Standard Specification for Glycerin Base Engine Coolant for Automobile and Light-Duty Service

ABSTRACT
This specification covers the requirements for glycerin base engine coolants used in automobiles or other light duty service cooling systems. The requirements for engine coolant concentrates, prediluted glycerin base engine coolants, glycerin base coolant concentrates, and coolant concentrates include colour, effect on non-metals, relative density, and corrosion in glassware.
SCOPE
1.1 This specification covers the requirements for glycerin base engine coolants used in automobiles or other light duty service cooling systems. When concentrates are used at 50 to 60 % concentration by volume in water, or when prediluted glycerin base engine coolants (50 volume % minimum) are used without further dilution, they will function effectively to provide protection against freezing, boiling, and corrosion.  
1.2 The coolants governed by this specification are categorized as follows:    
Coolant Type  
Description  
I  
Glycerin base concentrate  
II  
Glycerin predilute (50 to 60 volume %)
Note 1: This specification is based on the knowledge of the performance of engine coolants prepared from new or virgin ingredients that comply with Specification D7640.  
1.3 The values stated in SI units are to be regarded as the standard. The values in parentheses are for information only.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. See X1.5 and X3.1.3 for specific warning statements.
Note 2: This specification applies to automobiles and light duty service. A glycerin based specification for heavy duty engine service is under development.

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Publication Date
31-Mar-2016
Current Stage
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NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
´1
Designation:D7714 −11 (Reapproved 2016)
Standard Specification for
Glycerin Base Engine Coolant for Automobile and Light-
Duty Service
This standard is issued under the fixed designation D7714; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision.Anumber in parentheses indicates the year of last reapproval.A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
ε NOTE—Caution statement in X1.5 was changed to a Warning and Table X1.1 was editorially corrected inMay 2016.
1. Scope D516Test Method for Sulfate Ion in Water
D1119Test Method for Percent Ash Content of Engine
1.1 This specification covers the requirements for glycerin
Coolants
base engine coolants used in automobiles or other light duty
D1120Test Method for Boiling Point of Engine Coolants
service cooling systems. When concentrates are used at 50 to
D1121Test Method for ReserveAlkalinity of Engine Cool-
60 % concentration by volume in water, or when prediluted
ants and Antirusts
glycerin base engine coolants (50 volume % minimum) are
D1122Test Method for Density or Relative Density of
used without further dilution, they will function effectively to
EngineCoolantConcentratesandEngineCoolantsByThe
provide protection against freezing, boiling, and corrosion.
Hydrometer
1.2 The coolants governed by this specification are catego-
D1123Test Methods for Water in Engine Coolant Concen-
rized as follows:
trate by the Karl Fischer Reagent Method
Coolant Type Description
D1126Test Method for Hardness in Water
I Glycerin base concentrate
II Glycerin predilute (50 to 60 volume %)
D1177Test Method for Freezing Point of Aqueous Engine
Coolants
NOTE 1—This specification is based on the knowledge of the perfor-
mance of engine coolants prepared from new or virgin ingredients that
D1287TestMethodforpHofEngineCoolantsandAntirusts
comply with Specification D7640.
D1293Test Methods for pH of Water
1.3 The values stated in SI units are to be regarded as the
D1384Test Method for Corrosion Test for Engine Coolants
standard. The values in parentheses are for information only.
in Glassware
D1881Test Method for Foaming Tendencies of Engine
1.4 This standard does not purport to address all of the
Coolants in Glassware
safety concerns, if any, associated with its use. It is the
D1882Test Method for Effect of Cooling System Chemical
responsibility of the user of this standard to establish appro-
Solutions on Organic Finishes for Automotive Vehicles
priate safety and health practices and determine the applica-
bility of regulatory limitations prior to use. See X1.5 and D2570TestMethodforSimulatedServiceCorrosionTesting
X3.1.3 for specific warning statements. of Engine Coolants
NOTE 2—This specification applies to automobiles and light duty
D2809Test Method for Cavitation Corrosion and Erosion-
service. A glycerin based specification for heavy duty engine service is
Corrosion Characteristics of Aluminum Pumps With En-
under development.
gine Coolants
2. Referenced Documents
D3321Test Method for Use of the Refractometer for Field
Test Determination of the Freezing Point of Aqueous
2.1 ASTM Standards:
Engine Coolants
D512Test Methods for Chloride Ion In Water
D3634Test Method for Trace Chloride Ion in Engine Cool-
ants
ThisspecificationisunderthejurisdictionofASTMCommitteeD15onEngine
Coolants and Related Fluids and is the direct responsibility of Subcommittee
D4327Test Method forAnions in Water by Suppressed Ion
D15.07 on Specifications.
Chromatography
Current edition approved April 1, 2016. Published May 2016. Originally
D4340TestMethodforCorrosionofCastAluminumAlloys
approved in 2011. Last previous edition approved in 2011 as D7714-11. DOI:
10.1520/D7714-11R16E01.
in Engine Coolants Under Heat-Rejecting Conditions
For referenced ASTM standards, visit the ASTM website, www.astm.org, or
D4725TerminologyforEngineCoolantsandRelatedFluids
contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
D5827Test Method for Analysis of Engine Coolant for
Standards volume information, refer to the standard’s Document Summary page on
the ASTM website. Chloride and Other Anions by Ion Chromatography
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
´1
D7714−11 (2016)
D5931Test Method for Density and Relative Density of
Property Specific Values ASTM Test Method
Engine Coolant Concentrates and Aqueous Engine Cool-
Chlorides, µg/g 25 (1.5) max D5827, D512, D4327
ants by Digital Density Meter
(ppm, grains ⁄gal)
D6130Test Method for Determination of Silicon and Other
Sulfate, µg/g 50 (3.0) max D5827, D516, D4327
(ppm, grains ⁄gal)
Elements in Engine Coolant by Inductively Coupled
Hardness, as CaCO , 20 (1.2) max D6130, D1126
Plasma-Atomic Emission Spectroscopy
µg ⁄g (ppm, grains/gal)
D6660Test MethodforFreezingPointofAqueous Ethylene
pH 5.5 to 8.5 D1287, D1293
Iron, µg/g (ppm, grains/gal) 1.0 (0.06) max D6130, E394
Glycol Base Engine Coolants by Automatic Phase Tran-
sition Method
NOTE 3—Prediluted coolants are intended for direct addition to an
D7640Specification for Engine Coolant Grade Glycerin
enginecoolingsystemwithnofurtherdilution.However,ifcircumstances
require addition and prediluted aqueous engine coolant is not available,
E29Practice for Using Significant Digits in Test Data to
use the appropriate engine coolant concentrate (Type I) diluted to 50
Determine Conformance with Specifications
volume % with water of at least the quality outlined in Table X1.1.
E394Test Method for Iron in Trace Quantities Using the
1,10-Phenanthroline Method 4.4 When diluting engine coolant concentrates for actual
2.2 Other Standards:
service, use municipal (treated) water, or low-mineral content
Federal Method 2540BTotal Dissolved Solids Dried at
wellwater(seeAppendixX1,TableX1.1).Ifsuchwaterisnot
103-105°C
available,usedeionized(demineralized)ordistilledwater.This
procedure will minimize the formation of hard water scale and
3. Terminology
avoid the introduction of mineral components, such as chlo-
3.1 Definitions:
rides and sulfates, which can increase the corrosion rate of
3.1.1 glycerin base engine coolant, n—engine coolant in
aluminum and iron.
which the freeze point depressant is 1,2,3 propanetriol, with
4.5 Wheninstalledinaccordancewiththevehiclemanufac-
inhibitors to minimize foaming and corrosion.
turer’srecommendationsandthoseontheproductlabel,engine
3.1.2 other glycols, n—in ethylene glycol base engine
coolant concentrates or prediluted glycerin base engine cool-
coolant, diethylene glycol, triethylene glycol, tetraethylene
ants shall be suitable for use in a properly maintained cooling
glycol, propylene glycol, dipropylene glycol, tripropylene
system (Appendix X1) in normal light-duty service for a
glycol, and 1,3-propanediol.
minimum of one year without adversely affecting fluid flow
3.1.3 other glycols, n—in propylene glycol base engine
and heat transfer.
coolant, ethylene glycol, diethylene glycol, triethylene glycol,
tetraethylene glycol, dipropylene glycol, tripropylene glycol,
5. Detailed Requirements
and 1,3-propanediol.
5.1 Glycerin base coolant concentrates and prediluted cool-
3.2 For definitions of other terms used in this specification,
ants shall be in accordance with the physical and chemical
refer to Terminology D4725.
requirements prescribed in Table 2 depending on coolant type
(see 1.2).
4. General Requirements
4.1 Engine coolant concentrates or prediluted glycerin base
5.2 TherequirementslistedinTable2forpredilutedcoolant
engine coolants shall be formulated with glycerin meeting
(Type II) are prescribed for the coolant as packaged, without
Specification D7640, water, and suitable corrosion inhibitors,
further dilution or adjustment.
dye, and a foam suppressor.
5.3 All coolant concentrates and prediluted coolants shall
4.2 All engine coolant concentrates or prediluted glycerin
conform to the performance requirements listed in Table 3.
base engine coolants shall be in accordance with the general
5.4 Coolant concentrates shall be diluted for performance
requirements given in Table 1.
testing as described in the individual ASTM test methods.
TABLE 1 General Requirements
5.5 If necessary, the freezing point of prediluted coolants
Property Specified Values ASTM Test Method
shall be adjusted with deionized water before proceeding with
Color Distinctive . . .
performance testing. The freezing point of prediluted glycerin
Effect on nonmetals No adverse effect Under consideration
base coolants (Type II) shall be −°27.0°C (−°16.6°F).
5.6 Adjusted, prediluted engine coolant performance test
4.3 Prediluted glycerin (Type II) base engine coolants shall
solutions shall be prepared as described in Table 3, Footnotes
be formulated using water that meets the following require-
B through F.
ments:
6. Keywords
Standard Method for the Examination of Water and Wastewater, American
6.1 engine coolant; engine coolant concentrate; glycerin;
Public Health Association, et al, 800 I Street, NW, Washington, DC 20001,
http://www.apha.org. light duty engine coolant; prediluted engine coolant
´1
D7714−11 (2016)
TABLE 2 Physical and Chemical Requirements
Property Type I Type II ASTM Test Method
Relative density, 15.5/15.5°C (60/60°F) 1.249 to 1.265 1.130 min
Relative density, 25/25°C (77/77°F) 1.252 to 1.262 1.127 min D1122, D5931
A, B
Freezing Point, °C (°F):
50 % (vol) in DI water -27.0 (-16.6) max
D1177, D6660
Undiluted -27.0 (-16.6) max
C
Boiling point, °C (°F): D1120
50 % (vol) in DI water 106 (223) min
Undiluted 172 (342) min 106 (223) min
Ash content, mass % 5 max 2.5 max D1119
pH: D1287
50 vol % in DI water 7.5 to 11
Undiluted 7.5to11
D
Chloride, µg/g 25 max 25 max D3634, D5827
Water, mass % 5 max not applicable D1123
E E
Reserve alkalinity, mL report report D1121
F
Effect on automotive finish (use clear coat no effect no effect D1882
thermoset urethane or acrylic ure
...


This document is not an ASTM standard and is intended only to provide the user of an ASTM standard an indication of what changes have been made to the previous version. Because
it may not be technically possible to adequately depict all changes accurately, ASTM recommends that users consult prior editions as appropriate. In all cases only the current version
of the standard as published by ASTM is to be considered the official document.
´1
Designation: D7714 − 11 D7714 − 11 (Reapproved 2016)
Standard Specification for
Glycerin Base Engine Coolant for Automobile and Light-
Duty Service
This standard is issued under the fixed designation D7714; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
ε NOTE—Caution statement in X1.5 was changed to a Warning and Table X1.1 was editorially corrected in May 2016.
1. Scope
1.1 This specification covers the requirements for glycerin base engine coolants used in automobiles or other light duty service
cooling systems. When concentrates are used at 50 to 60 % concentration by volume in water, or when prediluted glycerin base
engine coolants (50 volume % minimum) are used without further dilution, they will function effectively to provide protection
against freezing, boiling, and corrosion.
1.2 The coolants governed by this specification are categorized as follows:
Coolant Type Description
I Glycerin base concentrate
II Glycerin predilute (50 to 60 volume %)
NOTE 1—This specification is based on the knowledge of the performance of engine coolants prepared from new or virgin ingredients that comply with
Specification D7640.
1.3 The values stated in SI units are to be regarded as the standard. The values in parentheses are for information only.
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility
of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory
limitations prior to use. See X1.5 and X3.1.3 for specific caution statement.warning statements.
NOTE 2—This specification applies to automobiles and light duty service. A glycerin based specification for heavy duty engine service is under
development.
2. Referenced Documents
2.1 ASTM Standards:
D512 Test Methods for Chloride Ion In Water
D516 Test Method for Sulfate Ion in Water
D1119 Test Method for Percent Ash Content of Engine Coolants
D1120 Test Method for Boiling Point of Engine Coolants
D1121 Test Method for Reserve Alkalinity of Engine Coolants and Antirusts
D1122 Test Method for Density or Relative Density of Engine Coolant Concentrates and Engine Coolants By The Hydrometer
D1123 Test Methods for Water in Engine Coolant Concentrate by the Karl Fischer Reagent Method
D1126 Test Method for Hardness in Water
D1177 Test Method for Freezing Point of Aqueous Engine Coolants
D1287 Test Method for pH of Engine Coolants and Antirusts
D1293 Test Methods for pH of Water
D1384 Test Method for Corrosion Test for Engine Coolants in Glassware
D1881 Test Method for Foaming Tendencies of Engine Coolants in Glassware
D1882 Test Method for Effect of Cooling System Chemical Solutions on Organic Finishes for Automotive Vehicles
D2570 Test Method for Simulated Service Corrosion Testing of Engine Coolants
This specification is under the jurisdiction of ASTM Committee D15 on Engine Coolants and Related Fluids and is the direct responsibility of Subcommittee D15.07
on Specifications.
Current edition approved Oct. 1, 2011April 1, 2016. Published October 2011May 2016. Originally approved in 2011. Last previous edition approved in 2011 as D7714-11.
DOI: 10.1520/D7714-11.10.1520/D7714-11R16E01.
For referenced ASTM standards, visit the ASTM website, www.astm.org, or contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM Standards
volume information, refer to the standard’s Document Summary page on the ASTM website.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
´1
D7714 − 11 (2016)
D2809 Test Method for Cavitation Corrosion and Erosion-Corrosion Characteristics of Aluminum Pumps With Engine Coolants
D3321 Test Method for Use of the Refractometer for Field Test Determination of the Freezing Point of Aqueous Engine Coolants
D3634 Test Method for Trace Chloride Ion in Engine Coolants
D4327 Test Method for Anions in Water by Suppressed Ion Chromatography
D4340 Test Method for Corrosion of Cast Aluminum Alloys in Engine Coolants Under Heat-Rejecting Conditions
D4725 Terminology for Engine Coolants and Related Fluids
D5827 Test Method for Analysis of Engine Coolant for Chloride and Other Anions by Ion Chromatography
D5931 Test Method for Density and Relative Density of Engine Coolant Concentrates and Aqueous Engine Coolants by Digital
Density Meter
D6130 Test Method for Determination of Silicon and Other Elements in Engine Coolant by Inductively Coupled Plasma-Atomic
Emission Spectroscopy
D6660 Test Method for Freezing Point of Aqueous Ethylene Glycol Base Engine Coolants by Automatic Phase Transition
Method
D7640 Specification for Engine Coolant Grade Glycerin
E29 Practice for Using Significant Digits in Test Data to Determine Conformance with Specifications
E394 Test Method for Iron in Trace Quantities Using the 1,10-Phenanthroline Method
2.2 Other Standards:
Federal Method 2540B Total Dissolved Solids Dried at 103-105°C
3. Terminology
3.1 Definitions:
3.1.1 glycerin base engine coolant, n—engine coolant in which the freeze point depressant is 1,2,3 propanetriol, with inhibitors
to minimize foaming and corrosion.
3.1.2 other glycols, n—in ethylene glycol base engine coolant, diethylene glycol, triethylene glycol, tetraethylene glycol,
propylene glycol, dipropylene glycol, tripropylene glycol, and 1,3-propanediol.
3.1.3 other glycols, n—in propylene glycol base engine coolant, ethylene glycol, diethylene glycol, triethylene glycol,
tetraethylene glycol, dipropylene glycol, tripropylene glycol, and 1,3-propanediol.
3.1.3 glycerin base engine coolant, n—engine coolant in which the freeze point depressant is 1,2,3 propanetriol, with inhibitors
to minimize foaming and corrosion.
3.2 For definitions of other terms used in this specification, refer to Terminology D4725.
4. General Requirements
4.1 Engine coolant concentrates or prediluted glycerin base engine coolants shall be formulated with glycerin meeting
Specification D7640, water, and suitable corrosion inhibitors, dye, and a foam suppressor.
4.2 All engine coolant concentrates or prediluted glycerin base engine coolants shall be in accordance with the general
requirements given in Table 1.
TABLE 1 General Requirements
Property Specified Values ASTM Test Method
Color Distinctive . . .
Effect on nonmetals No adverse effect Under consideration
4.3 Prediluted glycerin (Type II) base engine coolants shall be formulated using water that meets the following requirements:
Standard Method for the Examination of Water and Wastewater, American Public Health Association, et al, 1015 15th Street800 I Street, NW, Washington, DC
20000520001, http://www.apha.org.
´1
D7714 − 11 (2016)
Specific ASTM
Property
Values Test Method
Specific ASTM
Property
Values Test Method
Chlorides, μg/g 25 (1.5) max D5827, D512, D4327
(ppm, grains/gal)
Chlorides, μg/g 25 (1.5) max D5827, D512, D4327
(ppm, grains ⁄ gal)
Sulfate, μg/g 50 (3.0) max D5827, D516, D4327
(ppm, grains/gal)
Sulfate, μg/g 50 (3.0) max D5827, D516, D4327
(ppm, grains ⁄ gal)
Hardness, as CaCO , μg/g 20 (1.2) max D6130, D1126
(ppm, grains/gal)
Hardness, as CaCO , 20 (1.2) max D6130, D1126
μg ⁄ g (ppm, grains/gal)
pH 5.5 to 8.5 D1287, D1293
Iron, μg/g (ppm, grains/gal) 1.0 (0.06) max D6130, E394
NOTE 3—Prediluted coolants are intended for direct addition to an engine cooling system with no further dilution. However, if circumstances require
addition and prediluted aqueous engine coolant is not available, use the appropriate engine coolant concentrate (Type I) diluted to 50 volume % with water
of at least the quality outlined in Table X1.1.
4.4 When diluting engine coolant concentrates for actual service, use municipal (treated) water, or low-mineral content well
water (see Appendix X1, Table X1.1). If such water is not available, use deionized (demineralized) or distilled water. This
procedure will minimize the formation of hard water scale and avoid the introduction of mineral components, such as chlorides
and sulfates, which can increase the corrosion rate of aluminum and iron.
4.5 When installed in accordance with the vehicle manufacturer’s recommendations and those on the product label, engine
coolant concentrates or prediluted glycerin base engine coolants shall be suitable for use in a properly maintained cooling system
(Appendix X1) in normal light-duty service for a minimum of one year without adversely affecting fluid flow and heat transfer.
5. Detailed Requirements
5.1 Glycerin base coolant concentrates and prediluted coolants shall be in accordance with the physical and chemical
requirements prescribed in Table 2 depending on coolant type (see 1.2).
5.2 The requirements listed in Table 2 for prediluted coolant (Type II) are prescribed for the coolant as packaged, without further
dilution or adjustment.
TABLE 2 Physical and Chemical Requirements
Property Type I Type II ASTM Test Method
Relative density, 15.5/15.5°C (60/60°F) 1.249 to 1.265 1.130 min
Relative density, 25/25°C (77/77°F) 1.252 to 1.262 1.127 min D1122, D5931
A,B
Freezing Point, °C (°F):
A, B
Freezing Point, °C (°F):
50% (vol) in DI water -27.0 (-16.6) max
D1177, D6660
50 % (vol) in DI water -27.0 (-16.6) max
D1177, D6660
Undiluted -27.0 (-16.6) max
C
Boiling point, °C (°F): D1120
50% (vol) in DI water 106 (223) min
50 % (vol) in DI water 106 (223) min
Undiluted 172 (342) min 106 (223) min
Ash content, mass % 5 max 2.5 max D1119
pH: D1287
50 vol % in DI water 7.5 to 11
Undiluted 7.5 to 11
D
Chloride, μg/g 25 max 25 max D3634, D5827
Water, mass % 5 max not applicable D1123
E E
Reserve alkalinity, mL report report D1121
F
Effect on automotive finish (use clear coat no effect no effect D1882
thermoset urethane or acrylic urethane finish)
F
Effect on automotive finish (use clear coat no effect no effect D1882
thermoset urethane or acrylic urethane finish)
A
For purposes of determining conformance with this specification, an observed value shall be rounded “to the nearest unit” in the last right-hand digit used in expressing
the specification limit, in accordance with the rounding method of Practice E29.
B
The blender/user should be advised that due to the relatively high density of glycerin; % vol and % mass are not interchangeable. For example, 50%50 % solution by
volume is equivalent to 56%56 % by weight.
C
Some precipitate may be observed at the end of the test. This should not be cause for rejection.
D
In case of dispute, Test Method D3634 shall be the preferred test method.
E
Value as agreed upon between the supplier and the customer.
F
Currently, many vehicle manufacturers prepare test panels using the specific paint finishes employed on their actual products. Coolant suppliers and vehicle
manufacturers should agree on the exact test procedures and acceptance criteria on an individual basis.
´1
D7714 − 11 (2016)
5.3 All coolant concentrates and prediluted coolants shall conform to the performance requirements listed in Table 3.
5.4 Coolant concentrates shall be diluted for performance testing as described in the individual ASTM test methods.
5.5 If necessary, the freezing point of prediluted coolants shall be adjusted with deionized water before proceeding with
performance testing. The freezing point of prediluted glycerin base coolants (Type II) shall be −°27.0°C (−°16.6°F).
5.6 Adjusted, prediluted engine coolant performance test solutions shall be prepared as described in Table 3, Footnotes B
through F.
6. Keywords
6.1 engine coolant; engine coolant concentrate; glycerin; light duty engine coolant; prediluted engine coolant
APPENDIXES
(Nonmandatory Information)
X1. COOLING SYSTEM MAINTENANCE
X1.1 Filling the Cooling System
X1.1.1 Before installing engine coolant, the cooling system should be inspected and necessary service work completed.
X1.1.2 Cooling system fill should consist of coolant concentrate and water or prediluted glycerin base engine coolant (50 %
volume minimum).
A
TABLE 3 Performance Requirements
ASTM Test Solution Concentration,
Property Specific Values
Test Method vol % Glycerin Antifreeze
B
Corrosion in glassware D1384 33
Weight loss, mg/specimen:
copper 10 max
solder 30 max
brass 10 max
steel 10 max
cast iron 10 max
aluminum 30 max
C
Simulated service test D2570 44
Weight loss, mg/specimen:
copper 20 max
solder 60 max
brass 20 max
steel 20 max
cast iron 20 max
aluminum 60 max
D
Corrosion of cast aluminum alloys 1.0 max D4340 25
at heat-rejecting surfaces, mg/cm /week
D
Corrosion of cast aluminum alloys 1.0 max D4340 25
at heat-rejecting surfaces, mg/cm /week
E
Foaming D1881 33
Volume, mL 150 max
Break time, s 5 max
F
Cavitation-Erosion 8 min D2809 17
Rating for pitting, cavitation, and
erosion of the water pump
A
For engine coolant concentrates, test solutions shall be prepared in accordance with the directions provided in the individual ASTM test methods noted. For prediluted
engine coolants, prepare test solutions using the directions provided in Footnotes B through F.
B
For prediluted coolants, prepare the test solution by mixing 67 volume % of the adjusted (see 4.4) prediluted product with 33 volume % ASTM Type IV reagent water.
Add 99 mg of sodium sulfate, 110 mg of sodium chloride, and 92 mg of sodium bicarbonate per litre of test solution.
C
For prediluted coolants, prepare the test solution by mixing 88 volume % of the adjusted (see 4.4) prediluted product with 12 volume % ASTM Type IV reagent water.
Add 83 mg of sodium sulfate, 92 mg of sodium chloride, and 77 mg of sodium bicarbonate per litre of test solution.
D
For prediluted coolants, prepare the test solution by mixing 50 volume % of the adjusted (see 4.4) prediluted product with 50 volume % ASTM Type IV reagent water.
Add 165 mg of sodium chloride per litre of test solution.
E
For prediluted coolants, prepare the test solution by mixing 67 volume % of the adjusted (see 4.4) prediluted product with 33 volume % ASTM Type II reagent water.
F
For prediluted coolants, prepare the test solution by mixing 33 volume % of the adjusted (see 4.4) prediluted product with 67 volume % ASTM Type IV reagent water.
Add 123 mg of sodium sulfate, 137 mg of sodium chloride, and 115 m
...

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