ASTM D7357-07(2012)
(Specification)Standard Specification for Cellulose Fibers for Fiber-Reinforced Concrete
Standard Specification for Cellulose Fibers for Fiber-Reinforced Concrete
SCOPE
1.1 This specification covers minimum requirements for cellulose fibers intended for use in fiber-reinforced concrete, and other cementitious products.
1.2 This specification provides for measurement of properties, definition of types, typical properties, and prescribes testing procedures to establish conformance to these requirements.
1.3 In the case of conflict between a more stringent requirement of a product specification and a requirement of this specification, the product specification shall prevail. In the case of a conflict between a requirement of the product specification or a requirement of this specification and a more stringent requirement of the purchase order, the purchase order shall prevail. The purchase order requirements shall not take precedence if they, in any way, violate the requirements of the product specification or this specification; for example, by the waiving of a test requirement or by making a test requirement less stringent.
1.4 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the two systems may result in non-conformance with the standard.
1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.
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Designation: D7357 −07 (Reapproved 2012)
Standard Specification for
Cellulose Fibers for Fiber-Reinforced Concrete
This standard is issued under the fixed designation D7357; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope C1116 Specification for Fiber-Reinforced Concrete and
Shotcrete
1.1 This specification covers minimum requirements for
D6942 Test Method for Stability of Cellulose Fibers in
cellulose fibers intended for use in fiber-reinforced concrete,
Alkaline Environments
and other cementitious products.
2.2 TAPPI (Technical Association of the Pulp and Paper
1.2 This specification provides for measurement of
Industry):
properties, definition of types, typical properties, and pre-
T 205 Forming handsheets for physical tests of pulps
scribes testing procedures to establish conformance to these
T 222 Acid-insoluble lignin in wood and pulp
requirements.
T 231 Zero-span breaking strength of pulp (dry zero-span
1.3 In the case of conflict between a more stringent require-
tensile)
ment of a product specification and a requirement of this
T 232 Fiber length of pulp by projection
specification,theproductspecificationshallprevail.Inthecase
T 233 Fiber length of pulp by classification
of a conflict between a requirement of the product specification
T 234 Coarseness of pulp fibers
or a requirement of this specification and a more stringent
T 236 Kappa number of pulp
requirement of the purchase order, the purchase order shall
T 259 Species identification of non-wood plant fibers
prevail. The purchase order requirements shall not take prece-
T 263 Identification of wood and fibers from conifers
dence if they, in any way, violate the requirements of the 4
2.3 ACI (American Concrete Institute) Documents:
product specification or this specification; for example, by the
544.1R Committee Report on Fiber-Reinforced Concrete
waiving of a test requirement or by making a test requirement
2.4 ICC-ES Documents:
less stringent.
AC 217 Acceptance Criteria for Concrete with Virgin Cel-
1.4 The values stated in either SI units or inch-pound units
lulose Fibers
are to be regarded separately as standard. The values stated in
each system may not be exact equivalents; therefore, each
3. Terminology
system shall be used independently of the other. Combining
3.1 Definitions:
values from the two systems may result in non-conformance
3.1.1 alkaline stability, n—resistance to strength loss due to
with the standard.
exposuretoalkalineenvironments,asmeasuredinTestMethod
1.5 This standard does not purport to address all of the
D6942.
safety concerns, if any, associated with its use. It is the
3.1.2 coarseness, n—linear density given in units of mg/
responsibility of the user of this standard to establish appro-
100m. (See TAPPI T 234.) This unit is termed decigrex, and
priate safety and health practices and determine the applica-
can be converted to the standard textile linear density unit,
bility of regulatory limitations prior to use.
denier, which is weight in grams of 9000 meters of synthetic
fiber.
2. Referenced Documents
3.1.3 durability/compatibility with concrete, n—resistance
2.1 ASTM Standards:
to strength loss based on ZSSR testing (Test Method D6942)
using saturated calcium hydroxide and 1N sodium hydroxide
This specification is under the jurisdiction of ASTM Committee D01 on Paint
as alkaline environments. (See ICC-ES AC 217, section 4.6.)
and Related Coatings, Materials, andApplications and is the direct responsibility of
Subcommittee D01.36 on Cellulose and Cellulose Derivatives.
Current edition approved June 1, 2012. Published August 2012. Originally
approved in 2007. Last previous edition approved in 2007 as D7357 – 07. DOI: Available from TechnicalAssociation of the Pulp and Paper Industry (TAPPI),
10.1520/D7357-07R12. 15 Technology Parkway South, Norcross, GA 30092, http://www.tappi.org.
2 4
For referenced ASTM standards, visit the ASTM website, www.astm.org, or Available fromAmerican Concrete Institute (ACI), P.O. Box 9094, Farmington
contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM Hills, MI 48333-9094, http://www.aci-int.org.
Standards volume information, refer to the standard’s Document Summary page on Available from ICC-ES, 5360 Workman Mill Road, Whittier, CA 90601,
the ASTM website. http://www.icc-es.org, under “Approved Criteria.”
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
D7357 − 07 (2012)
3.1.4 zero-span stability ratio (ZSSR), n— the ratio of the 7.2 Unbleached, semibleached and fully bleached chemical
zero-span tensile after exposure to an alkaline environment to wood pulps have cellulose as the predominant polymer. Unpu-
the zero-span tensile of the control fibers (that is, fibers not rified vegetable fibers will have hemicelluloses as the predomi-
exposed to an alkaline environment) as defined in Test Method nate polymer.
D6942.
7.3 Mechanical wood pulps will have approximately equal
amounts of cellulose, hemicellulose, and lignin.
3.1.5 zero-span tensile, n—measurement of individual fiber
strength, as defined in TAPPI Method T 231 based on testing
7.4 Purified chemical (“fully bleached”) wood pulps do not
standard handsheets made according to TAPPI Method T 205.
contain lignin, but mechanical, unbleached, and semi-bleached
pulps still retain some residual lignin. Fibers that are not
4. Classification
lignin-free should be certified by the level of lignin present
using either the kappa number test (TAPPI T 236) or the
4.1 Cellulose fibers are described in ACI 544.1R-96, chap-
acid-insoluble lignin test (TAPPI T 222).
ter 5 as a class of natural fibers. Specification C1116 also uses
the term natural fiber to describe cellulosic fibers.
8. Physical Properties
4.2 Unknown cellulosic plant fibers must be identified as
8.1 The average fiber length of the cellulosic fibers will be
such or identified by appropriate microscopic examination.
specified based on projected length (TAPPI T 232), classified
(TAPPIT 259providesfortheidentificationofnon-woodplant
length (TAPPI T 233) or instrumental determination by a fiber
fibers, and T 263 provides for the identification of fibers from
analyzer.
conifers.)
8.2 The average fiber coarseness of the cellulosic fibers will
4.3 If known, the common name and scientific classification
be specified based on microscopic examination (TAPPI T 234)
of the fibers will be provided. For example, wood fibers
or instrumental determination by a fiber analyzer.
derived from pulping slash pine trees should be designated;
8.3 The average zero-span tensile strength of the cellulosic
“slash pine (Pinus elliottii ) fibers.” A classificati
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