ASTM A646/A646M-17(2022)
(Specification)Standard Specification for Premium Quality Alloy Steel Blooms and Billets for Aircraft and Aerospace Forgings
Standard Specification for Premium Quality Alloy Steel Blooms and Billets for Aircraft and Aerospace Forgings
ABSTRACT
This specification deals with the standard requirements for premium quality alloy steel semifinished rolled or forged blooms and billets for reforging into aircraft and aerospace critical parts such as landing-gear forgings. Covered here are three basic classifications of steel, namely: Class I, steel manufactured by vacuum-induction melting or consumable-electrode vacuum melting process; Class II, air-melted steel manufactured by electric-furnace vacuum degassing process; Class III, air-melted steel manufactured by electric-furnace ladle refining and vacuum degassing processes. Steel materials shall be heat-treated and hot-worked by either hot rolling or forging. Alloy steels shall be examined by heat and product analyses and hardenability tests, and shall conform to chemical composition and maximum annealed Brinell hardness requirements. Quality evaluation tests, such as macrotech, microcleanliness, and nondestructive ultrasonic (both immersion and contact examination) inspection, shall be performed as well.
SCOPE
1.1 This specification covers premium quality alloy steel semifinished rolled or forged blooms and billets for reforging into critical parts such as aircraft landing-gear forgings.
1.2 Blooms and billets, hereinafter referred to as blooms, are semifinished steel products, hot rolled or forged to approximate cross-sectional dimensions. Blooms may be square, round, hexagonal, octagonal, or rectangular in section. For the purposes of this specification, minimum bloom section size will be 16 in.2 [103 cm2].
1.3 This specification covers two basic classifications of steel:
1.3.1 Class I—Vacuum-induction melted or consumable-electrode vacuum melted, or other suitable processes which will satisfy the quality requirements of this specification.
1.3.2 Class II—Air-melted vacuum degassed.
1.3.3 Class III—Air melted electric furnace ladle refined and vacuum degassed.
1.4 The values stated in either inch-pound units or SI (metric) units are to be regarded separately as standard. Within the text and tables, the SI units are shown in brackets. The values stated in each system are not necessarily exact equivalents; therefore, to ensure conformance with the standard, each system shall be used independently of the other, and values from the two systems shall not be combined.
1.5 Unless the order specifies the applicable “M” specification the material shall be furnished to the inch-pound units.
1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
General Information
Relations
Standards Content (Sample)
This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the
Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
Designation:A646/A646M −17 (Reapproved 2022)
Standard Specification for
Premium Quality Alloy Steel Blooms and Billets for Aircraft
and Aerospace Forgings
This standard is issued under the fixed designationA646/A646M; the number immediately following the designation indicates the year
of original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval.
A superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope* 2. Referenced Documents
2.1 ASTM Standards:
1.1 This specification covers premium quality alloy steel
A255 Test Methods for Determining Hardenability of Steel
semifinished rolled or forged blooms and billets for reforging
A388/A388M Practice for Ultrasonic Examination of Steel
into critical parts such as aircraft landing-gear forgings.
Forgings
1.2 Blooms and billets, hereinafter referred to as blooms,
A788/A788M Specification for Steel Forgings, General Re-
are semifinished steel products, hot rolled or forged to approxi-
quirements
mate cross-sectional dimensions. Blooms may be square,
A604/A604M Practice for Macroetch Testing of Consum-
round, hexagonal, octagonal, or rectangular in section. For the
able Electrode Remelted Steel Bars and Billets
purposes of this specification, minimum bloom section size
E45 Test Methods for Determining the Inclusion Content of
2 2
will be 16 in. [103 cm ].
Steel
1.3 This specification covers two basic classifications of
E114 Practice for Ultrasonic Pulse-Echo Straight-Beam
steel:
Contact Testing
1.3.1 Class I—Vacuum-induction melted or consumable- E214 Practice for Immersed Ultrasonic Testing by the Re-
electrode vacuum melted, or other suitable processes which
flection Method Using Pulsed Longitudinal Waves (With-
will satisfy the quality requirements of this specification. drawn 2007)
1.3.2 Class II—Air-melted vacuum degassed. E381 Method of Macroetch Testing Steel Bars, Billets,
Blooms, and Forgings
1.3.3 Class III—Air melted electric furnace ladle refined
E428 Practice for Fabrication and Control of Metal, Other
and vacuum degassed.
than Aluminum, Reference Blocks Used in Ultrasonic
1.4 The values stated in either inch-pound units or SI
Testing (Withdrawn 2019)
(metric) units are to be regarded separately as standard. Within
2.2 AMS Standards:
the text and tables, the SI units are shown in brackets. The
AMS 2300 Steel Cleanliness, Premium-Quality
values stated in each system are not necessarily exact equiva-
AMS 2301 Steel Cleanliness, Aircraft-Quality
lents; therefore, to ensure conformance with the standard, each
AMS 2304 Steel Cleanliness, Special Aircraft-Quality
system shall be used independently of the other, and values
from the two systems shall not be combined.
3. Terminology
1.5 Unless the order specifies the applicable “M” specifica-
3.1 In addition to the terminology requirements of Specifi-
tion the material shall be furnished to the inch-pound units.
cation A788/A788M, the following terms that are specific to
this specification apply:
1.6 This international standard was developed in accor-
dance with internationally recognized principles on standard-
3.2 Definitions:
ization established in the Decision on Principles for the
3.2.1 air-melted vacuum-degassed steel—arc- or induction-
Development of International Standards, Guides and Recom-
furnace-melted steel that is vacuum treated immediately prior
mendations issued by the World Trade Organization Technical
to or during the operation of pouring the ingot.
Barriers to Trade (TBT) Committee.
For referenced ASTM standards, visit the ASTM website, www.astm.org, or
contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
This specification is under the jurisdiction of ASTM Committee A01 on Steel, Standards volume information, refer to the standard’s Document Summary page on
Stainless Steel and Related Alloys and is the direct responsibility of Subcommittee the ASTM website.
A01.06 on Steel Forgings and Billets. The last approved version of this historical standard is referenced on
Current edition approved March 1, 2022. Published March 2022. Originally www.astm.org.
approved in 1971. Last previous edition approved in 2017 as A646/A646M – 17. Available from SAE International (SAE), 400 Commonwealth Dr.,Warrendale,
DOI: 10.1520/A0646_A0646M-17R22. PA 15096, http://www.sae.org.
*A Summary of Changes section appears at the end of this standard
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
A646/A646M−17 (2022)
3.2.2 consumable-electrode vacuum-remelted steel—metal 5.1.1 The steel making provisions of Specification A788/
that has been remelted into a crucible in vacuum from single or A788M shall apply, except for the following modifications;
multiple electrodes.
5.1.1.1 Class I material shall be manufactured by the
vacuum-induction-melting process or by the consumable-
3.2.3 electroslag-melted steel—metal that has been remelted
electrode vacuum-melting (VAR) process. By agreement other
into a crucible from single or multiple electrodes utilizing an
processes such as electroslag or electron-beam melting may be
electrical discharge through molten slag as a source of heat.
considered acceptable.
3.2.3.1 Discussion—For the purposes of this specification
5.1.1.2 Class II material shall be manufactured by an
the parent heat from which any electrode for remelting by the
electric-furnace vacuum-degassed process.
electroslag process has been produced shall have been either
5.1.1.3 Class III material shall be manufactured by the
melted under vacuum or vacuum degassed immediately prior
electric furnace process with ladle refining and vacuum degas-
to or during pouring of the heat.
sing.
3.2.4 vacuum induction melted steel—metal that has been
melted, refined, and poured from an induction furnace operat-
5.2 Hot-Working Procedure:
ing under vacuum.
5.2.1 Blooms may be either hot rolled or forged.
5.2.2 Blooms having cross-sectional areas ranging from
4. Ordering Information and General Requirements
2 2 2 2
16 in. to 225 in. [100 cm to 1450 cm ] when made from
4.1 Material supplied to this specification shall conform to
air-melt ingots shall have at least 2 to 1 reduction of area from
2 2
the requirements of Specification A788/A788M, which out-
ingot to bloom. On blooms exceeding 225 in. [1450 cm ]
lines additional ordering information, manufacturing
forging reduction requirements shall be by agreement. Ingot-
requirements, testing and retesting methods and procedures,
to-final forging reduction is not included in this requirement.
marking, certification, product analysis variations, and addi-
5.3 Heat Treatment:
tional supplementary requirements.
5.3.1 Unless otherwise specified all material purchased to
4.1.1 If the requirements of this specification are in conflict
this specification will be furnished in the as forged or rolled
with the requirements of Specification A788/A788M, the
(untreated)condition.Inthisconditionsomegradesmaynotbe
requirements of this specification shall prevail.
soft enough for cold sawing, and may be prone to cracking.
4.2 In addition to the ordering requirements of Specification
5.3.2 When specified, the material may be ordered annealed
A788/A788M, the following information should be supplied
or normalized and tempered to a maximum Brinell Hardness,
by the purchaser:
as specified in Table 2 or by agreement.
4.2.1 Class designation (see 1.3),
5.3.3 Material shall be furnished in condition to withstand,
4.2.2 Quality level (Table 1), grade designation (Table 2), or
for an indefinite time, exposure to all climatic conditions
detailed chemistry for nonstandard grades,
withoutdevelopinganyexternalorinternalcracks.Themethod
4.2.3 Desired billet or bloom size,
of cooling after hot working or of heat treatment before
4.2.4 Weight or quantity and length,
shipment shall be optional with the manufacturer, who shall be
4.2.5 Minimum forging reduction required if ordered size
responsible (in the same manner as for discontinuities dis-
2 2
exceeds 225 in. [1450 cm ] (see 5.2.2),
closed after delivery) for cracks which may develop before
4.2.6 Annealing, if required (see 5.3.2),
material is subjected to reheating. When a specific heat
4.2.7 Macroetch standards of acceptance (see 7.1),
treatment or conditioning of material is specified by the
4.2.8 Microcleanliness standards of acceptance (see 7.2),
purchaser, the manufacturer shall be responsible only for
4.2.9 Specific ultrasonic examination requirements, such as
carrying out those specific operations and not for any cracking
transducer type and size, whether contact or immersion
that may subsequently develop.
preferred, level of reportable discontinuities and any special
surface finish requirements.
6. Chemical Requirements
4.2.10 Hardenability standards of acceptance (see 8.1), and
6.1 General Requirements:
4.2.11 Any supplementary requirements desired.
6.1.1 Table 2 lists standard grades of alloy steel that are
5. Manufacture
currently produced in premium quality; however, it is not the
intent of this specification to restrict application only to the
5.1 Melting Practice:
materials listed in Table 2.
6.1.2 When a standard grade is ordered, the analysis shall
TABLE 1 Maximum Permissible Discontinuities in Ultrasonic
Examination
conform to the requirements as to chemical composition
prescribed in Table 2 for the ordered grade.
Response,
in. [mm]
Quality Stringers,
6.1.3 The steel, when ordered to other than a standard
Level Length in. [mm]
Single Multiple
analysis, shall conform to the requirements of the order.
Discontinuities Discontinuities
3 2 2 1
6.2 Heat Analysis:
AA ⁄64 [1.0] ⁄64 [0.8] ⁄64 – ⁄2 [1.0–12.0]
5 3 3
A ⁄64 [2.0] ⁄64 [1.0] ⁄64 –1 [1.0–25]
6.2.1 The heat analysis obtained from sampling in accor-
8 5 5
B ⁄64 [3.0] ⁄64 [2.0] ⁄64 –1 [2.0–25]
dance with Specification A788/A788M shall comply with
12 8 8
C ⁄64 [5.0] ⁄64 [3.0] ⁄64 –1 [3.0–25]
Table 2 for standard grades, or to the requirements of the order.
A646/A646M−17 (2022)
A
TABLE 2 Chemical and Hardness Requirements
Composition, %
Grade Maximum
Proprietary
No. Manga- Phos- Chro- Molyb- Vana- Annealed
Name or Carbon Sulfur Silicon Nickel Others
nese phorus mium denum dium Brinell
Grade
Hardness
3310 1 0.08–0.13 0.45–0.60 0.015max 0.012 max 0.20–0.35 3.25–3.75 1.40–1.75 . . . . . . . . . 262
9310 2 0.08–0.13 0.45–0.65 0.015 max 0.012 max 0.20–0.35 3.00–3.50 1.00–1.40 0.08–0.15 . . . . . . 262
4620 3 0.17–0.22 0.45–0.65 0.015 max 0.012 max 0.20–0.35 1.65–2.00 . . . 0.20–0.30 . . . . . . 229
8620 4 0.18–0.23 0.70–0.90 0.015max 0.012 max 0.20–0.35 0.40–0.70 0.40–0.60 0.15–0.25 . . . . . . 229
4330 Mod. 5 0.28–0.33 0.75–1.00 0.015 max 0.012 max 0.20–0.35 1.65–2.00 0.70–0.95 0.35–0.50 0.05–0.10 . . . 285
4335 Mod. 6 0.33–0.38 0.60–0.90 0.015 max 0.012 max 0.40–0.60 1.65–2.00 0.65–0.90 0.30–0.40 0.17–0.23 . . . 285
4340 7 0.38–0.43 0.65–0.85 0.015 max 0.012 max 0.20–0.35 1.65–2.00 0.70–0.90 0.20–0.30 . . . . . . 285
300 M 8 0.38–0.43 0.65–0.90 0.012 max 0.012 max 1.45–1.80 1.65–2.00 0.70–0.95 0.35–0.45 0.05–0.10 . . . 285
D6AC 9 0.45–0.50 0.60–0.90 0.010 max 0.010 max 0.15–0.30 0.40–0.70 0.90–1.20 0.90–1.10 0.08–0.15 . . . 285
H-11 10 0.38–0.43 0.20–0.40 0.015 max 0.015 max 0.80–1.00 . . . 4.75–5.25 1.20–1.40 0.40–0.60 . . . 235
4130 11 0.28–0.33 0.40–0.60 0.015 max 0.012 max 0.20–0.35 . . . 0.80–1.10 0.15–0.25 . . . . . . 229
4140 12 0.38–0.43 0.75–1.00 0.015 max 0.012 max 0.20–0.35 . . . 0.80–1.10 0.15–0.25 . . . . . . 235
98BV40 13 0.40–0.46 0.75–1.00 0.015 max 0.012 max 0.50–0.80 0.60–0.90 0.80–1.05 0.45–0.60 0.01–0.06 0.0005 min, 285
Boron
6150 14 0.48–0.53 0.70–0.90 0.015 max 0.012 max 0.20–0.35 . . . 0.80–1.10 . . . 0.15 min . . . 235
52100 15 0.98–1.10 0.25–0.45 0.015 max 0.010 max 0.20–0.35 . . . 1.30–1.60 . . . . . . . . . 302
HP 9-4-20 16 0.17–0.23 0.20–0.40 0.010 max 0.010 max 0.10 max 8.5–9.5 0.65–0.85 0.90–1.10 0.06–0.12 Co 4.25–4.75 341
HP 9-4-30 17 0.29–0.34 0.10–0.35 0.010 max 0.010 max 0.10 max 7.0–8.0 0.90–1.10 0.90–1.10 0.06–0.12 Co 4.25–4.75 341
Marage 18 0.03 max 0.10 max 0.010 max 0.010 max 0.10 max 17.0–19.0 . . . 3.0–3.50 . . . Co 8.0–9.0 321
200 Ti 0.10–0.25
Al 0.05–0.15
B, Zr, Ca added
Marage 19 0.03 max 0.10 max 0.010 max 0.010 max 0.10 max 17.0–19.0 . . . 4.6–5.2 . . . Co 7.0–8.5 321
250 Ti 0.30–0.50
Al 0.05–0.15
B, Zr, Ca added
Marage 20 0.03 max 0.10 max 0.010 max 0.010 max 0.10 max 18.0–19.0 . . . 4.7–5.2 . . . Co 8.5–9.5 321
300 Ti 0.50–0.80
Al 0.05–0.15
B, Zr, Ca added
Nit. 135 21 0.38–0.43 0.50–0.70 0.015 max 0.012 max 0.20–0.40 . . . 1.40–1.80 0.30–0.40 . . . Al 0.95–1.30 285
A
If any of the following elements are not specified, the following maximum limits shall apply: Nickel 0.35 %; Chromium 0.20 %; Molybdenum 0.06 %; Copper 0.35 %.
6.3 Product Analysis: Test Methods E45, using Method D (Modified JK Chart) for
6.3.1 The purchaser may use the product analysis provision Class I steel and Method A (JK Chart) for Classes II and III
of Specification A788/A788M to obtain a product analysis steel. Standards of acceptance shall be specified by the pur-
from a billet or bloom representing each heat or multiple heat. chaser in the order.
7.3 Nondestructive Testing, Ultrasonic Inspection:
7. Quality Evaluation Tests
7.3.1 General:
7.1 Macroetch—Macroetch inspection shall be required for
7.3.1.1 All material ordered to this specification shall be
all material furnished to this specification. Samples represent-
subjected to ultrasonic examination. Inspection may be per-
ing the top and bottom of each ingot shall be examined.
formed by either the immersion or the contact method provid-
Macroetching shall be performed in accordance with Method
ing that the manufacturer can ensure adequate resolution of the
E381 and Practice A604/A604M, as applicable. Standards of
applicable reference standards with the chosen method.
acceptance shall be specified by the purchaser in the order.
7.3.1.2 The usage of reference blocks containing flat-
7.2 Microcleanliness—All material furnished to this speci- bottomed holes for calibration is the preferred method for
evaluation of discontinuity size up to billet cross-sectional
fication shall be inspected for microcleanliness. At least one
sample shall be removed from a location midway between the dimensions of approximately 12 in. [300 mm]. With larger
center and outside surface representing the top and bottom of sizes, it is recognized that reference block fabrication becomes
the first and last ingots of each heat or from an ingot from each difficult and
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