
bination of materials or products, or both.
E 535 Practice for Preparation of Fire-Test-Response Stan-
3.2.2 composite, n—a combination of materials which are
dards
generally recognized as distinct entities, for example coated or
E 603 Guide for Room Fire Experiments
laminated materials.
E 638 Test Method for Calibration of Heat Transfer Rate
3.2.3 continuous (as related to data acquisition), adj—
Calorimeters Using a Narrow-Angle Blackbody Radiation
conducted at data collection intervals of5sor less.
Facility
3.2.4 essentially flat surface, n—surface where the irregu-
E 906 Test Method for Heat and Visible Smoke Release
larity from a plane does not exceed 6 1 mm.
Rates for Materials and Products
3.2.5 exposed surface, n—that surface of the specimen
E 1354 Test Method for Heat and Visible Smoke Release
subjected to the incident heat.
Rates for Materials and Products Using an Oxygen Con-
3.2.6 flashing, n—existence of flame on or over the surface
sumption Calorimeter
of the specimen for periods of less than 1 s.
E 1474 Test Method for Determining the Heat Release Rate
3.2.7 irradiance (at a point of a surface), n—ratio of the
of Upholstered Furniture and Mattress Components or
radiant flux incident on a small but measurable element of
Composites Using a Bench Scale Oxygen Consumption
surface containing the point, by the area of that element.
Calorimeter
3.2.7.1 Discussion—Convective heating is negligible in the
E 1537 Test Method for Fire Testing of Real Scale Uphol-
horizontal specimen orientation. In the vertical orientation, it is
stered Furniture
small, but not negligible. Despite this contribution from
E 1590 Test Method for Fire Testing of Real Scale Mat-
convective heating, the term “irradiance” is used instead of
tresses
“heat flux” throughout this test method as it best indicates the
E 1623 Test Method for Determining Fire and Thermal
essentially radiative mode of heat transfer.
Parameters of Materials, Products and Systems Using and
3.2.8 material, n—single substance, or uniformly dispersed
Intermediate Scale Calorimeter (ICAL)
mixture, for example metal, stone, timber, concrete, mineral
E 1740 Test Method for Determining the Heat Release Rate
fiber, or polymer.
and Other Fire-Test-Response Characteristics of Wallcov-
3.2.9 orientation, n—the plane in which the exposed face of
ering Composites Using a Cone Calorimeter
the specimen is located during testing.
E 1822 Test Method for Fire Testing of Real Scale Stacked
3.2.9.1 Discussion—For this standard, the specimen orien-
Chairs
tation may only be either vertical or horizontal.
IEEE/ASTM SI-10, International System of Units (SI) The
Modernized Metric System
Available from International Standardization Organization, P.O. Box 56,
CH-1211; Geneva 20, Switzerland or American National Standards Institute, 11
Annual Book of ASTM Standards, Vol 10.02. West 42nd Street, New York, NY, 10046
3 6
Annual Book of ASTM Standards, Vol 04.07. Available from British Standards Institution, PO Box 4033, Linford Wood,
Annual Book of ASTM Standards, Vol 15.03. Milton Keynes, MK 14 6LE, United Kingdom
E2102–00
3.2.10 sample, n—an amount of the material, product, or propensity for the material, product, or assembly to become
assembly, to be tested, which is representative of the item as a involved and contribute to fire spread or growth; however this
whole. method does not assess the smoke or combustion products
3.2.11 specimen, n—representative piece of the product released.
which is to be tested together with any substrate or treatment. 5.1.4 The apparatus used for this test method is suitable to
3.2.11.1 Discussion—This may include an air gap. assess the critical heat flux for ignition of the materials,
3.2.12 sustained flaming, n—the existence of flame on or products, or assemblies tested, by assessing ignitability at
over the surface of the specimen for a period of4sor more. various heat fluxes (see Appendix X3 for guidance).
3.2.13 time to ignition, n—time between the start of the test 5.2 Values determined by this test are specific to the
and the presence of a flame on or over most of the specimen specimen in the form and thickness tested and are not inherent
surface for a period of at least 4 s. fundamental properties of the material, product, or assembly
3.2.14 time to sustained flaming, n—time to ignition. tested. Thus, closely repeatable or reproducible experimental
3.2.15 transitory flaming, n—the existence of flame on or results are not to be expected from this test method when tests
over the surface of the specimen for periods of between 1 and are conducted for a given material, product, or assembly, while
4s. introducing variations in properties such as specimen thickness
or density.
4. Summary of Test Method
5.3 No incident irradiance is specified in this test method.
4.1 This test method employs a conically-shaped The instrument is capable of generating irradiances ranging up
electrically-heated radiant-energy source, positioned so as to
to 100 kW/m . The choice of irradiance is a function of the
produce an irradiance level of up to 100 kW/m , averaged over application of the material, product, or assembly to be tested,
the center of the exposed surface of an essentially planar
and of the fire scenario the user is investigating. However, the
specimen. An external spark ignitor is available, if required. method is not suitable for incident irradiances below 10
This test method is used to determine continuously the mass
kW/m (see 5.7.3).
lost during the combustion process, using a load cell, for
5.4 The method used for optionally measuring heat release,
screening purposes. Ignitability is also assessed by the test
a thermopile, is not as accurate as the conventional oxygen
method.
consumption calorimetry method, used in the cone calorimeter,
4.1.1 Optionally, the test method is capable of obtaining an
Test Method E 1354, in its applications standards, such as Test
estimate of the heat released by the specimen during the
Method E 1474 and E 1740, or in intermediate scale or a large
burning process, using a thermopile housed above the burning
scale calorimetry test methods, such as Test Methods E 1623,
specimen (See Annex A2). Determinations of heat release
E 1537, E 1590 or D 5537 (see also Annex A2). On the other
using a similar radiant-energy source and oxygen consumption
hand the thermopile method of assessing heat release has been
calorimetry, are made with the cone calorimeter, Test Method
used extensively because of its simplicity, including Test
E 1354.
Method E 906, and other applications discussed in Guide
4.2 The specimen is essentially planar, 100 mm by 100 mm
E 603.
(3.9 by 3.9 in.) in size, at a thickness not exceeding 25 mm (1 5.5 Testing of composites and dimensionally unstable ma-
in.) and is mounted within a holder.
terials requires special procedures (see 8.4 and 8.5).
5.6 Testing in the vertical orientation is feasible with the test
5. Significance and Use
method, but not recommended, as it has been shown to have
5.1 This test method provides a means for screening mate-
the potential to lead to serious measurement errors on time to
rials, products, or assemblies, for the mass loss, and ignitability
ignition.
they exhibit under specified heat flux exposure conditions. As
5.7 Limitations
an option, the test method is also suitable for screening for the
5.7.1 No universal formula exists for calculation of heat
heat released, by using a thermopile method (See Annex A2).
release as a function of mass loss. If heat release data are
5.1.1 Terminology E 176, on fire standards, states that
desired, calibration curves must be developed by the user, and
fire-test-response characteristics include ease of ignition and
they are specific to the material, product, or assembly tested.
mass loss (both measured in this test method), as well as flame
5.7.2 If during the test of one or more of the three replicate
spread, smoke generation, fire endurance, and toxic potency of
test specimens, any of the following unusual behavior occurs:
smoke.
(1) molten material overflows the specimen holder trough, (2)
5.1.2 The mass loss rate of a material, pr
...
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