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ASTM D5594-18

(Test Method)

Standard Test Method for Determination of the Vinyl Acetate Content of Ethylene-Vinyl Acetate (EVA) Copolymers by Fourier Transform Infrared Spectroscopy (FT-IR)

Standard Test Method for Determination of the Vinyl Acetate Content of Ethylene-Vinyl Acetate (EVA) Copolymers by Fourier Transform Infrared Spectroscopy (FT-IR)

SIGNIFICANCE AND USE
5.1 Properties of EVA copolymers are affected by the amount of vinyl acetate incorporated in the copolymer: This test method provides a means to determine the vinyl acetate level in copolymer samples.  
5.2 Before proceeding with this test method, reference should be made to the specification of the material being tested. Any test specimen preparation, conditioning, dimensions, or testing parameters, or a combination thereof, covered in the materials specification shall take precedence over those mentioned in this test method. If there are no material specifications, then the default conditions apply.
SCOPE
1.1 This test method covers infrared procedures for determining the vinyl acetate content of EVA copolymers using pressed films (Procedure A) or molded plaques (Procedure B) and internal corrections for sample thickness.  
1.2 This test method is applicable to the analysis of EVA copolymers containing 0.5 to 55 % vinyl acetate except as specified in 1.3.  
1.3 Talc interferes with the 1020 cm−1 vinyl acetate band. Resins containing  
1.4 The values stated in SI units are to be regarded as the standard. The values given in parentheses are provided for information purposes only.  
1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. Specific precautionary statements are given in Section 8.
Note 1: This test method is not equivalent to ISO 8985.  
1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

General Information

Status
Historical
Publication Date
31-Jul-2018
ICS
83.080.20 - Thermoplastic materials
Technical Committee
D20 - Plastics
Drafting Committee
D20.70 - Analytical Methods
Current Stage
Ref Project

Relations

Replaces
ASTM D5594-98(2012) - Standard Test Method for Determination of the Vinyl Acetate Content of Ethylene-Vinyl Acetate (EVA) Copolymers by Fourier Transform Infrared Spectroscopy (FT-IR)
Effective Date
01-Aug-2018
Referred By
ASTM D4439-23b - Standard Terminology for Geosynthetics
Effective Date
01-Aug-2018
Referred By
ASTM D5576-00(2021)e1 - Standard Practice for Determination of Structural Features in Polyolefins and Polyolefin Copolymers by Infrared Spectrophotometry (FT-IR)
Effective Date
01-Aug-2018

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ASTM D5594-18 - Standard Test Method for Determination of the Vinyl Acetate Content of Ethylene-Vinyl Acetate (EVA) Copolymers by Fourier Transform Infrared Spectroscopy (FT-IR)ASTM D5594-18 - Standard Test Method for Determination of the Vinyl Acetate Content of Ethylene-Vinyl Acetate (EVA) Copolymers by Fourier Transform Infrared Spectroscopy (FT-IR)
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ASTM D5594-18 - Standard Test Method for Determination of the Vinyl Acetate Content of Ethylene-Vinyl Acetate (EVA) Copolymers by Fourier Transform Infrared Spectroscopy (FT-IR)
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REDLINE ASTM D5594-18 - Standard Test Method for Determination of the Vinyl Acetate Content of Ethylene-Vinyl Acetate (EVA) Copolymers by Fourier Transform Infrared Spectroscopy (FT-IR)REDLINE ASTM D5594-18 - Standard Test Method for Determination of the Vinyl Acetate Content of Ethylene-Vinyl Acetate (EVA) Copolymers by Fourier Transform Infrared Spectroscopy (FT-IR)
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Standards Content (Sample)

NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
Designation: D5594 − 18
Standard Test Method for
Determination of the Vinyl Acetate Content of Ethylene-Vinyl
Acetate (EVA) Copolymers by Fourier Transform Infrared
1
Spectroscopy (FT-IR)
This standard is issued under the fixed designation D5594; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision.Anumber in parentheses indicates the year of last reapproval.A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope E168Practices for General Techniques of Infrared Quanti-
tative Analysis
1.1 This test method covers infrared procedures for deter-
E177Practice for Use of the Terms Precision and Bias in
mining the vinyl acetate content of EVA copolymers using
ASTM Test Methods
pressed films (Procedure A) or molded plaques (Procedure B)
E691Practice for Conducting an Interlaboratory Study to
and internal corrections for sample thickness.
Determine the Precision of a Test Method
1.2 This test method is applicable to the analysis of EVA
IEEE/ASTM SI-10Use of the International System of Units
copolymers containing 0.5 to 55% vinyl acetate except as
(SI): The Modem Metric System
specified in 1.3.
E691Practice for Conducting an Interlaboratory Study to
−1
Determine the Precision of a Test Method
1.3 Talc interferes with the 1020 cm vinyl acetate band.
Resins containing <5% vinyl acetate and talc are excluded
2.2 ISO Standard:
from the scope of this test method.
ISO 8985 Plastics—Ethylene/Vinyl Acetate Copolymer
3,4
Thermoplastics—Determination of VinylAcetate
1.4 The values stated in SI units are to be regarded as the
standard. The values given in parentheses are provided for
3. Terminology
information purposes only.
3.1 Definitions:
1.5 This standard does not purport to address all of the
3.1.1 Units, symbols, and abbreviations used in this test
safety concerns, if any, associated with its use. It is the
method appear in Terminology E131 or IEEE/ASTM SI-10.
responsibility of the user of this standard to establish appro-
3.2 Abbreviations:
priate safety and health practices and determine the applica-
3.2.1 EVA—ethylene-vinyl acetate copolymer.
bility of regulatory limitations prior to use. Specific precau-
3.2.2 PTFE—tetrafluorethylene polymer.
tionary statements are given in Section 8.
3.2.3 FT-IR—Fourier transform infrared.
NOTE 1—This test method is not equivalent to ISO 8985.
1.6 This international standard was developed in accor-
4. Summary of Test Method
dance with internationally recognized principles on standard-
4.1 The vinyl acetate content is measured using infrared
ization established in the Decision on Principles for the
−1
absorptionbandat1020cm (0.5to5%vinylacetate)or609
Development of International Standards, Guides and Recom-
−1
cm (5 to 55% vinyl acetate).
mendations issued by the World Trade Organization Technical
Barriers to Trade (TBT) Committee.
4.2 Sample thickness is measured internally using an ethyl-
−1
ene infrared absorption band at 720 cm (28 to 55% vinyl
2. Referenced Documents
−1 −1
acetate), 2020 cm (0.5 to 28% vinyl acetate), or 4250 cm
2
2.1 ASTM Standards:
(5 to 28% vinyl acetate).
E131Terminology Relating to Molecular Spectroscopy
4.3 Regression analysis is performed on vinyl acetate/
ethylene ratios versus known vinyl acetate contents for EVA
1
ThistestmethodisunderthejurisdictionofASTMCommitteeD20onPlastics
and is the direct responsibility of Subcommittee D20.70 on Analytical Methods.
Current edition approved Aug. 1, 2018. Published August 2018. Originally
3
approved in 1994. Last previous edition approved in 2012 as D5594-98 (2012). Available fromAmerican National Standards Institute (ANSI), 25 W. 43rd St.,
DOI: 10.1520/D5594-18. 4th Floor, New York, NY 10036, http://www.ansi.org.
2 4
For referenced ASTM standards, visit the ASTM website, www.astm.org, or Nicolet20S×B,availablefromNicoletInstrumentCorp.,AnalyticalDivision,
contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM 5225 Verona Rd., Madison, WI 53711-4495, and Perkin Elmer 1760, a registered
Standards volume information, refer to the standard’s Document Summary page on trademark of Perkin-Elmer Corp., 761 Main Ave., Norwalk, CT 06859-0156, or
the ASTM website. equivalents, have been found suitable for this purpose.
*A Summary of Changes section appears at the end of this standard
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
1

---------------------- Page: 1 ----------------------
D5594 − 18
copolymer standards. The resulting equation is used to calcu- dureA),andglovesshouldbewornwhenplaquesareprepared
late the vinyl acetate content for subsequent EVA copolymer using a heated press (Sample Preparation Procedure B).
samples.
8.2 Care also
...

This document is not an ASTM standard and is intended only to provide the user of an ASTM standard an indication of what changes have been made to the previous version. Because
it may not be technically possible to adequately depict all changes accurately, ASTM recommends that users consult prior editions as appropriate. In all cases only the current version
of the standard as published by ASTM is to be considered the official document.
Designation: D5594 − 98 (Reapproved 2012) D5594 − 18
Standard Test Method for
Determination of the Vinyl Acetate Content of Ethylene-Vinyl
Acetate (EVA) Copolymers by Fourier Transform Infrared
1
Spectroscopy (FT-IR)
This standard is issued under the fixed designation D5594; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope
1.1 This test method covers infrared procedures for determining the vinyl acetate content of EVA copolymers using pressed
films (Procedure A) or molded plaques (Procedure B) and internal corrections for sample thickness.
1.2 This test method is applicable to the analysis of EVA copolymers containing 0.5 to 55 % vinyl acetate except as specified
in 1.3.
−1
1.3 Talc interferes with the 1020 cm vinyl acetate band. Resins containing <5 % vinyl acetate and talc are excluded from the
scope of this test method.
1.4 The values stated in SI units are to be regarded as the standard. The values given in bracketsparentheses are provided for
information purposes only.
1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility
of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory
limitations prior to use. Specific precautionary statements are given in Section 8.
NOTE 1—This test method is not equivalent to ISO 8985.
1.6 This international standard was developed in accordance with internationally recognized principles on standardization
established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued
by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
2. Referenced Documents
2
2.1 ASTM Standards:
E131 Terminology Relating to Molecular Spectroscopy
E168 Practices for General Techniques of Infrared Quantitative Analysis
E177 Practice for Use of the Terms Precision and Bias in ASTM Test Methods
E691 Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method
IEEE/ASTM SI-10 Use of the International System of Units (SI): The Modem Metric System
E691 Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method
2.2 ISO Standard:
3 ,4
ISO 8985 Plastics—Ethylene/Vinyl Acetate Copolymer Thermoplastics—Determination of Vinyl Acetate
3. Terminology
3.1 Definitions:
3.1.1 Units, symbols, and abbreviations used in this test method appear in Terminology E131 or IEEE/ASTM SI-10.
3.2 Abbreviations:
1
This test method is under the jurisdiction of ASTM Committee D20 on Plastics and is the direct responsibility of Subcommittee D20.70 on Analytical Methods.
Current edition approved April 1, 2012Aug. 1, 2018. Published June 2012August 2018. Originally approved in 1994. Last previous edition approved in 20042012 as
D5594 - 98 (2004).(2012). DOI: 10.1520/D5594-98R12.10.1520/D5594-18.
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM Standards
volume information, refer to the standard’s Document Summary page on the ASTM website.
3
Available from American National Standards Institute (ANSI), 25 W. 43rd St., 4th Floor, New York, NY 10036, http://www.ansi.org.
4
Nicolet 20 S × B, available from Nicolet Instrument Corp., Analytical Division, 5225 Verona Rd., Madison, WI 53711-4495, and Perkin Elmer 1760, a registered
trademark of Perkin-Elmer Corp., 761 Main Ave., Norwalk, CT 06859-0156, or equivalents, have been found suitable for this purpose.
*A Summary of Changes section appears at the end of this standard
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
1

---------------------- Page: 1 ----------------------
D5594 − 18
3.2.1 EVA—ethylene-vinyl acetate copolymer.
3.2.2 PTFE—tetrafluorethylene polymer.
3.2.3 FT-IR—Fourier transform infrared.
4. Summary of Test Method
−1 −1
4.1 The vinyl acetate content is measured using infrared absorption band at 1020 cm (0.5 to 5 % vinyl acetate) or 609 cm
(5 to 55 % vinyl acetate).
−1
4.2 Sample thickness is measured internally using an ethylene infrared absorption band at 720 cm (28 to 55 % vinyl acetate),
−1 −1
2020 cm (0.5 to 28 % vinyl acetate),
...

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SCOPE
1.1 This test method provides a means to assess the drop impact resistance of water-filled, blow-molded thermoplastic containers, which is a summation of the effects of material, manufacturing conditions, container design, and perhaps other factors.  
1.2 Two procedures are provided as follows:  
1.2.1 Procedure A, Static Drop Height Method—This procedure is particularly useful for quality control since it is quick.  
1.2.2 Procedure B, Bruceton Staircase Method—This procedure is used to determine the mean failure height and the standard deviation of the distribution.  
1.3 The values stated in SI units are to be regarded as standard. The inch-pound units given in parentheses are for information only.  
Note 1: There is no known ISO equivalent to this standard.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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ASTM
ASTM D3030-23(Test Method)
Standard Test Method for Volatile Matter (Including Water) of Vinyl Chloride Resins

SIGNIFICANCE AND USE
5.1 The quantity of volatile components in a vinyl chloride resin can be established by this test method. This test method does not identify the components.
SCOPE
1.1 This test method covers the quantitative determination of the volatile matter (including water) present in vinyl chloride resins.  
1.2 The values stated in SI units are to be regarded as standard.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
Note 1: This test method is identical ISO 1269.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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ASTM
ASTM D3275-18(2023)(Classification)
Standard Classification System for E-CTFE-Fluoroplastic Molding, Extrusion, and Coating Materials

ABSTRACT
This classification system covers melt processible molding, extrusion, and coating materials of ethylene-chlorotrifluoroethylene (E-CTFE) fluoroplastics. The resin is a copolymer of ethylene and chlorotrifluoroethylene. The classification of ECTFE materials into groups in accordance with their physical appearance, and further into classes based on melt flow rate, is provided. The test specimens shall be subjected to tests to determine their melt flow rate, melting endotherm peak, specific gravity, tensile property, dielectric constant and dissipation factor, and oxygen index.
SCOPE
1.1 This classification system covers melt processible molding, extrusion, and coating materials of ethylene-chlorotrifluoroethylene (E-CTFE) fluoroplastics. The resin is a copolymer of ethylene and chlorotrifluoroethylene containing approximately 80 weight % of chlorotrifluoroethylene.  
1.2 The values stated in SI units, as detailed in IEEE/ASTM SI-10, are to be regarded as standard.  
1.3 The following precautionary statement pertains only to the test methods portion, Section 11 of this classification system. This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
Note 1: Although this classification system and ISO 20568-1 and ISO 20568-2 differ in approach or detail, data obtained using either are technically equivalent.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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ASTM
ASTM D4878-23(Test Method)
Standard Test Methods for Polyurethane Raw Materials: Determination of Viscosity of Polyols

SIGNIFICANCE AND USE
4.1 These test methods are suitable for research or as quality control or specification tests.  
4.2 Viscosity measures the resistance of a fluid to uniformly continuous flow without turbulence or other forces.
SCOPE
1.1 These test methods (A and B) determine the viscosity of polyols in the range from 10 to 100 000 mPa·s(cP) at 25°C. Test Method A is a rotational procedure for determining dynamic viscosity. Test Method B is a general procedure for kinematic viscosity of transparent polyols. (See Note 1.)  
1.2 The values stated in SI units are to be regarded as the standard. Other equivalent units are provided because of current common usage.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
Note 1: Test Method A is equivalent to ISO 3219. Test Method B is equivalent to ISO 3104.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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