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ASTM D2042-01

(Test Method)

Standard Test Method for Solubility of Asphalt Materials in Trichloroethylene

Standard Test Method for Solubility of Asphalt Materials in Trichloroethylene

SIGNIFICANCE AND USE
This test method is a measure of the solubility of asphalt in trichloroethylene. The portion that is soluble in trichloroethylene represents the active cementing constituents.
SCOPE
1.1 This test method covers the determination of the degree of solubility in trichloroethylene of asphalt materials having little or no mineral matter.
Note 1—Use of carbon disulfide, carbon tetrachloride, and benzene has been discontinued in this method because of the safety hazards involved. This method is not applicable to tars and their distillation residues or highly cracked petroleum products. For methods covering tars, pitches, and other highly cracked petroleum products, and the use of other solvents, see Test Methods D 4, D 2318, and D 2764.
1.2 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. Specific precaution statements are given in Section 7.

General Information

Status
Historical
Publication Date
09-Dec-2001
ICS
75.140 - Waxes, bituminous materials and other petroleum products
Technical Committee
D04 - Road and Paving Materials
Drafting Committee
D04.47 - Miscellaneous Asphalt Tests
Current Stage
Ref Project

Relations

Replaces
ASTM D2042-97 - Standard Test Method for Solubility of Asphalt Materials in Trichloroethylene
Effective Date
10-Dec-2001
Replaced By
ASTM D2042-09 - Standard Test Method for Solubility of Asphalt Materials in Trichloroethylene
Effective Date
01-Jun-2009
Referred By
ASTM D2027/D2027M-19 - Standard Specification for Cutback Asphalt (Medium-Curing Type)
Effective Date
10-Dec-2001
Referred By
ASTM D5505-14(2020) - Standard Practice for Classifying Emulsified Recycling Agents
Effective Date
10-Dec-2001
Referred By
ASTM D977-20 - Standard Specification for Emulsified Asphalt
Effective Date
10-Dec-2001
Referred By
ASTM D244-09(2017) - Standard Test Methods and Practices for Emulsified Asphalts
Effective Date
10-Dec-2001
Referred By
ASTM D8239-23 - Standard Specification for Performance-Graded Asphalt Binder Using the Multiple Stress Creep and Recovery (MSCR) Test
Effective Date
10-Dec-2001
Referred By
ASTM D8125-18(2023) - Standard Specification for Re-Refined Engine Oil Bottoms (REOB)/Vacuum Tower Asphalt Extender (VTAE)
Effective Date
10-Dec-2001
Referred By
ASTM D2028/D2028M-15(2021)e1 - Standard Specification for Cutback Asphalt (Rapid-Curing Type)
Effective Date
10-Dec-2001
Referred By
ASTM D6152/D6152M-12(2018) - Standard Specification for SEBS-Modified Mopping Asphalt Used in Roofing
Effective Date
10-Dec-2001
Referred By
ASTM D449/D449M-03(2021) - Standard Specification for Asphalt Used in Dampproofing and Waterproofing
Effective Date
10-Dec-2001
Referred By
ASTM D3381/D3381M-18 - Standard Specification for Viscosity-Graded Asphalt Binder for Use in Pavement Construction
Effective Date
10-Dec-2001
Referred By
ASTM D7654/D7654M-10(2018) - Standard Specification for Asphalt Used in Roofing Measured by Dynamic Shear Rheometer
Effective Date
10-Dec-2001
Referred By
ASTM D3141/D3141M-21 - Standard Specification for Asphalt for Undersealing Portland-Cement Concrete Pavements
Effective Date
10-Dec-2001
Referred By
ASTM D2397/D2397M-20 - Standard Specification for Cationic Emulsified Asphalt
Effective Date
10-Dec-2001

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ASTM D2042-01 - Standard Test Method for Solubility of Asphalt Materials in TrichloroethyleneASTM D2042-01 - Standard Test Method for Solubility of Asphalt Materials in Trichloroethylene
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ASTM D2042-01 - Standard Test Method for Solubility of Asphalt Materials in Trichloroethylene
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Standards Content (Sample)

NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
Designation:D2042–01
Standard Test Method for
1
Solubility of Asphalt Materials in Trichloroethylene
This standard is issued under the fixed designation D 2042; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (e) indicates an editorial change since the last revision or reapproval.
This standard has been approved for use by agencies of the Department of Defense.
1. Scope 3. Summary of Method
1.1 This test method covers the determination of the degree 3.1 The sample is dissolved in trichloroethylene and filtered
of solubility in trichloroethylene of asphalt materials having through a glass fiber pad. The insoluble material is washed,
little or no mineral matter. dried, and weighed.
NOTE 1—Useofcarbondisulfide,carbontetrachloride,andbenzenehas
4. Significance and Use
been discontinued in this method because of the safety hazards involved.
4.1 This test method is a measure of the solubility of asphalt
This method is not applicable to tars and their distillation residues or
in trichloroethylene. The portion that is soluble in trichloroet-
highly cracked petroleum products. For methods covering tars, pitches,
and other highly cracked petroleum products, and the use of other hylene represents the active cementing constituents.
solvents, see Test Methods D 4, D 2318, and D 2764.
5. Apparatus and Materials
1.2 This standard does not purport to address all of the
5.1 The assembly of the filtering apparatus is illustrated in
safety concerns, if any, associated with its use. It is the
Fig. 1. Details of the component parts are as follows:
responsibility of the user of this standard to establish appro-
5.1.1 Gooch Crucible, glazed inside and outside with the
priate safety and health practices and determine the applica-
exception of outside bottom surface. The approximate dimen-
bility of regulatory limitations prior to use. Specific precaution
sions shall be a diameter of 44 mm at the top, tapering to 36
statements are given in Section 7.
mm at the bottom, and a depth of 24-28 mm.
7
2. Referenced Documents
5.1.2 Glass Fiber Pad, 3.2-cm.
5.1.3 Filter Flask, heavy-wall, with side tube, 250- or
2.1 ASTM Standards:
2
500-mL capacity.
D 4 Test Method for Bitumen Content
5.1.4 Filter Tube, 40- to 42-mm inside diameter.
D 2318 Test Method for Quinoline-Insoluble (QI) Content
3
5.1.5 Rubber Tubing or Adapter, for holding the Gooch
of Tar and Pitch
crucible on the filter tube.
D 2764 Test Method for Dimethylformamide-Insoluble
4
(DMF-I) Content of Tar and Pitch
NOTE 2—Other suitable assemblies permitting vacuum filtration with a
E 177 Practice for the Use of the Terms Precision and Bias
Gooch crucible may be used.
5
in ASTM Test Methods
5.1.6 Erlenmeyer Flask, 125 mL.
2.2 AASHTO Standard:
5.1.7 Oven, capable of maintaining a temperature of 110 6
T44 Solubility of Bituminous Materials in Organic Sol-
5°C.
6
vents
6. Reagent
1
6.1 Trichloroethylene, technical grade.
This test method is under the jurisdiction of ASTM Committee D04 on Road
and Paving Materials and is the direct responsibility of Subcommittee D04.47 on
Miscellaneous Asphalt Tests. 7. Safety Precautions
Current edition approved Dec. 10, 2001. Published March 2002. Originally
7.1 Trichloroethylene is toxic, and good ventilation should
published as D 2042 – 66. Last previous edition D 2042 – 97.
2
be provided. It is more flammable than carbon tetrachloride.
Annual Book of ASTM Standards, Vol 04.04.
3
Annual Book of ASTM Standards, Vol 05.01.
4
Annual Book of ASTM Standards, Vol 05.02.
5
Annual Book of ASTM Standards, Vol 14.02.
6 7
Available fromAASHTO, 444 N. Capitol St., NW, Suite 249, Washington, DC Whatman Grade 934 AH glass microfiber filter pad, available from Reeves
20001. Angel and Co., Clifton, NJ, has been found suitable.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, United States.
1

---------------------- Page: 1 ----------------------
D2042–01
appreciable, retain as much of it as possible in the container
until the solution has drained through the mat. Wash the
containerwithasmallamountofsolventand,usingastreamof
solvent from a wash bottle, transfer all insoluble matter to the
crucible. Use a “policeman” if necessary to remove any
insolublematteradheringtothecontainer.Rinsethepoliceman
and container thoroughly. Wash the insoluble matter in the
crucible with solvent until the filtrate is substantially colorless,
then apply strong suction to remove the remaining solvent.
Remove the crucible from the tube, wash the bottom free of
any dissolved matter, and place the crucible on top of an oven
or on a steam bath until all odor of the trichloroethylene is
removed (see safety prec
...

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5.1 This method indicates approximate change in properties of asphalt during conventional hot-mixing at about 150 °C [302 °F] as indicated by viscosity, penetration, or ductility measurements. It yields a residue which approximates the asphalt condition as incorporated in the pavement. If the mixing temperature differs appreciably from the 150 °C [302 °F] level, more or less effect on properties will occur.
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1.3 Warning—Mercury has been designated by the United States Environmental Protection Agency and many state agencies as a hazardous material that can cause central nervous system, kidney, and liver damage. Mercury, or its vapor, may be hazardous to health and corrosive to materials. Caution should be taken when handling mercury and mercury-containing products. See the applicable Material Safety Data Sheet (MSDS) for details and EPA’s website—http://www.epa.gov/mercury/index.htm—for additional information. Users should be aware that selling mercury and/or mercury-containing products into your state may be prohibited by state law.  
1.4 The text of this standard references notes and footnotes which provide explanatory material. These notes and footnotes (excluding those in tables and figures) shall not be considered as requirements of the standard.  
1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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ASTM
ASTM D7870/D7870M-20(Practice)
Standard Practice for Moisture Conditioning Compacted Asphalt Mixture Specimens by Using Hydrostatic Pore Pressure

SIGNIFICANCE AND USE
4.1 This practice provides an accelerated conditioning method under cyclic loading. This system is capable of operating at higher than normal temperatures and creating pore pressure within a compacted asphalt mixture to achieve an acceleration of the effects that a mixture would experience over time from traffic at normal temperatures and conditions. The accelerated conditioning in this practice is intended to simulate the stresses induced in a wet pavement by a passing vehicle tire. The pulse shape produced by this system approximates a Lorentzian function with a half peak width of approximately 1 s at 276 kPa [40 psi].  
4.2 The factors that influence the potential for moisture damage to occur include aggregate mineralogy, mixture air voids, water, cyclic applied stress, and elevated temperature. This practice provides a method and apparatus that is capable of producing three of these factors: water, stress, and high temperature. Aggregate mineralogy and air voids are mixture properties.  
4.3 Specimens conditioned by this system can be tested using a variety of different tests, including Test Method D6931, Test Method D6927, bulk specific gravity difference obtained by Test Method D6926 or D6752/D6752M for before and after conditioning, dynamic modulus, flow number, AASHTO T 378, and visual inspection for stripped aggregates.
Note 1: The quality of the results produced by this standard are dependent on the competence of the personnel performing the procedure and the capability, calibration, and maintenance of the equipment used. Agencies that meet the criteria of Specification D3666 are generally considered capable of competent and objective testing, sampling, inspection, etc. Users of this standard are cautioned that compliance with Specification D3666 alone does not completely ensure reliable results. Reliable results depend on many factors; following the suggestions of Specification D3666 or some similar acceptance guideline provides a means of evaluating ...
SCOPE
1.1 This practice includes procedures for preparing compacted asphalt mixture specimens, exposing the specimens to hydrostatic pore pressure inside an enclosed chamber, and guidance on testing the specimens for the effect of water on the tensile strength or change in other properties of the asphalt mixture, such as density, modulus, etc.  
1.2 Specimens conditioned according to this practice can be tested using methods and test procedures referenced in this document, and those results may provide information as to the effect of the moisture conditioning of this practice on the moisture sensitivity of those mixtures.  
1.3 The text of this standard references notes and footnotes which provide explanatory material. These notes and footnotes (excluding those in tables and figures) shall not be considered as requirements of the standard.  
1.4 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the two systems may result in nonconformance with the standard.  
1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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ASTM
ASTM D7173-20(Practice)
Standard Practice for Determining the Separation Tendency of Polymer from Polymer-Modified Asphalt

SIGNIFICANCE AND USE
4.1 Purchasers of polymer-modified asphalt need guidelines on proper storage and handling procedures to maintain the integrity of material they have purchased. This practice provides a significant tool for understanding the characteristics of these materials as well as comparing various sources of supply.
Note 1: The quality of the results produced by this standard are dependent on the competence of the personnel performing the procedure and the capability, calibration, and maintenance of the equipment used. Agencies that meet the criteria of Specification D3666 are generally considered capable of competent and objective testing, sampling, inspection, etc. Users of this standard are cautioned that compliance with Specification D3666 alone does not completely ensure reliable results. Reliable results depend on many factors; following the suggestions of Specification D3666 or some similar acceptable guideline provides a means of evaluating and controlling some of those factors.
SCOPE
1.1 This practice describes a laboratory procedure for determining the tendency of polymer to separate from polymer-modified asphalt under static heated storage conditions. The results of testing on material prepared according to this practice may be used as a guideline when formulating products or to establish field handling procedures. Large differences in test results between top and bottom specimens indicate that there is a degree of incompatibility between the polymer and the base asphalt.  
1.2 The values stated in SI units are to be regarded as the standard. No other units of measurement are included in this standard.  
1.3 The text of this standard references notes and footnotes which provide explanatory material. These notes and footnotes (excluding those in tables and figures) shall not be considered as requirements of the standard.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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