ASTM D3169-89(2001)
(Specification)Standard Specification for Refined Sunflower Oil (Withdrawn 2007)
Standard Specification for Refined Sunflower Oil (Withdrawn 2007)
SCOPE
1.1 This specification covers once-refined sunflower oil, technical grade, suitable for use in protective coatings.
WITHDRAWN RATIONALE
This specification covers once-refined sunflower oil, technical grade, suitable for use in protective coatings.
Formerly under the jurisdiction of Committee D01 on Paint and Related Coatings, Materials, and Applications, this specification was withdrawn in February 2007. This standard is being withdrawn without replacement due to its limited use by industry.
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NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
Designation: D 3169 – 89 (Reapproved 2001)
Standard Specification for
Refined Sunflower Oil
This standard is issued under the fixed designation D 3169; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (e) indicates an editorial change since the last revision or reapproval.
1. Scope D 1967 Test Method for Color After Heating of Drying
Oils
1.1 This specification covers once-refined sunflower oil,
D 2090 Test Method for Clarity and Cleanness of Paint and
technical grade, suitable for use in protective coatings.
Ink Liquids
2. Referenced Documents
3. Properties
2.1 ASTM Standards:
2 3.1 Sunflower oil shall be obtained solely from sunflower
D 555 Guide for Testing Drying Oils
seed and shall be suitably processed to conform to the
D 1466 Test Method for Sampling Liquid Oils and Fatty
requirements given in Table 1.
Acids Commonly Used In Paints, Varnishes, and Related
Materials
TABLE 1 Properties of Once-Refined Sunflower Oil
D 1544 Test Method for Color of Transparent Liquids
ASTM Test
(Gardner Color Scale)
Property Requirement
Method
D 1639 Test Method for Acid Value of Organic Coating
2 Specific gravity 25/25°C 0.918 to 0.921 D 1963
Materials
Acid value 0.3 max D 1639
D 1952 Test Method for Quantitative Determination of
Saponification value 188 to 194 D 1962
Unsaponifiable matter, % 1.5 max D 1965
Break in Drying Oils
Iodine value (Wijs) 134 to 144 D 1959
D 1959 Test Method for Iodine Value of Drying Oils and
Loss on heating at 105°C, % 0.2 max D 1960
Fatty Acids
Color 7 max D 1544
Color after heating 2 max D 1967
D 1960 Test Method for Loss on Heating of Drying Oils
Quantitative break, % 0.02 max D 1952
D 1962 Test Method for Saponification Value of Drying
Clarity clear and transparent at 25°C D 2090
Oils, Fatty Acids, and Polymerized Fatty Acids
D 1963 Test Method for Specific Gravity of Drying Oils,
Varnishes, Resins, and Related Materials at 25/25°C
4. Sampling
D 1965 Test Method for Unsaponifiable Matter in Drying
4.1 Sample in accordanc
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4.4 This practice addresses neither evaluation and scaling techniques, nor the sampling, handling, and preparing of solid fats.
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Sampling
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Appearance
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Color
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Specific Gravity
7
Refractive Index
8
Composition
9
Moisture
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1.2.2 The two methods for determining the amount of the individual fatty acids and rosin acids are the “internal standard” method, which yields absolute values, and the “area percent” method, which yields relative values.
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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1.3 The techniques used in this practice are applicable to oils (liquid at room temperature) and liquified fats (solid at room temperature).
1.4 The values in SI units are to be regarded as the standard.
1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
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4.1 This test method is useful when oils and fats are suspected as an ignition source or a fuel source in a fire.
4.1.1 The identification of oil and fat residues in samples from a fire scene can support the field investigator’s opinion regarding the origin and cause of the fire.
4.1.2 The positive identification of fatty acid(s) does not necessarily mean that the fire was caused by self heating.
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4.3 This test method is a sensitive separation technique and can detect quantities as small as 3 µL of oil or fat residue in an extract from a debris sample.
4.4 This test method shall be performed after all required traditional testing for ignitable liquid residues is completed.
4.5 This test method extracts liquids and residues from porous and nonporous materials of various sizes.
4.6 This test method can be hampered by coincident extraction of interfering compounds present in the fire debris samples.
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1.1 This test method covers the extraction, derivatization, and identification of fatty acids indicative of vegetable oils and fats in fire debris and liquid samples. This procedure will also extract animal oils and fats, as these are similar in chemical composition to vegetable oils and fats. Herein, the phrase “oils and fats” will be used to refer to both animal and vegetable derived oils and fats.
1.2 This test method is suitable for successfully extracting oil and fat residues having 8 to 24 carbon atoms.
1.3 The identification of a specific type of oil (for example, olive, corn, linseed) requires a quantitative analysis of the fatty acid esters and is beyond the scope of this test method.
1.4 This test method cannot replace the requisite knowledge, skills, or abilities acquired through appropriate education, training, and experience and should be used in conjunction with sound professional judgment.
1.5 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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ABSTRACT
This specification covers SEBS (styrene-ethylenebutylene-styrene)-modified mopping asphalt intended for use in built-up roof construction, construction of some modified bitumen systems, construction of bituminous vapor retarder systems, and for adhering insulation boards used in various types of roofing systems. This specification is intended as a material specification and issues regarding the suitability of specific roof constructions or application techniques are beyond its scope. The specified tests and property values are intended to establish minimum properties. In place system design criteria or performance attributes are factors beyond the scope of this specification. The base asphalt shall be prepared from crude petroleum and the SEBS-modified asphalt shall incorporate sufficient SEBS as the primary polymeric modifier. The SEBS modified asphalt shall be homogeneous and free of water and shall conform to the prescribed physical properties including (1) softening point before and after heat exposure, (2) softening point change, (3) flash point, (4) penetration before and after heat exposure, (5) penetration change, (6) solubility in trichloroethylene, (7) tensile elongation, (8) elastic recovery, and (9) low temperature flexibility. The sampling and test methods to determine compliance with the specified physical properties, as well as the evaluation for stability during heat exposure are detailed.
SCOPE
1.1 This specification covers SEBS (styrene-ethylene-butylene-styrene)-modified asphalt intended for use in built-up roof construction, construction of some modified bitumen systems, construction of bituminous vapor retarder systems, and for adhering insulation boards used in various types of roof systems.
1.2 This specification is intended as a material specification. Issues regarding the suitability of specific roof constructions or application techniques are beyond its scope.
1.3 The specified tests and property values used to characterize SEBS-modified asphalt are intended to establish minimum properties. In-place system design criteria or performance attributes are factors beyond the scope of this specification.
1.4 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the two systems may result in nonconformance with the standard.
1.5 This standard does not purport to address the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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