ASTM D4446-02
(Test Method)Standard Test Method for Anti-Swelling Effectiveness of Water-Repellent Formulations and Differential Swelling of Untreated Wood When Exposed to Liquid Water Environments
Standard Test Method for Anti-Swelling Effectiveness of Water-Repellent Formulations and Differential Swelling of Untreated Wood When Exposed to Liquid Water Environments
SCOPE
1.1 This test method is designed to evaluate the effectiveness of water-repellent compositions for retarding dimensional changes in coated wood submerged in water. It can also be used to measure the differential swelling of untreated wood when exposed to liquid water environments. The compositions tested are designed to be mixed until uniform and applied by brush, roller, dip or spray to an exterior wood surface.
1.2 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.
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Designation:D4446–02
Standard Test Method for
Anti-Swelling Effectiveness of Water-Repellent Formulations
and Differential Swelling of Untreated Wood When Exposed
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to Liquid Water Environments
This standard is issued under the fixed designation D 4446; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (e) indicates an editorial change since the last revision or reapproval.
1. Scope 3.2 The swelling differences of untreated wood species
when subjected to water immersion can also be determined by
1.1 This test method is designed to evaluate the effective-
this test method.
ness of water-repellent compositions for retarding dimensional
3.3 This method is a basic screening test and thus provides
changesincoatedwoodsubmergedinwater.Itcanalsobeused
an initial determination of the anti-swelling efficiency of water
to measure the differential swelling of untreated wood when
repellents. It is a qualitative method designed to provide a
exposed to liquid water environments.The compositions tested
reproducible means of establishing: (1) the anti-swelling effi-
are designed to be mixed until uniform and applied by brush,
ciency of water-repellent formulations, and (2) the relative
roller, dip or spray to an exterior wood surface.
swelling of untreated wood species when both are exposed to
1.2 This standard does not purport to address all of the
liquid water environments.
safety concerns, if any, associated with its use. It is the
responsibility of the user of this standard to establish appro-
4. Apparatus
priate safety and health practices and determine the applica-
4.1 Conditioning Room or Chamber, having a controlled
bility of regulatory limitations prior to use.
temperature of 80 6 5°F (276 3°C), and a controlled relative
2. Summary of Method humidity of 65 6 5 %.This room is used to establish a uniform
moisture content in the test specimens. In all studies the
2.1 Wood samples in the form of elongated slats that
temperature and relative humidity selected by the investigator
represent the timber species or product/treatment combination
must be stated and must remain constant throughout a given
to be evaluated are exposed in soak containers. The elongated
conditioning and test period.
slats are immersed in the water-repellent formulation, condi-
4.2 Balance, sensitive to at least 0.01 g.
tioned with appropriate weighing, then subjected to immersion
4.3 Treating Tank (Fig. 1).
in distilled water for a prescribed period. The untreated slats
4.4 Swellometer, as illustrated in Fig. 2, Fig. 3, and Fig. 4.
omit the immersion in the water-repellent formulation. The
swelling resulting from immersion for the selected time period
5. Test Specimens
is determined by reading a dial gage calibrated in increments of
5.1 Wood used for these tests must be straight-grained,
0.001 in. (0.025 mm).
flat-sawn, clear, kiln-dried Ponderosa pine sapwood or other
2.2 A water repellent efficiency of 60 % is required to pass
suitable species. Cut the parent boards in a manner to give
this test.
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specimens ⁄4 in. (6 mm) in the longitudinal dimension, 1 ⁄2 in.
3. Significance and Use (38 mm) in the radial dimension, and 10 in. (254 mm) in the
tangential dimension. Cut with a sharp, fine-toothed saw to
3.1 This test method is useful in determining the relative
obtain as smooth a surface as possible without sanding.
anti-swelling efficiency of various water-repellent formulations
Number each specimen for identification and reference.
when applied to wood. It is the initial means of estimating the
5.1.1 Selection of Ponderosa pine sapwood can be assured
ability of water-repellent treated wood to perform satisfactorily
by the following quick chemical test: (1) prepare a solution of
when exposed to liquid water environments.
5 g of benzidine in 25 g of hydrochloric acid and 970 g of
water, and (2) prepare a second solution consisting of a 10 %
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This test method is under the jurisdiction of ASTM Committee D01 on Paint concentration of sodium nitrite in water. When the test is to be
and Related Coatings, Materials, andApplications and is the direct responsibility of
made, pour equal amounts of the two solutions together and
Subcommittee D01.42 on Architectural Coatings.
then apply to the wood surface by means of brushing or
Current edition approved Sept. 10, 2002. Published November 2002. Originally
e1
published as D 4446 – 95. Last previous edition D 4446 – 95 .
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, United States.
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D4446–02
FIG. 1 Treating Tank—Five Samples Tested Simultaneously
FIG. 2 Single Tes
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