ASTM C1470-20
(Guide)Standard Guide for Testing the Thermal Properties of Advanced Ceramics
Standard Guide for Testing the Thermal Properties of Advanced Ceramics
SIGNIFICANCE AND USE
5.1 The high-temperature capabilities of advanced ceramics are a key performance benefit for many demanding engineering applications. In many of those applications, advanced ceramics will have to perform across a broad temperature range. The thermal expansion, thermal diffusivity/conductivity, specific heat, and emittance/emissivity are crucial engineering factors in integrating ceramic components into aerospace, automotive, and industrial systems.
5.2 This guide is intended to serve as a reference and information source for testing the thermal properties of advanced ceramics, based on an understanding of the relationships between the composition and microstructure of these materials and their thermal properties.
5.3 The use of this guide assists the testing community in correctly applying the ASTM thermal test methods to advanced ceramics to ensure that the thermal test results are properly measured, interpreted, and understood. This guide also assists the user in selecting the appropriate thermal test method to evaluate the particular thermal properties of the advanced ceramic of interest.
5.4 The thermal properties of advanced ceramics are critical data in the development of ceramic components for aerospace, automotive, and industrial applications. In addition, the effect of environmental exposure on thermal properties of the advanced ceramics must also be assessed.
SCOPE
1.1 This guide covers the thermal property testing of advanced ceramics, to include monolithic ceramics, particulate/ whisker-reinforced ceramics, and continuous fiber-reinforced ceramic composites. It is intended to provide guidance and information to users on the special considerations involved in determining the thermal properties of these ceramic materials.
1.2 Five thermal properties (specific heat capacity, thermal conductivity, thermal diffusivity, thermal expansion, and emittance/emissivity) are presented in terms of their definitions and general test methods. The relationship between thermal properties and the composition, microstructure, and processing of advanced ceramics (monolithic and composite) is briefly outlined, providing guidance on which material and specimen characteristics have to be considered in evaluating the thermal properties of advanced ceramics. Additional sections describe sampling considerations, test specimen preparation, and reporting requirements.
1.3 Current ASTM test methods for thermal properties are tabulated in terms of test method concept, testing range, specimen requirements, standards/reference materials, capabilities, limitations, precision, and special instructions for monolithic and composite ceramics.
1.4 This guide is based on the use of current ASTM standards for thermal properties, where appropriate, and on the development of new test standards, where necessary. It is not the intent of this guide to rigidly specify particular thermal test methods for advanced ceramics. Guidance is provided on how to utilize the most commonly available ASTM thermal test methods, considering their capabilities and limitations.
1.5 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard. See IEEE/ASTM SI 10.
1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the
Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
Designation: C1470 − 20
Standard Guide for
1
Testing the Thermal Properties of Advanced Ceramics
This standard is issued under the fixed designation C1470; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision.Anumber in parentheses indicates the year of last reapproval.A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope priate safety, health, and environmental practices and deter-
mine the applicability of regulatory limitations prior to use.
1.1 This guide covers the thermal property testing of ad-
1.7 This international standard was developed in accor-
vanced ceramics, to include monolithic ceramics, particulate/
dance with internationally recognized principles on standard-
whisker-reinforced ceramics, and continuous fiber-reinforced
ization established in the Decision on Principles for the
ceramic composites. It is intended to provide guidance and
Development of International Standards, Guides and Recom-
information to users on the special considerations involved in
mendations issued by the World Trade Organization Technical
determining the thermal properties of these ceramic materials.
Barriers to Trade (TBT) Committee.
1.2 Five thermal properties (specific heat capacity, thermal
conductivity, thermal diffusivity, thermal expansion, and 2. Referenced Documents
emittance/emissivity)arepresentedintermsoftheirdefinitions 2
2.1 ASTM Standards:
and general test methods. The relationship between thermal
2.1.1 Specific Heat:
propertiesandthecomposition,microstructure,andprocessing
C351Test Method for Mean Specific Heat of Thermal
3
of advanced ceramics (monolithic and composite) is briefly
Insulation (Withdrawn 2008)
outlined, providing guidance on which material and specimen
D2766Test Method for Specific Heat of Liquids and Solids
3
characteristics have to be considered in evaluating the thermal
(Withdrawn 2018)
properties of advanced ceramics. Additional sections describe
E1269Test Method for Determining Specific Heat Capacity
samplingconsiderations,testspecimenpreparation,andreport-
by Differential Scanning Calorimetry
ing requirements.
E2716Test Method for Determining Specific Heat Capacity
1.3 Current ASTM test methods for thermal properties are by Sinusoidal Modulated Temperature Differential Scan-
tabulated in terms of test method concept, testing range, ning Calorimetry
specimen requirements, standards/reference materials, 2.1.2 Thermal Conductivity:
capabilities, limitations, precision, and special instructions for C177Test Method for Steady-State Heat Flux Measure-
monolithic and composite ceramics. ments and Thermal Transmission Properties by Means of
the Guarded-Hot-Plate Apparatus
1.4 This guide is based on the use of current ASTM
C182Test Method for Thermal Conductivity of Insulating
standardsforthermalproperties,whereappropriate,andonthe
Firebrick
development of new test standards, where necessary. It is not
C201Test Method forThermal Conductivity of Refractories
theintentofthisguidetorigidlyspecifyparticularthermaltest
C202Test Method for Thermal Conductivity of Refractory
methods for advanced ceramics. Guidance is provided on how
Brick
to utilize the most commonly available ASTM thermal test
C408Test Method for Thermal Conductivity of Whiteware
methods, considering their capabilities and limitations.
Ceramics
1.5 The values stated in SI units are to be regarded as
C518Test Method for Steady-State Thermal Transmission
standard. No other units of measurement are included in this
Properties by Means of the Heat Flow Meter Apparatus
standard. See IEEE/ASTM SI10.
C767Test Method for Thermal Conductivity of Carbon
1.6 This standard does not purport to address all of the Refractories
safety concerns, if any, associated with its use. It is the
C1044Practice for Using a Guarded-Hot-PlateApparatus or
responsibility of the user of this standard to establish appro- Thin-Heater Apparatus in the Single-Sided Mode
1 2
This guide is under the jurisdiction of ASTM Committee C28 on Advanced For referenced ASTM standards, visit the ASTM website, www.astm.org, or
Ceramics and is the direct responsibility of Subcommittee C28.03 on Physical contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
Properties and Non-Destructive Evaluation. Standards volume information, refer to the standard’s Document Summary page on
Current edition approved Jan. 1, 2020. Published January 2020. Originally the ASTM website.
3
approved in 2000. Last previous edition approved in 2013 as C1470–06 (2013). The last approved version of this historical standard is referenced on
...
This document is not an ASTM standard and is intended only to provide the user of an ASTM standard an indication of what changes have been made to the previous version. Because
it may not be technically possible to adequately depict all changes accurately, ASTM recommends that users consult prior editions as appropriate. In all cases only the current version
of the standard as published by ASTM is to be considered the official document.
Designation: C1470 − 06 (Reapproved 2013) C1470 − 20
Standard Guide for
1
Testing the Thermal Properties of Advanced Ceramics
This standard is issued under the fixed designation C1470; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope
1.1 This guide covers the thermal property testing of advanced ceramics, to include monolithic ceramics, particulate/
whisker-reinforced ceramics, and continuous fiber-reinforced ceramic composites. It is intended to provide guidance and
information to users on the special considerations involved in determining the thermal properties of these ceramic materials.
1.2 Five thermal properties (specific heat capacity, thermal conductivity, thermal diffusivity, thermal expansion, and
emittance/emissivity) are presented in terms of their definitions and general test methods. The relationship between thermal
properties and the composition, microstructure, and processing of advanced ceramics (monolithic and composite) is briefly
outlined, providing guidance on which material and specimen characteristics have to be considered in evaluating the thermal
properties of advanced ceramics. Additional sections describe sampling considerations, test specimen preparation, and reporting
requirements.
1.3 Current ASTM test methods for thermal properties are tabulated in terms of test method concept, testing range, specimen
requirements, standards/reference materials, capabilities, limitations, precision, and special instructions for monolithic and
composite ceramics.
1.4 This guide is based on the use of current ASTM standards for thermal properties, where appropriate, and on the development
of new test standards, where necessary. It is not the intent of this guide to rigidly specify particular thermal test methods for
advanced ceramics. Guidance is provided on how to utilize the most commonly available ASTM thermal test methods, considering
their capabilities and limitations.
1.5 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
See IEEE/ASTM SI 10.
1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility
of the user of this standard to establish appropriate safety safety, health, and healthenvironmental practices and determine the
applicability of regulatory limitations prior to use.
1.7 This international standard was developed in accordance with internationally recognized principles on standardization
established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued
by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
2. Referenced Documents
2
2.1 ASTM Standards:
2.1.1 Specific Heat:
3
C351 Test Method for Mean Specific Heat of Thermal Insulation (Withdrawn 2008)
3
D2766 Test Method for Specific Heat of Liquids and Solids (Withdrawn 2018)
E1269 Test Method for Determining Specific Heat Capacity by Differential Scanning Calorimetry
E2716 Test Method for Determining Specific Heat Capacity by Sinusoidal Modulated Temperature Differential Scanning
Calorimetry
2.1.2 Thermal Conductivity:
1
This guide is under the jurisdiction of ASTM Committee C28 on Advanced Ceramics and is the direct responsibility of Subcommittee C28.03 on Physical Properties
and Non-Destructive Evaluation.
Current edition approved Feb. 1, 2013Jan. 1, 2020. Published March 2013January 2020. Originally approved in 2000. Last previous edition approved in 20062013 as
C1470 – 06.C1470 – 06 (2013). DOI: 10.1520/C1470-06R13.10.1520/C1470-20.
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM Standards
volume information, refer to the standard’s Document Summary page on the ASTM website.
3
The last approved version of this historical standard is referenced on www.astm.org.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
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C1470 − 20
C177 Test Method for Steady-State Heat Flux Measurements and Thermal Transmission Properties by Means of the
Guarded-Hot-Plate Apparatus
C182 Test Method for Thermal Conductivity o
...
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