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ASTM D4277-83(1998)

(Guide)

Standard Guide for Testing Amino Resins (Withdrawn 2007)

Standard Guide for Testing Amino Resins (Withdrawn 2007)

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1.1 This guide covers test methods suitable for testing heat-reactive nitrogen resins, particularly urea-formaldehyde and melamine-formaldehyde resins. The test methods used are listed in Table 1.
WITHDRAWN RATIONALE
This guide covers test methods suitable for testing heat-reactive nitrogen resins, particularly urea-formaldehyde and melamine-formaldehyde resins. The test methods used are D 1013, D 1198, D 1209, D 1259, D 1475, D 1545, D 1639, and D 3278.
Formerly under the jurisdiction of Committee D01 on Paint and Related Coatings, Materials, and Applications, this guide was withdrawn in March 2007 in accordance with section 10.5.3.1 of the Regulations Governing ASTM Technical Committees, which requires that standards shall be updated by the end of the eighth year since the last approval date.

General Information

Status
Withdrawn
Publication Date
31-Dec-1992
Withdrawal Date
20-Mar-2007
ICS
83.080.10 - Thermosetting materials
Technical Committee
D01 - Paint and Related Coatings, Materials, and Applications
Drafting Committee
D01.33 - Polymers and Resins
Current Stage
Ref Project

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ASTM D4277-83(1998) - Standard Guide for Testing Amino Resins (Withdrawn 2007)ASTM D4277-83(1998) - Standard Guide for Testing Amino Resins (Withdrawn 2007)
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ASTM D4277-83(1998) - Standard Guide for Testing Amino Resins (Withdrawn 2007)
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NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
Designation:D4277–83 (Reapproved 1998)
Standard Guide for
Testing Amino Resins
This standard is issued under the fixed designation D 4277; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (e) indicates an editorial change since the last revision or reapproval.
TABLE 1 Methods for Testing Nitrogen Resins
1. Scope
Test Method Section ASTM Designation
1.1 This guide covers test methods suitable for testing
Total nitrogen in resins and plastics 5 D 1013
heat-reactive nitrogen resins, particularly urea-formaldehyde
Solvent tolerance of amino resins 6 D 1198
and melamine-formaldehyde resins. The test methods used are
Color of clear liquids 7 D 1209
listed in Table 1.
Nonvolatile content resin solutions 8 D 1259
Density 9 D 1475
Viscosity 10 D 1545
2. Referenced Documents
Acid value 11 D 1639
2.1 ASTM Standards:
Flash point 12 D 3278
D 883 Terminology Relating to Plastics
D 1013 Test Method for Determining Total Nitrogen in
4. Significance and Use
Resins and Plastics
D 1198 Test Method for Solvent Tolerance of Amine Res-
4.1 This guide summarizes the currently available ASTM
ins
test methods useful for testing amino resins. These test
D 1209 Test Method for Color of Clear Liquids (Platinum-
methods may be used by producers and users to characterize a
Cobalt Scale)
variety of properties of nitrogen resins related to their quality
D 1259 Test Methods for Nonvolatile Content of Resin
and safe use.
Solutions
5. Total Nitrogen
D 1475 Test Method for Density of Paint, Varnish, Lacquer,
and Related Products
5.1 Test Method D 1013 is a standard Kjeldahl procedure
D 1545 Test Method for Viscosity of Transparent Liquids for nitrogen determination, directly applicable to amino resins
by Bubble Time Method
and solutions thereof.
D 1639 Test Method for Acid Value of Organic Coating
6. Solvent Tolerance
Materials
D 3278 Test Methods for Flash Point of Liquids by Small
6.1 Theamountofhydrocarbonthatanaminoresintolerates
Scale Closed-Cup Apparatus is measured in accordance with Test Method D 1198. The end
point of this titration, a defined degree of turbidity, is sensitive
3. Terminology
to both the alkylation and degree of polymerization of the
3.1 Definition—The following definition is taken from Ter-
amino resin.
minology D 883:
7. Color
3.1.1 amino resin—a resin made by polycondensation of a
compound containing amino groups such as urea or melamine 7.1 The color of solutions of amino resins can be measured
with an aldehyde, such as formaldehyde, or an aldehyde- using the platinum-cobalt scale according to the procedure in
yielding material. Test Method D 1209.
8. Nonvolatile Content
...

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