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ASTM D3803-91(2022)

(Test Method)

Standard Test Method for Nuclear-Grade Activated Carbon

Standard Test Method for Nuclear-Grade Activated Carbon

SIGNIFICANCE AND USE
5.1 The results of this test method give a conservative estimate of the performance of nuclear-grade activated carbon used in all nuclear power plant HVAC systems for the removal of radioiodine.
SCOPE
1.1 This test method is a very stringent procedure for establishing the capability of new and used activated carbon to remove radio-labeled methyl iodide from air and gas streams. The single test method described is for application to both new and used carbons, and should give test results comparable to those obtained from similar tests required and performed throughout the world. The conditions employed were selected to approximate operating or accident conditions of a nuclear reactor which would severely reduce the performance of activated carbons. Increasing the temperature at which this test is performed generally increases the removal efficiency of the carbon by increasing the rate of chemical and physical absorption and isotopic exchange, that is, increasing the kinetics of the radioiodine removal mechanisms. Decreasing the relative humidity of the test generally increases the efficiency of methyl iodide removal by activated carbon. The water vapor competes with the methyl iodide for adsorption sites on the carbon, and as the amount of water vapor decreases with lower specified relative humidities, the easier it is for the methyl iodide to be adsorbed. Therefore, this test method is a very stringent test of nuclear-grade activated carbon because of the low temperature and high relative humidity specified. This test method is recommended for the qualification of new carbons and the quantification of the degradation of used carbons.  
1.1.1 Guidance for testing new and used carbons using conditions different from this test method is offered in Annex A1.  
1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

General Information

Status
Published
Publication Date
31-Aug-2022
ICS
71.040.30 - Chemical reagents
Technical Committee
D28 - Activated Carbon
Drafting Committee
D28.04 - Gas Phase Evaluation Tests
Current Stage
Ref Project

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ASTM D3803-91(2022) - Standard Test Method for Nuclear-Grade Activated Carbon
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Standards Content (Sample)

This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the
Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
Designation: D3803 − 91 (Reapproved 2022)
Standard Test Method for
1
Nuclear-Grade Activated Carbon
This standard is issued under the fixed designation D3803; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision.Anumber in parentheses indicates the year of last reapproval.A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope 1.4 This international standard was developed in accor-
dance with internationally recognized principles on standard-
1.1 This test method is a very stringent procedure for
ization established in the Decision on Principles for the
establishing the capability of new and used activated carbon to
Development of International Standards, Guides and Recom-
remove radio-labeled methyl iodide from air and gas streams.
mendations issued by the World Trade Organization Technical
Thesingletestmethoddescribedisforapplicationtobothnew
Barriers to Trade (TBT) Committee.
and used carbons, and should give test results comparable to
those obtained from similar tests required and performed
2. Referenced Documents
throughout the world. The conditions employed were selected
2
2.1 ASTM Standards:
to approximate operating or accident conditions of a nuclear
D1193Specification for Reagent Water
reactor which would severely reduce the performance of
D2652Terminology Relating to Activated Carbon
activatedcarbons.Increasingthetemperatureatwhichthistest
D2854Test Method for Apparent Density of Activated
is performed generally increases the removal efficiency of the
Carbon
carbon by increasing the rate of chemical and physical absorp-
E300Practice for Sampling Industrial Chemicals
tion and isotopic exchange, that is, increasing the kinetics of
E691Practice for Conducting an Interlaboratory Study to
the radioiodine removal mechanisms. Decreasing the relative
Determine the Precision of a Test Method
humidityofthetestgenerallyincreasestheefficiencyofmethyl
2.2 Code of Federal Regulations:
iodideremovalbyactivatedcarbon.Thewatervaporcompetes
CFR Title 49,Section 173.34, “Qualification, Maintenance,
with the methyl iodide for adsorption sites on the carbon, and
3
and Use of Cylinders’’
as the amount of water vapor decreases with lower specified
CFR Title 49,Part 178, Subpart C, “Specifications for
relative humidities, the easier it is for the methyl iodide to be
3
Cylinders’’
adsorbed.Therefore, this test method is a very stringent test of
2.3 Military Standards:
nuclear-grade activated carbon because of the low temperature
MIL-F-51068D Filter, Particulate High Efficiency, Fire
and high relative humidity specified. This test method is
4
Resistant
recommended for the qualification of new carbons and the
MIL-F-51079A Filter, Medium Fire Resistant, High Effi-
quantification of the degradation of used carbons.
4
ciency
1.1.1 Guidance for testing new and used carbons using
4
MIL-STD-45662 Calibration Systems Requirements
conditions different from this test method is offered in Annex
2.4 Other Standards:
A1.
ANSI/ASME N45.2.6 Qualifications of Inspection,
1.2 The values stated in SI units are to be regarded as
Examination, and Testing Personnel for Nuclear Power
standard. No other units of measurement are included in this 5
Plants
standard.
3. Terminology
1.3 This standard does not purport to address all of the
safety concerns, if any, associated with its use. It is the
3.1 Definitions of Terms Specific to This Standard:
responsibility of the user of this standard to establish appro-
priate safety, health, and environmental practices and deter-
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or
mine the applicability of regulatory limitations prior to use.
contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
Standards volume information, refer to the standard’s Document Summary page on
the ASTM website.
3
Published by the General Service Administration, 18th and “F”’ St., N. W.,
1
This test method is under the jurisdiction of ASTM Committee D28 on Washington, DC 20405.
4
Activated Carbon and is the direct responsibility of Subcommittee D28.04 on Gas Available from Standardization Documents Order Desk, DODSSP, Bldg. 4,
Phase Evaluation Tests. Section D, 700 Robbins Ave., Philadelphia, PA 19111-5098, http://
Current edition approved Sept. 1, 2022. Published October 2022. Originally dodssp.daps.dla.mil.
5
approved in 1979. Last previous edition approved in 2014 as D3803–91 (2014). Available fromAmerican National Standards Institute (ANSI), 25 W. 43rd St.,
DOI: 10.1520/D3803-91R22. 4th Floor, New York, NY 10036, http://www.ansi.org.
Copyright
...

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ASTM D2867-23(Test Method)
Standard Test Methods for Moisture in Activated Carbon

SIGNIFICANCE AND USE
4.1 The moisture content of activated carbon is often required to define and express its properties in relation to the net weight of the carbon.  
4.2 The moisture content of activated carbon packed in typical shipping containers will usually increase during transportation and storage. Users of activated carbon in applications where low moisture content is important should be aware of this effect.
SCOPE
1.1 These test methods provide three procedures for the determination of the moisture content of activated carbon. The procedures may also be used to dry samples required for other tests. The oven drying and moisture balance methods are used when water is the only volatile material present and is in significant quantities, and the activated carbon is not heat sensitive (some activated carbons can ignite spontaneously at temperatures as low as 150 °C). The xylene extraction method is used when a carbon is known or suspected to be heat sensitive or to contain miscible organic compounds instead of or in addition to water. The interferences posed by miscible inorganic compounds has not been determined. The oven drying method described in these test methods may be used as the reference for development of instrumental techniques for moisture determination in activated carbon.  
1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
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ASTM D5158-23(Test Method)
Standard Test Method for Determination of Particle Size of Fine Mesh and Powdered Activated Carbon by Air-Jet Sieving

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5.1 The particle size of fine mesh and powdered activated carbon is sometimes used to evaluate filter cake filtration rates and the filter penetration in filtering applications.  
5.2 The selection and handling of fine mesh or powdered activated carbon, and operation of processes using fine mesh or powdered activated carbon, requires the knowledge of the particle size.  
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Note 1: Relative humidity (RH) can affect the repeatability and accuracy of this test. Activated carbon not at equilibrium with the RH of the ambient air may lose or gain weight accordingly, dependent upon whether the carbon picks up or loses moisture.
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1.1 This test method covers the determination of the particle size of powdered activated carbons using an air-jet sieve device. For purposes of this test method, powdered activated carbon is defined as activated carbon in particle sizes predominantly in a range of 80 mesh (0.180 mm) through 500 mesh (0.025 mm).  
1.2 The values stated in SI units are to be regarded as the standard. The inch-pound units given in parentheses are for information only.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
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ASTM D8176-18(2023)(Test Method)
Standard Test Method for Mechanically Tapped Density of Activated Carbon (Powdered and Fine Mesh)

SIGNIFICANCE AND USE
5.1 This test method is used to determine the density expressed in g/mL for powdered or fine mesh carbon. Due to the nature of the small particles, the density of these carbon types cannot be measured using the same procedure as granular carbon.
SCOPE
1.1 This test method covers the determination of the mechanically tapped density of powdered and fine mesh activated carbon. For the purpose of this test method, “powdered carbon” is defined as having a mean particle diameter less than 45 µm, and “fine mesh carbon” is defined as having a particle size predominately between 80 and 325 U.S. Standard mesh.  
1.2 The values in SI units are to be regarded as standard. No other units of measure are included in this standard.  
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ASTM D6646-03(2022)(Test Method)
Standard Test Method for Determination of the Accelerated Hydrogen Sulfide Breakthrough Capacity of Granular and Pelletized Activated Carbon

SIGNIFICANCE AND USE
5.1 This method compares the performance of granular or pelletized activated carbons used in odor control applications, such as sewage treatment plants, pump stations, etc. The method determines the relative breakthrough performance of activated carbon for removing hydrogen sulfide from a humidified gas stream. Other organic contaminants present in field operations may affect the H2S breakthrough capacity of the carbon; these are not addressed by this test. This test does not simulate actual conditions encountered in an odor control application, and is therefore meant only to compare the hydrogen sulfide breakthrough capacities of different carbons under the conditions of the laboratory test.  
5.2 This test does not duplicate conditions that an adsorber would encounter in practical service. The mass transfer zone in the 23 cm column used in this test is proportionally much larger than that in the typical bed used in industrial applications. This difference favors a carbon that functions more rapidly for removal of H2S over a carbon with slower kinetics. Also, the 1 % H2S challenge gas concentration used here engenders a significant temperature rise in the carbon bed. This effect may also differentiate between carbons in a way that is not reflected in the conditions of practical service.  
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SCOPE
1.1 This test method is intended to evaluate the performance of virgin, newly impregnated or in-service, granular or pelletized activated carbon for the removal of hydrogen sulfide from an air stream, under the laboratory test conditions described herein. A humidified air stream containing 1 % (by volume) hydrogen sulfide is passed through a carbon bed until 50 ppm breakthrough of H2S is observed. The H2S adsorption capacity of the carbon per unit volume at 99.5 % removal efficiency (g H2S/cm3 carbon) is then calculated. This test is not necessarily applicable to non-carbon adsorptive materials.  
1.2 This standard as written is applicable only to granular and pelletized activated carbons with mean particle diameters (MPD) less than 2.5 mm. See paragraph 5.3 if activated carbons with larger MPDs are to be tested.  
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Standard Guide for Dusting Attrition of Granular Activated Carbon

SIGNIFICANCE AND USE
4.1 Three forces can mechanically degrade a granular activated carbon: impact, crushing, and attrition. Of these three, attrition, or abrasion, is the most common cause of dust formation in actual service. Published test procedures to determine the “hardness” of activated carbons produce results that in general cannot be correlated with field experience. For example, the ball-pan hardness test applies all three forces to the sample in a variable manner determined by the size, shape, and density of the particles. The “stirring bar” abrasion test measures attrition so long as the particle size is smaller than 12 mesh. There is some evidence, however, that the results of this test method are influenced by particle geometry. The procedure set forth in this guide measures the effect of friction forces between vibrating or slowly moving particles during the test and may be only slightly dependent on particle size, shape, and density effects.
SCOPE
1.1 This guide presents a procedure for evaluating the resistance to dusting attrition of granular activated carbons. For the purpose of this guide, the dust attrition coefficient, DA, is defined as the weight (or calculated volume) of dust per unit time, collected on a preweighed filter, in a given vibrating device during a designated time per unit weight of carbon. The initial dust content of the sample may also be determined. Granular activated carbon is defined as a minimum of 90 % being larger than 80 mesh (0.18 mm) (see Test Methods D2867).  
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ASTM D6586-03(2021)(Practice)
Standard Practice for the Prediction of Contaminant Adsorption on GAC in Aqueous Systems Using Rapid Small-Scale Column Tests

SIGNIFICANCE AND USE
5.1 Granular activated carbon (GAC) is commonly used to remove contaminants from water. However if not used properly, GAC can not only be expensive but can at times be ineffective. The development of engineering data for the design of full-scale adsorbers often requires time-consuming and expensive pilot plant studies. This rapid standard practice has been developed to predict adsorption in large-scale adsorbers based upon results from small column testing. In contrast to pilot plant studies, the small-scale column test presented in this practice does not allow for a running evaluation of factors that may affect GAC performance over time. Such factors may include, for example, an increased removal of target compounds by bacterial colonizing GAC3 or long-term fouling of GAC caused by inorganic compounds or background organic matter.4 Nevertheless, this practice offers more relevant operational data than isotherm testing without the principal drawbacks of pilot plant studies, namely time and expense; and unlike pilot plant studies, small-scale studies can be performed in a laboratory using water sampled from a remote location.  
5.2 This practice known as the rapid small-scale column test (RSSCT) uses empty bed contact time (EBCT) and hydraulic loading to describe the adsorption process. Mean carbon particle diameter is used to scale RSSCT results to predict the performance of a full-scale adsorber.  
5.3 This practice can be used to compare the effectiveness of different activated carbons for the removal of contaminants from a common water stream.
SCOPE
1.1 This practice covers a test method for the evaluation of granular activated carbon (GAC) for the adsorption of soluble pollutants from water. This practice can be used to estimate the operating capacities of virgin and reactivated granular activated carbons. The results obtained from the small-scale column testing can be used to predict the adsorption of target compounds on GAC in a large column or full-scale adsorber application.  
1.2 This practice can be applied to all types of water including synthetically contaminated water (prepared by spiking high-purity water with selected contaminants), potable waters, industrial wastewaters, sanitary wastes, and effluent waters.  
1.3 This practice is useful for the determination of breakthrough curves for specific contaminants in water, the determination of the lengths of the adsorbates mass transfer zones (MTZ), and the prediction of GAC usage rates for larger scale adsorbers.  
1.4 The following safety caveat applies to the procedure section, Section 10, of this practice: This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
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ASTM D4069-95(2020)(Specification)
Standard Specification for Impregnated Activated Carbon Used to Remove Gaseous Radio-Iodines from Gas Streams

ABSTRACT
This standard covers the specifications for physical properties and performance requirements of virgin impregnated activated carbon to be used for the removal of gaseous radioiodine species from gas streams. The activated carbon furnished under this specification shall be virgin material. Each batch of impregnated activated carbon shall conform to the requirements for physical properties prescribed. The following test methods shall used to determine the physical properties and performance capability of the sample: apparent density; particle size distribution; ash content; moisture content; ignition temperature; ball-pan hardness; and pH.
SIGNIFICANCE AND USE
5.1 Activated carbons used in containment systems for nuclear reactors must be capable of functioning under both normal operating conditions and those conditions which may exist following a design basis accident (DBA). Adsorbent beds that are part of recirculatory systems inside containment may be exposed to the peak pressure, temperature, and steam content of a post-DBA condition.  
5.2 Carbon beds outside containment will be protected by fast-acting shutoff valves from the sudden rise in pressure, temperature, and humidity of the containment atmosphere which would exist following a DBA. However, some rise in temperature and humidity will be experienced even by beds outside containment if they are reconnected to containment after the initial pressure rise (due to escape of steam into the containment volume) has been reduced by containment coolers. The amount of radioactivity that can reach either type of adsorption system is conceivably quite high; hence, there is a possibility of a bed temperature rise due to decay heating. The gaseous radioactive contaminants of most interest are organic iodides. In this test, CH3I is used to typify the performance of the carbon on organic iodine compounds in general. The test described here provide a reasonable picture of the effectiveness of an activated carbon for organic iodides under normal and post-DBA conditions. The equipment and methods described can be used, with discretion, for similar tests at different gas flow conditions and, to some extent, on different gaseous radioactive contaminants and other adsorbents.
SCOPE
1.1 This standard covers the specifications for physical properties and performance requirements of virgin impregnated activated carbon to be used for the removal of gaseous radioiodine species from gas streams.  
1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.3 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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ASTM D5029-98(2020)(Test Method)
Standard Test Method for Water Solubles in Activated Carbon

SIGNIFICANCE AND USE
5.1 In certain applications, the ash, color, conductivity, or pH of the finished activated carbon product may be influenced by the quantity of water solubles it contains. This water solubles test provides a relative indication of the quantity of soluble materials that may be extracted from various activated carbons.
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1.1 This test method covers the determination of the water-soluble content of (unused) granular and powdered activated carbons. Water solubles are materials that can be extracted by distilled water under reflux conditions and are expressed as a percentage of dry carbon weight.  
1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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ASTM D6851-20(Test Method)
Standard Test Method for Determination of Contact pH with Activated Carbon

SIGNIFICANCE AND USE
4.1 The determination of contact pH can be used as a simple and fast measurement that can allow activated carbon producers and users to have a standard method for assessing the effect various carbons will have on the initial pH of the water in contact with the carbon. It has been determined that there is a bias between this method and Test Method D3838; they are not equivalent.
SCOPE
1.1 This method is to be used in the determination of the pH of water on initial contact with activated carbon. This test method is not meant as a replacement for Test Method D3838 and may give a different value.  
1.2 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.3 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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ASTM E200-23(Practice)
Standard Practice for Preparation, Standardization, and Storage of Standard and Reagent Solutions for Chemical Analysis

SIGNIFICANCE AND USE
4.1 The accuracy of many analytical measurements is dependent upon the manner in which the standard solutions are prepared and stored, and the accuracy with which they are standardized. Combining the methods recommended for the preparation and handling of such solutions into one practice eliminates the necessity for covering such details in all of the methods wherein the solutions are used.
SCOPE
1.1 This practice covers procedures for the preparation, standardization, and storage of the standard volumetric solutions and reagent testing solutions commonly used in chemical analysis.  
1.2 The information in this practice is arranged as follows:    
Sections  
Referenced Documents  
2  
Terminology  
3  
Significance and Use  
4  
Apparatus  
5  
Temperature effects  
6  
Measurements  
7  
Reagents  
8  
Concentration of solutions  
9  
Mixing of solutions  
10  
Storage of solutions  
11  
Preparation and standardization of solutions  
12  
Precision and Bias  
13  
Sodium hydroxide solution, 0.02 to 1.0 meq/mL (N)  
14 to 19  
Hydrochloric acid, 0.02 to 1.0 meq/mL (N)  
20 to 28  
Sulfuric acid, 0.02 to 1.0 meq/mL (N)  
29 to 33  
Hydrochloric acid, special 1 meq/mL (N)  
34 to 38  
Sulfuric acid, special 1 meq/mL (N)  
39 to 43  
Silver nitrate solution, 0.1 meq/mL (N)  
44 to 48  
Ammonium thiocyanate solution, 0.1 meq/mL (N)  
49 to 53  
Iodine solution, 0.1 meq/mL (N)  
54 to 58  
Sodium thiosulfate solution, 0.1 meq/mL (N)  
59 to 63  
Potassium permanganate solution, 0.1 meq/mL (N)  
64 to 68  
Potassium dichromate solution, 0.1 meq/mL(N)  
69 to 73  
Methanolic sodium hydroxide solution, 0.5 meq/mL (N)  
74 to 79  
Ceric sulfate solution, 0.1 meq/mL (N)  
80 to 84  
Acetous perchloric acid, 0.1 meq/mL (N)  
85 to 89  
Disodium ethylenediaminetetraacetate solution, 0.05 mol/L(M)  
90 to 94  
Standard ion solutions  
95  
Nonstandardized reagent solutions and indicator solutions  
96  
1.3 The values stated in SI units are to be regarded as standard. The values given in parentheses are for information only.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. Specific warning statements are given throughout this practice. Consult current OSHA regulations, suppliers’ Safety Data Sheets, and local regulations for all materials used in this specification.  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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