Standard Specification for ASTM Reference Fluid for Coolant Tests

ABSTRACT
This specification covers a reference ethylene glycol-base test fluid to be used in providing base line data for ASTM coolant test procedures. The reference test fluid concentrate shall be prepared to conform to the requirements as to chemical composition prescribed. The materials used to prepare the reference test fluid shall meet the requirements specified. The formulated reference test fluid concentrate shall conform to the requirements for laboratory test performance prescribed.
SIGNIFICANCE AND USE
5.1 The data obtained for the reference test fluid are intended to be used by laboratory personnel to determine their capability to perform tests properly. If a particular determination does not fall within the prescribed limits, it has to be assumed that an error occurred in the application of the test procedure.  
5.2 The coolant composition given in this specification is not intended to be a commercial product.
SCOPE
1.1 This specification covers a reference ethylene glycol-base test fluid to be used in providing base line data for ASTM coolant test procedures.  
1.2 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.3 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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Publication Date
29-Feb-2024
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This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the
Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
Designation: D3585 − 24
Standard Specification for
1
ASTM Reference Fluid for Coolant Tests
This standard is issued under the fixed designation D3585; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope Concentrates and Engine Coolants By The Hydrometer
D1123 Test Methods for Water in Engine Coolant Concen-
1.1 This specification covers a reference ethylene glycol-
trate by the Karl Fischer Reagent Method
base test fluid to be used in providing base line data for ASTM
D1176 Practice for Sampling and Preparing Aqueous Solu-
coolant test procedures.
tions of Engine Coolants or Antirusts for Testing Purposes
1.2 This standard does not purport to address all of the
D1177 Test Method for Freezing Point of Aqueous Engine
safety concerns, if any, associated with its use. It is the
Coolants
responsibility of the user of this standard to establish appro-
D1287 Test Method for pH of Engine Coolants and Antirusts
priate safety, health, and environmental practices and deter-
D1384 Test Method for Corrosion Test for Engine Coolants
mine the applicability of regulatory limitations prior to use.
in Glassware
1.3 This international standard was developed in accor-
D1613 Test Method for Acidity in Volatile Solvents and
dance with internationally recognized principles on standard-
Chemical Intermediates Used in Paint, Varnish, Lacquer,
ization established in the Decision on Principles for the
and Related Products
Development of International Standards, Guides and Recom-
D1881 Test Method for Foaming Tendencies of Engine
mendations issued by the World Trade Organization Technical
Coolants in Glassware
Barriers to Trade (TBT) Committee.
D3634 Test Method for Trace Chloride Ion in Engine Cool-
ants
2. Referenced Documents
D5827 Test Method for Analysis of Engine Coolant for
2
2.1 ASTM Standards:
Chloride and Other Anions by Ion Chromatography
D501 Test Methods of Sampling and Chemical Analysis of
D5931 Test Method for Density and Relative Density of
Alkaline Detergents
Engine Coolant Concentrates and Aqueous Engine Cool-
D538 Specification for Trisodium Phosphate (Withdrawn
ants by Digital Density Meter
3
2001)
E202 Test Methods for Analysis of Ethylene Glycols and
D891 Test Methods for Specific Gravity, Apparent, of Liquid
Propylene Glycols
Industrial Chemicals
D1078 Test Method for Distillation Range of Volatile Or-
3. Chemical Composition Requirements
ganic Liquids
3.1 The reference test fluid concentrate shall be prepared to
D1119 Test Method for Percent Ash Content of Engine
conform to the requirements as to chemical composition
Coolants
prescribed in Table 1.
D1120 Test Method for Boiling Point of Engine Coolants
D1121 Test Method for Reserve Alkalinity of Engine Cool-
4. Ingredient Requirements
ants and Antirusts
4.1 The materials used to prepare the reference test fluid
D1122 Test Method for Relative Density of Engine Coolant
shall meet the requirements given in Annex A1 – Annex A5.
1
5. Significance and Use
This specification is under the jurisdiction of ASTM Committee D15 on Engine
Coolants and Related Fluids and is the direct responsibility of Subcommittee
5.1 The data obtained for the reference test fluid are
D15.01 on Reference Test Materials.
intended to be used by laboratory personnel to determine their
Current edition approved March 1, 2024. Published March 2024. Originally
approved in 1989. Last previous edition approved in 2020 as D3585 – 08 (2020).
capability to perform tests properly. If a particular determina-
DOI: 10.1520/D3585-24.
tion does not fall within the prescribed limits, it has to be
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or
assumed that an error occurred in the application of the test
contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
Standards volume information, refer to the standard’s Document Summary page on procedure.
the ASTM website.
3
5.2 The coolant composition given in this specification is
The last approved version of this historical standard is referenced on
www.astm.org. not intended to be a commercial product.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
1

---------------------- Page: 1 ----------------------
D3585 − 24
TABLE 1 Chemical Composition Requirements
NOTE 1—The reference coolant shall be colored blue-green using Alizarine Cyanine Green G Extra 100 % added in the proportion of 0.3 g of d
...

This document is not an ASTM standard and is intended only to provide the user of an ASTM standard an indication of what changes have been made to the previous version. Because
it may not be technically possible to adequately depict all changes accurately, ASTM recommends that users consult prior editions as appropriate. In all cases only the current version
of the standard as published by ASTM is to be considered the official document.
Designation: D3585 − 08 (Reapproved 2020) D3585 − 24
Standard Specification for
1
ASTM Reference Fluid for Coolant Tests
This standard is issued under the fixed designation D3585; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope
1.1 This specification covers a reference ethylene glycol-base test fluid to be used in providing base line data for ASTM coolant
test procedures.
1.2 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility
of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of
regulatory limitations prior to use.
1.3 This international standard was developed in accordance with internationally recognized principles on standardization
established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued
by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
2. Referenced Documents
2
2.1 ASTM Standards:
D501 Test Methods of Sampling and Chemical Analysis of Alkaline Detergents
3
D538 Specification for Trisodium Phosphate (Withdrawn 2001)
D891 Test Methods for Specific Gravity, Apparent, of Liquid Industrial Chemicals
D1078 Test Method for Distillation Range of Volatile Organic Liquids
D1119 Test Method for Percent Ash Content of Engine Coolants
D1120 Test Method for Boiling Point of Engine Coolants
D1121 Test Method for Reserve Alkalinity of Engine Coolants and Antirusts
D1122 Test Method for Relative Density of Engine Coolant Concentrates and Engine Coolants By The Hydrometer
D1123 Test Methods for Water in Engine Coolant Concentrate by the Karl Fischer Reagent Method
D1176 Practice for Sampling and Preparing Aqueous Solutions of Engine Coolants or Antirusts for Testing Purposes
D1177 Test Method for Freezing Point of Aqueous Engine Coolants
D1287 Test Method for pH of Engine Coolants and Antirusts
D1384 Test Method for Corrosion Test for Engine Coolants in Glassware
D1613 Test Method for Acidity in Volatile Solvents and Chemical Intermediates Used in Paint, Varnish, Lacquer, and Related
Products
D1881 Test Method for Foaming Tendencies of Engine Coolants in Glassware
D3634 Test Method for Trace Chloride Ion in Engine Coolants
D5827 Test Method for Analysis of Engine Coolant for Chloride and Other Anions by Ion Chromatography
1
This specification is under the jurisdiction of ASTM Committee D15 on Engine Coolants and Related Fluids and is the direct responsibility of Subcommittee D15.01
on Reference Test Materials.
Current edition approved Jan. 1, 2020March 1, 2024. Published January 2020March 2024. Originally approved in 1989. Last previous edition approved in 20132020 as
D3585–08(2013).D3585 – 08 (2020). DOI: 10.1520/D3585–08R20.10.1520/D3585-24.
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM Standards
volume information, refer to the standard’s Document Summary page on the ASTM website.
3
The last approved version of this historical standard is referenced on www.astm.org.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
1

---------------------- Page: 1 ----------------------
D3585 − 24
D5931 Test Method for Density and Relative Density of Engine Coolant Concentrates and Aqueous Engine Coolants by Digital
Density Meter
E202 Test Methods for Analysis of Ethylene Glycols and Propylene Glycols
3. Chemical Composition Requirements
3.1 The reference test fluid concentrate shall be prepared to conform to the requirements as to chemical composition prescribed
in Table 1.
4. Ingredient Requirements
4.1 The materials used to prepare the reference test fluid shall meet the requirements given in Annex A1 – Annex A5.
5. Significance and Use
5.1 The data obtained for the reference test fluid are intended to be used by laboratory personnel to determine their capability to
perform tests properly. If a particular determination does not fall within the prescribed limits, it has to be assumed that an error
occurred in the application of the test procedure.
5.2 The coolant composition given in this specification is not intended to be a commercial
...

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