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ASTM D6666-04(2009)

(Guide)

Standard Guide for Evaluation of Aqueous Polymer Quenchants

Standard Guide for Evaluation of Aqueous Polymer Quenchants

SIGNIFICANCE AND USE
The significance and use of each test method will depend on the system in use and the purpose of the test method listed under Section 7. Use the most recent editions of the test methods.
SCOPE
1.1 This guide provides information, without specific limits, for selecting standard test methods for testing aqueous polymer quenchants for initial qualification, determining quality, and the effect of aging.  
1.2 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory requirements prior to use.

General Information

Status
Historical
Publication Date
14-Apr-2009
ICS
75.120 - Hydraulic fluids
Technical Committee
D02 - Petroleum Products, Liquid Fuels, and Lubricants
Drafting Committee
D02.L0.06 - Non-Lubricating Process Fluids
Current Stage
Ref Project

Relations

Replaces
ASTM D6666-04 - Standard Guide for Evaluation of Aqueous Polymer Quenchants
Effective Date
15-Apr-2009
Replaced By
ASTM D6666-04(2014) - Standard Guide for Evaluation of Aqueous Polymer Quenchants
Effective Date
01-May-2014

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Standards Content (Sample)

NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
Designation: D6666 − 04(Reapproved 2009)
Standard Guide for
1
Evaluation of Aqueous Polymer Quenchants
This standard is issued under the fixed designation D6666; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope D3867 Test Methods for Nitrite-Nitrate in Water
D4327 Test Method for Anions in Water by Suppressed Ion
1.1 This guide provides information, without specific limits,
Chromatography
forselectingstandardtestmethodsfortestingaqueouspolymer
D5296 Test Method for Molecular Weight Averages and
quenchants for initial qualification, determining quality, and
Molecular Weight Distribution of Polystyrene by High
the effect of aging.
Performance Size-Exclusion Chromatography
1.2 This standard does not purport to address all of the
D6482 Test Method for Determination of Cooling Charac-
safety concerns, if any, associated with its use. It is the
teristics of Aqueous Polymer Quenchants by Cooling
responsibility of the user of this standard to establish appro-
Curve Analysis with Agitation (Tensi Method)
priate safety and health practices and determine the applica-
D6549 Test Method for Determination of Cooling Charac-
bility of regulatory requirements prior to use.
teristics of Quenchants by Cooling Curve Analysis with
Agitation (Drayton Unit)
2. Referenced Documents
E70 Test Method for pH of Aqueous Solutions With the
2
2.1 ASTM Standards:
Glass Electrode
D95 Test Method for Water in Petroleum Products and
E979 Practice for Evaluation of Antimicrobial Agents as
Bituminous Materials by Distillation
Preservatives for Invert Emulsion and Other Water Con-
D445 Test Method for Kinematic Viscosity of Transparent
taining Hydraulic Fluids
and Opaque Liquids (and Calculation of Dynamic Viscos-
E2275 Practice for Evaluating Water-Miscible Metalwork-
ity)
ing Fluid Bioresistance and Antimicrobial Pesticide Per-
D892 Test Method for Foaming Characteristics of Lubricat-
formance
ing Oils
D1744 Test Method for Determination of Water in Liquid
3. Terminology
Petroleum Products by Karl Fischer Reagent (Withdrawn
3
3.1 Definitions of Terms Specific to This Standard:
2000)
3.1.1 austenite, n—solidsolutionofoneormoreelementsin
D1747 Test Method for Refractive Index of Viscous Mate-
face-centered cubic iron (gamma iron) and unless otherwise
rials
4
designated, the solute is generally assumed to be carbon (1).
D1796 Test Method for Water and Sediment in Fuel Oils by
the Centrifuge Method (Laboratory Procedure)
3.1.2 austenitizing, n—forming austenite by heating a fer-
D2624 Test Methods for Electrical Conductivity ofAviation
rous alloy into the transformation range (partial austenitizing)
and Distillate Fuels
or above the transformation range (complete austenitizing).
D3519 Test Method for Foam in Aqueous Media (Blender
When used without qualification, the term implies complete
Test)
austenitizing (1).
D3601 Test Method for Foam In Aqueous Media (Bottle
3.1.3 aqueous polymer quenchant, n—a solution containing
Test)
water, and one or more water-soluble polymers including
poly(alkylene glycol), poly(vinyl pyrrolidone), poly(sodium
1
This guide is under the jurisdiction of ASTM Committee D02 on Petroleum
acrylate), and poly(ethyl oxazoline) (2, 3) and additives for
ProductsandLubricantsandisthedirectresponsibilityofSubcommitteeD02.L0.06
corrosion and foam control, if needed.
on Non-Lubricating Process Fluids.
Current edition approved April 15, 2009. Published July 2009. Originally
3.1.4 biodegradation, n—theprocessbywhichasubstrateis
approved in 2001. Last previous edition approved in 2004 as D6666 – 04. DOI:
converted by biological, usually microbiological, agents into
10.1520/D6666-04R09.
simple, environmentally acceptable derivatives. (4)
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or
contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
Standards volume information, refer to the standard’s Document Summary page on
the ASTM website.
4
3
The last approved version of this historical standard is referenced on The boldface numbers in parentheses refer to the list of references at the end of
www.astm.org. this standard.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
1

---------------------- Page: 1 ----------------------
D6666 − 04 (2009)
FIG. 1 Cooling Mechanisms of the Quenching Process
3.1.5 biodeterioration, n—loss of product quality and per- 3.1.13 quenchant medium, n—any liquid or gas, or mixture,
formance and could be regarded as the initial stages of usedtocontrolthecoolingofametaltofacilitatetheforma
...

This document is not anASTM standard and is intended only to provide the user of anASTM standard an indication of what changes have been made to the previous version. Because
it may not be technically possible to adequately depict all changes accurately, ASTM recommends that users consult prior editions as appropriate. In all cases only the current version
of the standard as published by ASTM is to be considered the official document.
An American National Standard
Designation:D6666–01a Designation: D 6666 – 04 (Reapproved 2009)
Standard Guide for
1
Evaluation of Aqueous Polymer Quenchants
This standard is issued under the fixed designation D 6666; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope
1.1 This guide provides information, without specific limits, for selecting standard test methods for testing aqueous polymer
quenchants for initial qualification, determining quality, and the effect of aging.
1.2 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility
of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory
requirements prior to use.
2. Referenced Documents
2
2.1 ASTM Standards:
D95 Test Method for Water in Petroleum Products and Bituminous Materials by Distillation
D 445 Test Method for Kinematic Viscosity of Transparent and Opaque Liquids (and the Calculation of Dynamic Viscosity)
D 892 Test Method for Foaming Characteristics of Lubricating Oils
3
D 1744 Standard Test Method for Determination of Water in Liquid Petroleum Products by Karl Fischer Reagent
D 1747 Test Method for Refractive Index of Viscous Materials
D 1796 Test Method for Water and Sediment in Fuel Oils by the Centrifuge Method (Laboratory Procedure)
D 2624 Test Methods for Electrical Conductivity of Aviation and Distillate Fuels
D 3519 Test Method for Foam in Aqueous Media (Blender Test)
D 3601 Test Method for Foam inIn Aqueous Media (Bottle Test)
D 3867 Test Methods for Nitrite-Nitrate in Water
4
D3946Test Method for Evaluating the Bacteria Resistance of Water-Dilutable Metalworking Fluids
D 4327 Test Method for Anions in Water by Chemically Suppressed Ion Chromatography
D 5296 Test Method for Molecular WeightAverages and Molecular Weight Distribution of Polystyrene by High- Performance
Size-Exclusion Chromatography
D 6482 Test Method for Determination of Cooling Characteristics ofAqueous Polymer Quenchants by Cooling CurveAnalysis
with Agitation (Tensi Method)
D 6549 Test Method for Determination of Cooling Characteristics of Quenchants by Cooling Curve Analysis with Agitation
(Drayton Unit)
E70 Test Method for pH of Aqueous Solutions With the Glass Electrode
E686Test Method for Evaluation of Antimicrobial Agents in Aqueous Metal Working Fluids
E 979 Test Method for Evaluation of Antimicrobial Agents as Preservatives for Invert Emulsion and Other Water Containing
9
Hydraulic Fluids Practice for Evaluation of Antimicrobial Agents as Preservatives for Invert Emulsion and Other Water
Containing Hydraulic Fluids
E 2275 Practice for Evaluating Water-Miscible Metalworking Fluid Bioresistance and Antimicrobial Pesticide Performance
3. Terminology
3.1 Definitions of Terms Specific to This Standard:
3.1.1 austenite, n—solid solution of one or more elements in face-centered cubic iron (gamma iron) and unless otherwise
1
This guide is under the jurisdiction of ASTM Committee D02 on Petroleum Products and Lubricants and is the direct responsibility of Subcommittee D02.L0.06 on
Nonlubricating Process Fluids.
CurrenteditionapprovedDec.10,2001.PublishedFebruary2002.OriginallypublishedasD6666-01.LastpreviouseditionD6666-01. onNon-LubricatingProcessFluids.
Current edition approved April 15, 2009. Published July 2009. Originally approved in 2001. Last previous edition approved in 2004 as D 6666 – 04.
2
For referencedASTM standards, visit theASTM website, www.astm.org, or contactASTM Customer Service at service@astm.org. For Annual Book of ASTM Standards
, Vol 05.01.volume information, refer to the standard’s Document Summary page on the ASTM website.
3
Discontinued; see 1999 Annual Book of ASTM Standards , Vol 05.01.
3
Withdrawn.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, United States.
1

---------------------- Page: 1 ----------------------
D6666–04 (2009)
4
designated, the solute is generally assumed to be carbon (1).
3.1.2 austenitizing, n—formingaustenitebyheatingaferrousalloyintothetransformationrange(partialaustenitizing)orabove
the transformation range (complete austenitizing). When used without qualification, the term implies complete austenitizing (1).
3.1.3 aqueous polymer quenchant
...

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ASTM D7646-23(Test Method)
Standard Test Method for Determination of Cooling Characteristics of Aqueous Polymer Quenchants for Aluminum Alloys by Cooling Curve Analysis

SIGNIFICANCE AND USE
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SCOPE
1.1 This test method covers a constant volume vane pump test procedure operated at 1200 r/min and 13.8 MPa.  
1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.2.1 Exception—There are no SI equivalents for the inch fasteners and inch O-rings that are used in the apparatus in this test method.  
1.2.2 Exception—In some cases English pressure values are given in parentheses as a safety measure.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
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Standard Practice for Obtaining LPG Samples Using a Floating Piston Cylinder

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5.1 This practice allows the collection of a representative sample of LPG that may contain trace volatile dissolved components such as methane, ethane, and nitrogen. Sampling by Practice D1265 can result in a small, but predictable, loss of these lighter components. Practice D1265 is suitable for collecting samples for routine specification testing, as the small loss of light components is not significant under Specification D1835 specification requirements. Practice D3700 is recommended whenever highly accurate determination of light components is required. For example, compositions determined on samples collected according to Practice D3700 may be used to establish the product value of NGL mixtures (see Appendix X1).
SCOPE
1.1 This practice covers the equipment and procedures for obtaining a representative sample of liquefied petroleum gas (LPG), such as specified in ASTM Specification D1835, GPA 2140, and comparable international standards. It may also be used for other natural gas liquid (NGL) products that are normally single phase (for example, NGL mix, field butane, and so forth), defined in other industry specifications or contractual agreements, and for volatile (higher vapor pressure) crude oils.
Note 1: Some floating piston cylinders have such tight piston seals that the vapor pressure of some high vapor pressure crude oils may not be sufficient to allow sampling without a handle to move the piston. An alternative sampling practice for UN Class 3 liquids (under 300 kPa at 52 °C) is Practice D8009, which utilizes a Manual Piston Cylinder (MPC) sampler.  
1.2 This practice is not intended for non-specification products that contain significant quantities of undissolved gases (N2, CO2), free water or other separated phases, such as raw or unprocessed gas/liquids mixtures and related materials. The same equipment can be used for these purposes, but additional precautions are generally needed to obtain representative samples of multi-phase products (see Appendix X1).  
1.3 This practice includes recommendations for the location of a sample point in a line or vessel. It is the responsibility of the user to ensure that the sampling point is located so as to obtain a representative sample.  
1.4 The values stated in SI units are to be regarded as standard.  
1.4.1 Exception—The values given in parentheses are for information only.  
1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices, and determine the applicability of regulatory limitations prior to use.  
1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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