Standard Performance Specification for Coal-Tar Pitch Emulsion Pavement Sealer Mix Formulations Containing Mineral Aggregates and Optional Polymeric Admixtures

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1.1 This performance specification covers mixtures of emulsified coal-tar pitch (mineral colloid type), mineral aggregates, and optional polymeric admixtures that are used as a weather-protective and straight aliphatic hydrocarbon resistant coatings over bituminous pavements of airports, parking areas, and driveways.  
1.2 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the two systems may result in nonconformance with the standard.  
1.3 The following safety hazards statement applies only to the test method portion, Section 6, of this specification: This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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ASTM D4866/D4866M-88(2023) - Standard Performance Specification for Coal-Tar Pitch Emulsion Pavement Sealer Mix Formulations Containing Mineral Aggregates and Optional Polymeric Admixtures
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This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the
Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
Designation: D4866/D4866M −88 (Reapproved 2023)
Standard Performance Specification for
Coal-Tar Pitch Emulsion Pavement Sealer Mix Formulations
Containing Mineral Aggregates and Optional Polymeric
Admixtures
This standard is issued under the fixed designation D4866/D4866M; the number immediately following the designation indicates the
year of original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last
reapproval. A superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope Emulsions (Withdrawn 1998)
D2939 Test Methods for Emulsified Bitumens Used as
1.1 Thisperformancespecificationcoversmixturesofemul-
Protective Coatings (Withdrawn 2012)
sified coal-tar pitch (mineral colloid type), mineral aggregates,
D3699 Specification for Kerosine
and optional polymeric admixtures that are used as a weather-
D5727/D5727M Specification for Emulsified Refined Coal
protective and straight aliphatic hydrocarbon resistant coatings
Tar (Mineral Colloid Type)
over bituminous pavements of airports, parking areas, and
driveways.
3. Materials
1.2 The values stated in either SI units or inch-pound units
3.1 Ratios of component materials that make up the mixture
are to be regarded separately as standard. The values stated in
to be tested, as well as detailed specifications for the mineral
each system may not be exact equivalents; therefore, each
aggregate and optional polymeric admixture shall be as agreed
system shall be used independently of the other. Combining
upon between the purchaser and the seller.
values from the two systems may result in nonconformance
3.2 The base coal-tar emulsion shall meet the requirements
with the standard.
of Specification D5727/D5727M.
1.3 The following safety hazards statement applies only to
3.3 The mineral aggregate shall be either a natural or
the test method portion, Section 6, of this specification: This
manufactured product composed of clean, hard, durable, un-
standarddoesnotpurporttoaddressallofthesafetyconcerns,
coated particles, free from dirt, organic matter, and other
ifany,associatedwithitsuse.Itistheresponsibilityoftheuser
objectionable substances.
of this standard to establish appropriate safety, health, and
environmental practices and determine the applicability of
3.4 The optional polymeric admixture shall be any polymer
regulatory limitations prior to use.
or mixtures thereof, with added compounding ingredients of
1.4 This international standard was developed in accor-
such nature and quality that will allow the admixture to be
dance with internationally recognized principles on standard-
compatible with and enhance the performance of mineral
ization established in the Decision on Principles for the
aggregate modified coal-tar emulsion pavement sealers.
Development of International Standards, Guides and Recom-
3.5 The water used in mixing shall be potable and free from
mendations issued by the World Trade Organization Technical
harmful soluble salts. The temperature of the water shall be at
Barriers to Trade (TBT) Committee.
least 10 °C [50 °F].
2. Referenced Documents
4. Physical Requirements
2.1 ASTM Standards:
4.1 The mixture as applied shall be of uniform consistency
D466 Test Methods for Films Deposited From Bituminous
and suitable for application to properly prepared or primed
2 2
surfaces at a rate of 0.4 to 1.0 L/m [1.0 to 2.5 gal/100 ft ]
without appreciable drainage on inclines up to 0.8 %
This specification is under the jurisdiction of ASTM Committee D08 on [0.1 in.⁄ft].
Roofing and Waterproofing and is the direct responsibility of Subcommittee D08.09
NOTE 1—Pavement and ambient temperature should be not less than
on Liquid Applied Coatings for Roofing and Asphaltic Concrete Pavement.
7 °C [45 °F] at the time of application and for at least 12 h thereafter, with
Current edition approved Jan. 1, 2023. Published January 2023. Originally
approved in 1988. Last previous edition approved in 2017 as D4866/D4866M – 88 no precipitation of rain, snow, and so forth, until the emulsion has dried.
(2017). DOI: 10.1520/D4866_D4866M-88R23. NOTE 2—When these materials are applied in commercial quantities,
For referenced ASTM standards, visit the ASTM website, www.astm.org, or
contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
Standards volume information, refer to the standard’s Document Summary page on The last approved version of this historical standard is referenced on
the ASTM website. www.astm.org.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
D4866/D4866M − 88 (2023)
the purchaser or inspector should observe the mixing to ensure that after
6.4.2 Cureeachcoatfor96hinagitatedairat25 61 °C[77
each step no coagulation or separation of the ingredients occurs and that
6 2 °F] and at 50 6 10 % relative humidity.
the mix has a good application consistency. When possible, a small batch
6.4.3 After curing, affix metal ring to surface of coating.
should be mixed and observed prior to the onset of major work.
Because of the textured surface of the coating, the ring must be
4.2 The mixture shall conform to the physical properties
sealed to the dry second coat with a silicone rubber sealant.
prescribed in Table 1.
6.4.4 Fill the metal ring with kerosine. The kerosine shall
comply with Specification D3699. Expose the coating to
5. Sampling
kerosine for 24 h before evaluating. Remove the kerosine from
5.1 Sample in accordance with Test Methods D2939.
the ring and blot dry and immediately examine the film for
softness and loss of adhesion. Immediately after this film
6. Test Methods
examination, break the tile in half exposing that part of the tile
6.1 Redispersibility—The product (coal
...

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