ASTM D402/D402M-14
(Test Method)Standard Test Method for Distillation of Cutback Asphalt (Withdrawn 2023)
Standard Test Method for Distillation of Cutback Asphalt (Withdrawn 2023)
SIGNIFICANCE AND USE
4.1 This procedure measures the amount of the more volatile constituents in cutback asphalt. The properties of the residue after distillation are not necessarily characteristic of the bitumen used in the original mixture, nor of the residue which may be left at any particular time after field application of the cutback asphalt. The presence of silicone in the cutback asphalt may affect the distillation residue by retarding the loss of volatile material after the residue has been poured into the residue container.
SCOPE
1.1 This test method covers a distillation test for cutback asphaltic (bituminous) products.
1.2 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the two systems may result in non-conformance with the standard.
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.
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Designation: D402/D402M − 14 American Association State
Highway and Transportation Officials Standard
AASHTO No.: T78
27/74 (88)
Standard Test Method for
1
Distillation of Cutback Asphalt
This standard is issued under the fixed designation D402/D402M; the number immediately following the designation indicates the year
of original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval.
A superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope 3. Summary of Method
1.1 This test method covers a distillation test for cutback 3.1 Two hundred millilitres of the sample are distilled in a
asphalts. 500-mLflask,atacontrolledrate,toatemperatureintheliquid
of 360°C [680°F], and the volumes of distillate obtained at
1.2 The values stated in either SI units or inch-pound units
specified temperatures are measured. The residue from the
are to be regarded separately as standard. The values stated in
distillation, and also the distillate, may be tested as required.
each system may not be exact equivalents; therefore, each
system shall be used independently of the other. Combining
4. Significance and Use
values from the two systems may result in non-conformance
4.1 This procedure measures the amount of the more vola-
with the standard.
tile constituents in cutback asphalt. The properties of the
1.3 This standard does not purport to address all of the
residue after distillation are not necessarily characteristic of the
safety concerns, if any, associated with its use. It is the
bitumen used in the original mixture, nor of the residue which
responsibility of the user of this standard to establish appro-
may be left at any particular time after field application of the
priate safety and health practices and determine the applica-
cutbackasphalt.Thepresenceofsiliconeinthecutbackasphalt
bility of regulatory limitations prior to use.
may affect the distillation residue by retarding the loss of
volatile material after the residue has been poured into the
2. Referenced Documents
residue container.
2
2.1 ASTM Standards:
D86 Test Method for Distillation of Petroleum Products at
5. Apparatus
Atmospheric Pressure
5.1 Distillation Flask, 500-mL side-arm, having the dimen-
D370 Practice for Dehydration of Oil-Type Preservatives
sions shown in Fig. 1.
E1 Specification for ASTM Liquid-in-Glass Thermometers
E77 Test Method for Inspection and Verification of Ther- 5.2 Condenser, standard glass-jacketed, of nominal jacket
mometers
length from 200 to 300 mm and overall tube length of 450 6
E133 Specification for Distillation Equipment 10 mm (see Fig. 3).
E220 Test Method for Calibration of Thermocouples By
5.3 Adapter, heavy-wall (1-mm) glass, with reinforced top,
Comparison Techniques
having an angle of approximately 105°. The inside diameter at
E644 Test Methods for Testing Industrial Resistance Ther-
the large end shall be approximately 18 mm, and at the small
mometers
end, not less than 5 mm. The lower surface of the adapter shall
E1137 SpecificationforIndustrialPlatinumResistanceTher-
be on a smooth descending curve from the larger end to the
mometers
smaller. The inside line of the outlet end shall be vertical, and
the outlet shall be cut or ground (not fire-polished) at an angle
of 45 6 5° to the inside line.
1
This test method is under the jurisdiction of ASTM Committee D04 on Road
5.4 Shield, steel, lined with 3-mm fire proof insulation and
and Paving Materials and is the direct responsibility of Subcommittee D04.46 on
Durability and Distillation Tests.
fitted with transparent mica windows, of the form and dimen-
Current edition approved June 1, 2014. Published August 2014. Originally
sionsshowninFig.2,usedtoprotecttheflaskfromaircurrents
approved in 1934. Last previous edition approved in 2008 as D402 – 08. DOI:
and to reduce radiation. The cover (top) shall be made in two
10.1520/D0402_D0402M-14.
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or parts of 6.4-mm fire proof insulation.
contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
2
5.5 Shield and Flask Support—Two 15-cm sheets of 16-
Standards volume information, refer to the standard’s Document Summary page on
the ASTM website. mesh Chromel wire gauze on a tripod or ring.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
1
---------------------- Page: 1 ----------------------
D402/D402M − 14
FIG. 1 Distillation Flask
FIG. 2 Shield
NOTE1—Receiversofsmallercapacityhaving0.1-mLdivisionsmaybe
5.6 Heat Source:
used when low volumes of total distillate are expected and the added
5.6.1 Adjustable Tirrill-type gas burner or equivalent.
accuracy required.
5.6.2 An electric heater equipped with a transformer ca
...
This document is not an ASTM standard and is intended only to provide the user of an ASTM standard an indication of what changes have been made to the previous version. Because
it may not be technically possible to adequately depict all changes accurately, ASTM recommends that users consult prior editions as appropriate. In all cases only the current version
of the standard as published by ASTM is to be considered the official document.
Designation: D402 − 08 D402/D402M − 14 American Association State
Highway and Transportation Officials Standard
AASHTO No.: T78
27/74 (88)
Standard Test Method for
Distillation of Cutback Asphaltic (Bituminous)
1
ProductsAsphalt
This standard is issued under the fixed designation D402;D402/D402M; the number immediately following the designation indicates the
year of original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last
reapproval. A superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope
1.1 This test method covers a distillation test for cutback asphaltic (bituminous) products.asphalts.
1.2 The values givenstated in either SI units or inch-pound units are to be regarded separately as the standard. The inch-pound
units given in parentheses are for information only.values stated in each system may not be exact equivalents; therefore, each
system shall be used independently of the other. Combining values from the two systems may result in non-conformance with the
standard.
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility
of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory
limitations prior to use.
2. Referenced Documents
2
2.1 ASTM Standards:
D86 Test Method for Distillation of Petroleum Products at Atmospheric Pressure
D370 Practice for Dehydration of Oil-Type Preservatives
E1 Specification for ASTM Liquid-in-Glass Thermometers
E77 Test Method for Inspection and Verification of Thermometers
E133 Specification for Distillation Equipment
E220 Test Method for Calibration of Thermocouples By Comparison Techniques
E644 Test Methods for Testing Industrial Resistance Thermometers
E1137 Specification for Industrial Platinum Resistance Thermometers
2.2 IP Standards:
IP 123/ASTM D 86, Distillation of Petroleum Products
Thermometers as specified in IP Standards
Crow Receiver as specified in British Standards 658:1989
C.O.3—Standard Methods for Testing Tar and its Products (Published by the U.K. Standardization of Tar Products Tests
Committee)
3. Summary of Method
3.1 Two hundred millilitres of the sample are distilled in a 500-mL flask, at a controlled rate, to a temperature in the liquid of
360°C (680°F),[680°F], and the volumes of distillate obtained at specified temperatures are measured. The residue from the
distillation, and also the distillate, may be tested as required.
1
This test method is under the jurisdiction of ASTM Committee D04 on Road and Paving Materials and is the direct responsibility of Subcommittee D04.46 on Durability
and Distillation Tests.
Current edition approved July 15, 2008June 1, 2014. Published August 2008August 2014. Originally approved in 1934. Last previous edition approved in 20022008 as
D402 – 02.D402 – 08. DOI: 10.1520/D0402-08.10.1520/D0402_D0402M-14.
In the IP, this method is under the jurisdiction of the Standardization Committee. This method was adopted as a joint ASTM-IP standard in 1961.
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM Standards
volume information, refer to the standard’s Document Summary page on the ASTM website.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
1
---------------------- Page: 1 ----------------------
D402/D402M − 14
4. Significance and Use
4.1 This procedure measures the amount of the more volatile constituents in cutback asphaltic products. asphalt. The properties
of the residue after distillation are not necessarily characteristic of the bitumen used in the original mixture, nor of the residue
which may be left at any particular time after field application of the cutback asphaltic product. asphalt. The presence of silicone
in the cutback asphalt may affect the distillation residue by retarding the loss of volatile material after the residue has been poured
into the residue container.
5. Apparatus
5.1 Distillation Flask, 500-mL side-arm, having the dimensions shown in Fig. 1.
5.2 Condenser, standard glass-jacketed, of nominal jacket length from 200 to 300 mm and overall tube length of 450 6 10 mm
(see Fig. 3).
5.3 Adapter, heavy-wall (1-mm) glass, with reinforced top, having an angle of approximately 105°. The inside diameter at the
large end shall be approximately 18 mm, and at th
...
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