ASTM D346-04
(Practice)Standard Practice for Collection and Preparation of Coke Samples for Laboratory Analysis
Standard Practice for Collection and Preparation of Coke Samples for Laboratory Analysis
SCOPE
1.1 This practice covers procedures for the collection and reduction of samples of coke to be used for physical tests, chemical analyses, and the determination of total moisture.
1.2 The values given in SI units are to be regarded as the standard. The values given in parentheses are for information only.
This standard does not purport to address the safety concerns associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.
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Designation: D 346 – 04
Standard Practice for
Collection and Preparation of Coke Samples for Laboratory
1
Analysis
This standard is issued under the fixed designation D 346; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (e) indicates an editorial change since the last revision or reapproval.
INTRODUCTION
Coke, especially run of oven coke or foundry coke, or both, is a difficult material to sample. It is
imperative that every sample be collected and handled carefully and conscientiously and in strict
accordance with the standard procedure described herein.
Gross samples of not less than the quantities designated in this practice must be taken, whether the
coke to be sampled consists of a few tons or several hundred tons.
1. Scope 3. Significance and Use
1.1 This practice covers procedures for the collection and 3.1 This practice may be used to provide a representative
reduction of samples of coke to be used for physical tests, sample of the coke from which it is collected. Because of the
chemical analyses, and the determination of total moisture. variability of coke and the wide variety of sampling equipment,
1.2 The values given in SI units are to be regarded as the caution must be exercised in all stages of sampling, from
standard. The values given in parentheses are for information system specifications and equipment procurement to equip-
only. ment acceptance testing and actually taking the final sample.
1.3 This standard does not purport to address the safety 3.2 This practice also provides an analysis sample of coke
concerns associated with its use. It is the responsibility of the from the gross or divided sample. The analysis samples can be
user of this standard to establish appropriate safety and health used to determine the value of the coke represented, its ability
practices and determine the applicability of regulatory limita- to meet specifications, as well as for other purposes.
tions prior to use.
4. Place of Sampling
2. Referenced Documents
4.1 Sample coke while it is being loaded into or unloaded
2
2.1 ASTM Standards: from railroad cars, ships, barges, or trucks, or when discharged
D 167 Test Method for Apparent and True Specific Gravity from supply bins, grab buckets, belt conveyers, or other coke
and Porosity of Lump Coke conveying equipment. Sample close to the point of interest.
D 293 Test Method for the Sieve Analysis of Coke
5. Collection of Gross Sample
D 2013 Practice of Preparing Coal Samples for Analysis
5.1 Collect increments regularly, systematically, and with
D 2234/D 2234M Practice for Collection of a Gross Sample
of Coal such frequency, so that the entire quantity of coke sampled will
D 3038 Test Method for Drop Shatter Test for Coke be represented proportionately in the gross sample, and a gross
sample of the required amount will be collected. The standard
D 3302 Test Method for Total Moisture in Coal
D 3402 Test Method for Tumbler Test for Coke gross sample shall equal or exceed the quantities given in Table
1.
D 6883 Practice for Manual Sampling of Stationary Coal
from Railroad Cars, Barges, Trucks, or Stockpiles 5.1.1 The quantity of sample to be taken will depend on the
size of the coke being sampled and the amount of information
to be obtained from the sample.
1
This practice is under the jurisdiction of ASTM Committee D05 on Coal and
5.1.1.1 The size of the sieve analysis sample is governed by
Coke and is the direct responsibility of Subcommittee D05.23 on Sampling.
the homogeneity of the coke being sampled. The quantities
Current edition approved April 1, 2004. Published April 2004. Originally
given in Table 1 represent the minimum quantity to be
approved in 1932. Last previous edition approved in 1998 as D 346 – 90 (1998).
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or
collected. The sieve analysis sample will supply sufficient coke
contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
Standards volume information, refer to the standard’s Document Summary page on
the ASTM website.
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D346–04
TABLE 1 Minimum Gross Sample Weights of Coke, kg (lb)
Foundry Coke Furnace Coke
A
Usage Coke Breeze
Run of Oven Sized Run of Oven Sized
Sieve analysis (size consist) 364 (800) 227 (500) 227 (500) 182 (400) 45 (100)
Drop shatter test 182 (400) 159 (350) 136 (300) 91 (200) .
Tumbler test 68 (150) 45 (100) 57 (125) 57 (125) .
Apparent specific gravity 46 (100) 46 (100) 46 (100) 46 (100) 23 (50)
Coke moisture 46 (100) 46 (100) 46
...
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