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ASTM C227-10

(Test Method)

Standard Test Method for Potential Alkali Reactivity of Cement-Aggregate Combinations (Mortar-Bar Method) (Withdrawn 2018)

Standard Test Method for Potential Alkali Reactivity of Cement-Aggregate Combinations (Mortar-Bar Method) (Withdrawn 2018)

SIGNIFICANCE AND USE
Data correlating the results of tests performed using this test method with performance of cement-aggregate combinations in concrete in service, results of petrographic examination of aggregates (Guide C295), and results of tests for potential reactivity of aggregates by chemical methods have been published in Test Method C289 and should be consulted in connection with the use of results of tests performed using this test method as the basis for conclusions and recommendations concerning the use of cement-aggregate combinations in concrete.  
The results of tests performed using this method furnish information on the likelihood that a cement-aggregate combination is potentially capable of harmful alkali-silica reactivity with consequent deleterious expansion of concrete. Criteria to determine potential deleterious alkali-silica reactivity of cement-aggregate combinations from the results of this test method have been given in the Appendix of Specification C33.
Insignificant expansion may result when potentially deleteriously reactive siliceous rocks are present in comparatively high proportion even when a high-alkali cement is used. This may occur because the alkali-silica reaction products are characterized by an alkali to silica ratio that is so low as to minimize uptake of water and swelling, or because of alkali leaching from the bars (see section on containers). Dolomitic aggregates that are deleteriously affected by the alkali-carbonate reaction when employed as course aggregate in concrete may not produce notable expansion in this test method. Also, significant expansion may occur rarely in the test for reasons other than alkali-aggregate reaction, particularly the presence of sulfates in the aggregate that produce a sulfate attack upon the cement paste, ferrous sulfides (pyrite, marcasite, or pyrrhotite) that oxidize and hydrate with the release of sulfate, and materials such as free lime (CaO) or free magnesia (MgO) in the cement or aggregate that progre...
SCOPE
1.1 This test method covers the determination of the susceptibility of cement-aggregate combinations to expansive reactions involving hydroxyl ions associated with the alkalies (sodium and potassium) by measurement of the increase (or decrease) in length of mortar bars containing the combination during storage under prescribed conditions of test.
1.2 Alkalies participating in the expansive reactions usually are derived from the cement; under some circumstances they may be derived from other constituents of the concrete or from external sources. Two types of alkali reactivity of aggregates are recognized:  (1) an alkali-silica reaction involving certain siliceous rocks, minerals, and natural or artificial glasses and (2) an alkali-carbonate reaction involving dolomite in certain calcitic dolomites and dolomitic limestones (see Descriptive Nomenclature C294). The method is not recommended as a means to detect the latter reaction because expansions produced in the mortar-bar test by the alkali-carbonate reaction (see Test Method C586) are generally much less than those produced by the alkali-silica reaction for combinations having equally harmful effects in service.
1.3 The values stated in SI units are to be regarded as standard. When combined standards are cited, the selection of measurement system is at the user’s discretion subject to the requirements of the referenced standard.
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.
WITHDRAWN RATIONALE
This test method covered the determination of the susceptibility of cement-aggregate combinations to expansive reactions involving hydroxyl ions associated with the alkalies (sodium and potassium) by measurement of the increase (or dec...

General Information

Status
Withdrawn
Publication Date
31-Jan-2010
Withdrawal Date
12-Nov-2018
ICS
91.100.10 - Cement. Gypsum. Lime. Mortar
Technical Committee
C09 - Concrete and Concrete Aggregates
Drafting Committee
C09.50 - Aggregate Reactions in Concrete
Current Stage
Ref Project

Relations

Referred By
ASTM C1157/C1157M-23 - Standard Performance Specification for Hydraulic Cement
Effective Date
01-Feb-2010
Referred By
ASTM C1562-10(2018) - Standard Guide for Evaluation of Materials Used in Extended Service of Interim Spent Nuclear Fuel Dry Storage Systems
Effective Date
01-Feb-2010
Referred By
ASTM C311/C311M-22 - Standard Test Methods for Sampling and Testing Fly Ash or Natural Pozzolans for Use in Portland-Cement Concrete
Effective Date
01-Feb-2010

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ASTM C227-10 - Standard Test Method for Potential Alkali Reactivity of Cement-Aggregate Combinations (Mortar-Bar Method) (Withdrawn 2018)ASTM C227-10 - Standard Test Method for Potential Alkali Reactivity of Cement-Aggregate Combinations (Mortar-Bar Method) (Withdrawn 2018)
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ASTM C227-10 - Standard Test Method for Potential Alkali Reactivity of Cement-Aggregate Combinations (Mortar-Bar Method) (Withdrawn 2018)
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NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
Designation: C227 − 10
Standard Test Method for
Potential Alkali Reactivity of Cement-Aggregate
1
Combinations (Mortar-Bar Method)
This standard is issued under the fixed designation C227; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
This standard has been approved for use by agencies of the U.S. Department of Defense.
1. Scope* mendations issued by the World Trade Organization Technical
Barriers to Trade (TBT) Committee.
1.1 This test method covers the determination of the sus-
ceptibility of cement-aggregate combinations to expansive
2. Referenced Documents
reactions involving hydroxyl ions associated with the alkalies
2
(sodium and potassium) by measurement of the increase (or 2.1 ASTM Standards:
decrease) in length of mortar bars containing the combination
C33 Specification for Concrete Aggregates
during storage under prescribed conditions of test. C109/C109M Test Method for Compressive Strength of
Hydraulic Cement Mortars (Using 2-in. or [50-mm] Cube
1.2 Alkalies participating in the expansive reactions usually
Specimens)
are derived from the cement; under some circumstances they
C289 Test Method for Potential Alkali-Silica Reactivity of
may be derived from other constituents of the concrete or from
3
Aggregates (Chemical Method) (Withdrawn 2016)
external sources. Two types of alkali reactivity of aggregates
C294 Descriptive Nomenclature for Constituents of Con-
are recognized: (1) an alkali-silica reaction involving certain
crete Aggregates
siliceous rocks, minerals, and natural or artificial glasses and
C295 Guide for Petrographic Examination ofAggregates for
(2) an alkali-carbonate reaction involving dolomite in certain
Concrete
calcitic dolomites and dolomitic limestones (see Descriptive
C305 Practice for Mechanical Mixing of Hydraulic Cement
Nomenclature C294). The method is not recommended as a
Pastes and Mortars of Plastic Consistency
means to detect the latter reaction because expansions pro-
C441 Test Method for Effectiveness of Pozzolans or Ground
duced in the mortar-bar test by the alkali-carbonate reaction
Blast-Furnace Slag in Preventing Excessive Expansion of
(see Test Method C586) are generally much less than those
Concrete Due to the Alkali-Silica Reaction
produced by the alkali-silica reaction for combinations having
C490 Practice for Use ofApparatus for the Determination of
equally harmful effects in service.
Length Change of Hardened Cement Paste, Mortar, and
1.3 The values stated in SI units are to be regarded as
Concrete
standard. When combined standards are cited, the selection of
C511 Specification for Mixing Rooms, Moist Cabinets,
measurement system is at the user’s discretion subject to the
Moist Rooms, and Water Storage Tanks Used in the
requirements of the referenced standard.
Testing of Hydraulic Cements and Concretes
1.4 This standard does not purport to address all of the
C586 Test Method for PotentialAlkali Reactivity of Carbon-
safety concerns, if any, associated with its use. It is the
ate Rocks as Concrete Aggregates (Rock-Cylinder
responsibility of the user of this standard to establish appro-
Method)
priate safety and health practices and determine the applica-
C856 Practice for Petrographic Examination of Hardened
bility of regulatory limitations prior to use. Concrete
1.5 This international standard was developed in accor-
C1437 Test Method for Flow of Hydraulic Cement Mortar
dance with internationally recognized principles on standard- E11 Specification for Woven Wire Test Sieve Cloth and Test
ization established in the Decision on Principles for the
Sieves
Development of International Standards, Guides and Recom-
1 2
This test method is under the jurisdiction of ASTM Committee C09 on For referenced ASTM standards, visit the ASTM website, www.astm.org, or
Concrete and ConcreteAggregates and is the direct responsibility of Subcommittee contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
C09.50 on Aggregate Reactions in Concrete. Standards volume information, refer to the standard’s Document Summary page on
Current edition approved Feb. 1, 2010. Published March 2010. Originally the ASTM website.
3
approved in 1950. Last previous edition approved in 2003 as C227–03. DOI: The last approved version of this historical standard is referenced on
10.1520/C0227-10. www.astm.org.
*A Summary of Changes section appears at the end of this standard
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
1

---------------------- Page: 1 ----------------------
C227 − 10
3. Significance an
...

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4.1 This test method is intended to provide a means of assessing the ability of a hydraulic-cement grout to retain a stable volume during the stipulated testing period of 28 days, provided that the tendency to change height does not include the effects of drying caused by evaporation, uptake of moisture, carbonation, or exposure to temperatures outside the range 23.0 °C ± 2.0 °C [73 °F ± 3.5 °F] (Note 2). An exception is made when the options described in the section on test conditions are exercised.  
Note 2: This test method does not measure the change in height before setting (see Test Method C827/C827M).
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1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. (Warning—Fresh hydraulic cementitious mixtures are caustic and may cause chemical burns to exposed skin and tissue upon prolonged exposure.2)  
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ASTM C827/C827M-23(Test Method)
Standard Test Method for Change in Height at Early Ages of Cylindrical Specimens of Cementitious Mixtures

SIGNIFICANCE AND USE
4.1 This test method provides a means for comparing the relative shrinkage or expansion of cementitious mixtures. It is particularly applicable to grouting, patching, and form-filling operations where the objective is to completely fill a cavity or other defined space with a freshly mixed cementitious mixture that will continue to fill the same space at time of hardening. It would be appropriate to use this test method as a basis for prescribing mixtures having restricted or specified volume change before the mixture becomes hard.  
4.2 This test method can be used for research purposes to provide information on volume changes taking place in cementitious mixtures between the time just after mixing and the time of hardening. However, the specimen used in this test method is not completely unrestrained so that the measurements are primarily useful for comparative purposes rather than as absolute values. Further, the degree of restraint to which the specimen is subjected varies with the viscosity and degree of hardening of the mixture.
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1.1 This test method covers the determination of change in height of cylindrical specimens from the time of molding until the mixture is hard.  
1.2 This test method covers height change measurements at early ages for cementitious mixtures of paste, grout, mortar, and concrete.  
1.3 This test method is intended for determination of changes in height that occur from the time of placement until the specimen is fully hard. These include shrinkage or expansion due to hydration, settlement, evaporation, and other physical and chemical effects.  
1.4 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system are not necessarily exact equivalents; therefore, to ensure conformance with the standard, each system shall be used independently of the other, and values from the two systems shall not be combined  
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ASTM C387/C387M-23(Specification)
Standard Specification for Packaged, Dry, Combined Materials for Concrete and High Strength Mortar

ABSTRACT
This specification covers the production, properties, packaging, and testing of packaged, dry, combined materials for concrete and mortars. Concrete mixtures covered by this specification includes high-early strength concrete, normal strength concrete, normal weight concrete, high-strength mortar, and mortars for unit masonry. The purchaser shall specify the material desired as concrete, high strength mortar, or mortar for use with unit masonry, and the respective physical requirements. Materials used as ingredients in packaged, dry, combined materials for mortar and concrete shall be composed of aggregates, air-entraining admixtures, blended cement, chemical admixtures, fly ash, ground granulated blast-furnace slag, hydrated lime, latex and powder polymer modifiers, masonry cement, mortar cement, Portland cement, and silica fume. All aggregates shall be dried, without disintegration, to specific moisture content The proportions of cementitious material and aggregate shall be such that the strength requirements will be met. Packaged, dry, combined materials for concrete, high strength mortar and mortar for use with unit masonry shall conform to the respective compressive strength requirements. Scales conforming to the standards will be used for sampling concretes from a single batch using a sufficient quantity. A slump test will be performed to check if additional water is required. In sampling mortar, the contents of an entire package of dry, combined material for mortar for unit masonry or for concrete mortar shall be used. Mortar mixing equipment, which must be provided with a bowl positioning adapter, shall be used to ensure clearance for the largest size aggregate in the mix being tested. The specification includes the following testing methods for mortar: compressive strength, density and yield, air content, and water retention.
SCOPE
1.1 This specification covers the production, properties, packaging, and testing of packaged, dry, combined materials for concrete and high strength mortar. The classifications of concrete and mortar covered are defined in Section 3.
Note 1: The scope of this standard does not cover mortars for unit masonry. Dry preblended mortars for unit masonry are covered by Specification C1714/C1714M.  
1.2 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the two systems may result in non-conformance with the standard. Some values have only SI units because the inch-pound equivalents are not used in practice.  
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1.4 The following safety hazards caveat pertains only to the test method portion of this specification. This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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ASTM C87/C87M-23(Test Method)
Standard Test Method for Effect of Organic Impurities in Fine Aggregate on Strength of Mortar

SIGNIFICANCE AND USE
5.1 This test method is of significance in making a final determination of the acceptability of fine aggregates with respect to the requirements of Specification C33/C33M concerning organic impurities.  
5.2 This test method is applicable to those samples which, when tested in accordance with Test MethodC40/C40M, have produced a supernatant liquid with a color darker than the standard listed in Table 1 of C40/C40M (Organic plate No. 3, Gardner Color Standard No. 14, Circular Disk No. 14 or prepared color solution).  
5.3 Many specifications provide for the acceptance of fine aggregate producing a darker color in the Test Method C40/C40M test, if testing by this test method indicates the strength of the mortar cubes prepared with the unwashed fine aggregate is comparable to the strength of mortar cubes made with the washed fine aggregate.
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1.1 This test method covers the determination of the effect on mortar strength of the organic impurities in fine aggregate, whose presence is indicated using Test Method C40/C40M. Comparison is made between compressive strengths of mortar made with washed and unwashed fine aggregate.  
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Standard Guide for Comparing Performance of Concrete-Making Materials Using Mortar Mixtures

SIGNIFICANCE AND USE
4.1 The results of mortar mixture tests can be suitable for comparing the relative performance of combinations of concrete-making materials such as fine aggregate, chemical admixtures, supplementary cementitious materials (SCMs), water, and hydraulic cement. Furthermore, this guide can be useful to identify unexpected performances due to combination of various materials. The relative trends in performance observed with the mortar method may suggest relative performance in concrete mixtures batched with the same materials and relative mixture proportions.  
4.2 While there are a number of ways to proportion and mix mortar mixtures, three procedures described in this guide have been used extensively for evaluating the performance of admixtures. Method A enables evaluation of materials using mixture proportions that correspond to specific job conditions. Method B can be used as a general mixture using fixed amounts of a standard sand, cement, and supplementary cementitious materials. Method C is a modified version of Test Method C359 to evaluate the impact of chemical admixtures on the early stiffening of a mortar prepared with specified amounts of job cement, a standard sand, and an amount of water that will produce a mortar with a specified initial penetration measured in accordance with Test Method C359. The measurements of penetration over time can be related to the early stiffening processes associated with false and flash set. Methods A and B would be most applicable for investigating material incompatibility issues associated with ready mixed concrete, while Method C would be applicable for concrete mixed for a short period of time in stationary mixers and transported to the forms in non-agitating equipment.
SCOPE
1.1 This guide provides information on how to compare the relative performance and potential incompatibility of combinations of concrete-making materials. Performance tests on fresh and early-age properties of mortar mixtures can be useful indicators of concrete performance using similar materials. The performance tests described in this guide include mortar-slump, mortar spread, mortar-workability retention, early stiffening of mortar, time of setting, air entrainment, and hydration kinetics.  
1.2 Units—The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the two systems may result in non-conformance with this guide. Some values only have SI units because the inch-pound equivalents are not used in guide.  
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Standard Practice for Measuring Hydration Kinetics of Hydraulic Cementitious Mixtures Using Isothermal Calorimetry

SIGNIFICANCE AND USE
5.1 Thermal power curves are used to evaluate the isothermal hydration kinetics of the combined mixture of different materials during the early period after being mixed with water. These isothermal power curves, or hydration profiles, may provide indications relative to setting characteristics, compatibility of different materials, sulfate balance and early strength development. The isothermal hydration profiles can also be used to evaluate the effects of compositions, proportions, and time of addition of materials as well as curing temperature. Special care must be used in evaluating extended retardation with paste specimens, which have been shown to overestimate the retardation of some mixtures containing cement, SCM, and admixtures.  
5.2 This procedure can be used to measure the effect of chemical admixtures on the cement hydration profile. In many cases, the addition of chemical admixture changes the kinetics of cement hydration.  
5.3 Although this technique has been used historically to understand issues related to setting and slump loss, it must be emphasized that isothermal calorimetry results cannot predict concrete performance definitely, either positively or negatively. Extensive verification in concrete at planned dosages and temperatures, and at higher dosages, is needed. Isothermal calorimetry is an effective tool to identify sensitivities, so that concrete testing can be efficiently planned and performed.  
5.4 This practice provides a means of assessing the relative hydration performance of various test mixtures compared with control mixtures that are prepared in a similar manner.  
5.5 The procedure and apparatus can be used to monitor the thermal power from pastes and mortars alone or in combination with chemical admixtures.  
5.6 The isothermal calorimeter described here can be used to measure the thermal power and heat of hydration of mortars prepared independently or obtained by wet sieving from concrete in accordance with Practice C172/C1...
SCOPE
1.1 This practice describes the apparatus and procedure for measuring relative differences in hydration kinetics of hydraulic cementitious mixtures, either in paste or mortar (see Note 1), including those containing admixtures, various supplementary cementitious materials (SCM), and other fine materials by measuring the thermal power using an isothermal calorimeter.
Note 1: Paste specimens are often preferred for mechanistic research when details of individual reaction peaks are important or for particular calorimetry configurations. Mortar specimens may give results that have better correlation with concrete setting and early strength development and are often preferred to evaluate different mixture proportions for concrete. Both paste and mortar studies have been found to be effective in evaluating concrete field problems due to incompatibility of materials used in concrete mixtures.  
1.2 This practice does not cover the measurement of heat of hydration. Heat of hydration can be determined according to Test Method C1702.  
1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. (Warning—Fresh hydraulic cementitious mixtures are caustic and may cause chemical burns to skin and tissue upon prolonged exposure.2)  
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ASTM C1260-22(Test Method)
Standard Test Method for Potential Alkali Reactivity of Aggregates (Mortar-Bar Method)

SIGNIFICANCE AND USE
4.1 This test method provides a means of detecting the potential of an aggregate intended for use in concrete for undergoing alkali-silica reaction resulting in potentially deleterious internal expansion. It is based on the NBRI Accelerated Test Method (1-4).3 It is especially useful for aggregates that react slowly or produce expansion late in the reaction. However, it does not evaluate combinations of aggregates with cementitious materials nor are the test conditions representative of those encountered by concrete in service.  
4.2 Because the specimens are exposed to a NaOH solution, the alkali content of the cement is not a significant factor in affecting expansions.  
4.3 Results of tests conducted on an aggregate as described herein should form a part of the basis for a decision as to whether precautions should be taken against excessive expansion due to alkali-silica reaction. Refer to Guide C1778 for the interpretation of the test results from Test Method C1260.
SCOPE
1.1 This test method permits detection, within 16 days, of the potential for deleterious alkali-silica reaction of aggregate in mortar bars.  
1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard. When this test method refers to combined-unit standards, the selection of the measurement systems is at the user’s discretion.  
1.3 The text of this test method refers to notes and footnotes that provide explanatory material. These notes and footnotes (excluding those in tables and figures) shall not be considered as requirements of this test method.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. A specific precautionary statement is given in the section on Reagents.  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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ASTM C1709-22(Guide)
Standard Guide for Evaluation of Alternative Supplementary Cementitious Materials (ASCM) for Use in Concrete

SIGNIFICANCE AND USE
4.1 Supplementary cementitious materials (SCM) covered under existing ASTM specifications are fly ash, slag cement, raw and calcined natural pozzolans including calcined clays, silica fume, and ground-glass pozzolan. The use of these materials, and limits established in existing specifications, are based on data obtained from research programs, field testing, and long term performance monitoring. Performance of SCM in specific concrete mixtures is commonly verified through preconstruction testing. This guide provides an approach to assessing the properties of materials that are not covered under existing specifications, and for assessing the performance of those materials in concrete.  
4.2 If an ASCM does not yet have a significant record of performance in concrete, a comprehensive evaluation based on this Guide should be undertaken, and it should be recognized that this ASCM might be introduced for a specific project or into a limited marketplace to initially demonstrate its performance. The user should bear in mind the intended end use of the ASCM and use appropriate test methods to establish its suitability. An ASCM that demonstrates good performance through a comprehensive evaluation as outlined in this guide could then be considered to have access to broader markets and could be considered for inclusion in an ASTM standard for SCM. For this reason, the test program to demonstrate acceptable performance should include concrete mixtures with a range of characteristics specific to the ASCM’s intended use.  
4.3 In the absence of long-term durability or acceptable field performance, prospective users are advised to apply appropriate risk management and engineering practice in the use of an ASCM.
SCOPE
1.1 This guide is intended to provide a technical approach to the evaluation of alternative supplementary cementitious materials such as pozzolans and hydraulic materials that fall outside the scope of Specifications C618, C989/C989M, C1240, and C1866/C1866M. This guide provides the initial steps for a comprehensive evaluation of an ASCM that provides due diligence for its specific intended uses in concrete; however, it does not evaluate conformance to all possible performance criteria for all types of concrete mixtures.  
1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.3 Performing the tests or meeting the test limits in this guide should not imply that the material tested meets the requirements of Specifications C618, C989/C989M, C1240, and C1866/C1866M. These materials should not be represented as such and each specific source is to be evaluated separately.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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ASTM
ASTM C1753/C1753M-21a(Practice)
Standard Practice for Evaluating Early Hydration of Hydraulic Cementitious Mixtures Using Thermal Measurements

SIGNIFICANCE AND USE
5.1 This practice provides a means of assessing the relative early hydration performance of various test mixtures compared with control mixtures that are prepared in a similar manner.  
5.2 Thermal profiles are used to evaluate the hydration behavior of hydraulic cementitious mixtures after the addition of water. They may provide indications concerning setting characteristics, compatibility of different materials, sulfate balance, relative heat of hydration, and early strength development. They can be used to evaluate the effects of compositions, proportions, and time of addition of materials as well as the initial mixture and test temperatures. Thermal profile testing is an effective tool for identifying performance sensitivities or trends, and may help to reduce the number of concrete test mixtures required to develop and qualify mixtures, especially those to be subject to variable ambient environments. It may be used by concrete producers, materials suppliers, and other practitioners to support mixture development, selection of material types or sources, optimization of proportions, or troubleshooting of field problems.  
5.3 This practice can be used to understand concrete problems related to slump loss, setting, and early strength, but results may not predict field concrete performance. Performance verification with concrete is needed to quantify the trends identified using thermal testing.  
5.4 This practice can be used to evaluate the effects of chemical admixtures on the thermal profiles of cementitious mixtures. This can be especially useful in selecting dosages appropriate for different ambient conditions.  
5.5 Thermal measurement testing as described in this practice may have similar significance and use as isothermal calorimetry described by Practice C1679 or some types of near-adiabatic calorimetry. The selection of which practice or methods to use may depend on specific applications and circumstances. The thermal profiles obtained by this practic...
SCOPE
1.1 This practice describes the apparatus and procedure for evaluating relative differences in early hydration of hydraulic cementitious mixtures such as paste, mortar, or concrete, including those containing chemical admixtures, various supplementary cementitious materials (SCMs), and other finely divided materials, by measuring the temperature history of a specimen.  
1.2 Calorimetry is the measurement of heat lost or gained during a chemical reaction such as cement hydration; calorimetric measurements as a function of time can be used to describe and evaluate hydration and related early-age property development. Calorimetry may be performed under isothermal conditions (as described in Practice C1679) or under adiabatic or semi-adiabatic conditions. This practice cannot be described as calorimetry because no attempt is made to measure or compute the heat evolved from test specimens due to hydration, but it can in many cases be used for similar evaluations. Variables that should be considered in the application of this practice are discussed in the Appendix.  
1.3 Units—The values stated in either SI units or inch-pound units shall be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, each system must be used independently of the other. Combining values from the two systems may result in non-conformance with the standard. Some values have only SI units because the inch-pound equivalents are not used in practice.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
Note 1: Warning: Fresh hydraulic cementitious mixtures are caustic and may cause chemical burns to skin and tissue upon prolonged exposure.2  
1.5 This...

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ASTM
ASTM C1753/C1753M-21(Practice)
Standard Practice for Evaluating Early Hydration of Hydraulic Cementitious Mixtures Using Thermal Measurements

SIGNIFICANCE AND USE
5.1 This practice provides a means of assessing the relative early hydration performance of various test mixtures compared with control mixtures that are prepared in a similar manner.  
5.2 Thermal profiles are used to evaluate the hydration behavior of hydraulic cementitious mixtures after the addition of water. They may provide indications concerning setting characteristics, compatibility of different materials, sulfate balance, relative heat of hydration, and early strength development. They can be used to evaluate the effects of compositions, proportions, and time of addition of materials as well as the initial mixture and test temperatures. Thermal profile testing is an effective tool for identifying performance sensitivities or trends, and may help to reduce the number of concrete test mixtures required to develop and qualify mixtures, especially those to be subject to variable ambient environments. It may be used by concrete producers, materials suppliers, and other practitioners to support mixture development, selection of material types or sources, optimization of proportions, or troubleshooting of field problems.  
5.3 This practice can be used to understand concrete problems related to slump loss, setting, and early strength, but results may not predict field concrete performance. Performance verification with concrete is needed to quantify the trends identified using thermal testing.  
5.4 This practice can be used to evaluate the effects of chemical admixtures on the thermal profiles of cementitious mixtures. This can be especially useful in selecting dosages appropriate for different ambient conditions.  
5.5 Thermal measurement testing as described in this practice may have similar significance and use as isothermal calorimetry described by Practice C1679 or some types of near-adiabatic calorimetry. The selection of which practice or methods to use may depend on specific applications and circumstances. The thermal profiles obtained by this practic...
SCOPE
1.1 This practice describes the apparatus and procedure for evaluating relative differences in early hydration of hydraulic cementitious mixtures such as paste, mortar, or concrete, including those containing chemical admixtures, various supplementary cementitious materials (SCMs), and other finely divided materials, by measuring the temperature history of a specimen.  
1.2 Calorimetry is the measurement of heat lost or gained during a chemical reaction such as cement hydration; calorimetric measurements as a function of time can be used to describe and evaluate hydration and related early-age property development. Calorimetry may be performed under isothermal conditions (as described in Practice C1679) or under adiabatic or semi-adiabatic conditions. This practice cannot be described as calorimetry because no attempt is made to measure or compute the heat evolved from test specimens due to hydration, but it can in many cases be used for similar evaluations. Variables that should be considered in the application of this practice are discussed in the Appendix.  
1.3 Units—The values stated in either SI units or inch-pound units shall be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, each system must be used independently of the other. Combining values from the two systems may result in non-conformance with the standard. Some values have only SI units because the inch-pound equivalents are not used in practice.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
Note 1: Warning: Fresh hydraulic cementitious mixtures are caustic and may cause chemical burns to skin and tissue upon prolonged exposure.2  
1.5 This...

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