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ASTM D5471-10

(Specification)

Standard Specification for O-Xylene 980

Standard Specification for O-Xylene 980

ABSTRACT
This specification covers a grade of o-xylene identified as ortho-Xylene 980. O-xylene 980 shall be tested and sampled in accordance with standard test methods and practices and shall conform to the following requirements: purity; non-aromatic hydrocarbons; p-xylene plus m-xylene; C9 and heavier aromatics; cumene; bromine index; appearance which shall be a clear liquid, free of sediment and haze; color in the platinum-cobalt scale; and distillation range.
SCOPE
1.1 This specification covers a grade of o-xylene identified as ortho-Xylene 980.
1.2 The following applies to all specified limits in this specification: for purposes of determining conformance with this specification, an observed value or a calculated value shall be rounded off to the nearest unit in the last right-hand digit used in expressing the specification limit, in accordance with the rounding-off method of Practice E29.
1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.4 Consult current OSHA regulations and supplier's Material Safety Data Sheets, and local regulations for all materials used in this specification.

General Information

Status
Historical
Publication Date
14-Feb-2010
ICS
71.080.15 - Aromatic hydrocarbons
Technical Committee
D16 - Aromatic, Industrial, Specialty and Related Chemicals
Drafting Committee
D16.01 - Benzene, Toluene, Xylenes, Cyclohexane and Their Derivatives
Current Stage
Ref Project

Relations

Replaces
ASTM D5471-04e1 - Standard Specification for O-Xylene 980
Effective Date
15-Feb-2010
Replaced By
ASTM D5471-16 - Standard Specification for O-Xylene 980
Effective Date
01-Jun-2016

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Standards Content (Sample)

NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
Designation: D5471 −10
StandardSpecification for
1
O-Xylene 980
This standard is issued under the fixed designation D5471; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope* D5776 Test Method for Bromine Index of Aromatic Hydro-
carbons by Electrometric Titration
1.1 This specification covers a grade of o-xylene identified
D7504 Test Method for Trace Impurities in Monocyclic
as ortho-Xylene 980.
Aromatic Hydrocarbons by Gas Chromatography and
1.2 The following applies to all specified limits in this
Effective Carbon Number
specification: for purposes of determining conformance with
E29 Practice for Using Significant Digits in Test Data to
this specification, an observed value or a calculated value shall
Determine Conformance with Specifications
be rounded off to the nearest unit in the last right-hand digit
3
2.2 Other Document:
used in expressing the specification limit, in accordance with
OSHA Regulations, 29 CFR Paragraphs 1910.1000 and
the rounding-off method of Practice E29.
1910.1200
1.3 The values stated in SI units are to be regarded as
standard. No other units of measurement are included in this
3. Properties
standard.
3.1 O-Xylene 980 shall conform to the following require-
1.4 Consult current OSHAregulations and supplier’s Mate-
ments:
rial Safety Data Sheets, and local regulations for all materials
ASTM Test
Property Specification
A
used in this specification. Method
Purity, min, wt % 98.0 D3797 or D7504
2. Referenced Documents
Nonaromatic hydrocarbons, max, wt % 0.5 D3797 or D7504
p-Xylene plus m-Xylene, max, wt % 1.3 D3797 or D7504
2
2.1 ASTM Standards:
C9 and heavier aromatics, max, wt % 0.8 D3797 or D7504
B
D850 Test Method for Distillation of Industrial Aromatic Cumene, wt % 0.5 D3797 or D7504
Bromine index, max mg/100 g 100 D1492 or D5776
Hydrocarbons and Related Materials
C
Appearance .
D1209 Test Method for Color of Clear Liquids (Platinum-
Color, Pt-Co scale, max 10 D1209 or D5386
Cobalt Scale) Distillation range, including the tempera- 2.0 D850
ture, 144.4°C at 101.3 kPA (760 mm
D1492 Test Method for Bromine Index of Aromatic Hydro-
Hg) pressure, max, °C
carbons by Coulometric Titration
A
D3437 Practice for Sampling and Handling Liquid Cyclic
If more than one method is listed for a property the producer and user should
agree on the referee method.
Products
B
Cumene is a significant component in o-xylene as it may contribute to deflagra-
D3797 Test Method for Analysis of o-Xylene by Gas Chro-
tions in some processes under certain conditions.
C
matography
Clear liquid, free of sediment and haze when observed at 18.3 to 25.6°C.
D5386 Test Method for Color of L
...

This document is not an ASTM standard and is intended only to provide the user of an ASTM standard an indication of what changes have been made to the previous version. Because
it may not be technically possible to adequately depict all changes accurately, ASTM recommends that users consult prior editions as appropriate. In all cases only the current version
of the standard as published by ASTM is to be considered the official document.
´1
Designation:D5471–04 Designation: D5471 – 10
Standard Specification for
1
O-Xylene 980
This standard is issued under the fixed designation D5471; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1
´ NOTE—Section 3 editorially corrected in March 2005.
1. Scope*
1.1 This specification covers a grade of o-xylene identified as ortho-Xylene 980.
1.2 The following applies to all specified limits in this specification: for purposes of determining conformance with this
specification, an observed value or a calculated value shall be rounded off to the nearest unit in the last right-hand digit used in
expressing the specification limit, in accordance with the rounding-off method of Practice E29.
1.3Consult current OSHA regulations
1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.4 Consult current OSHA regulations and supplier’s Material Safety Data Sheets, and local regulations for all materials used
in this specification.
2. Referenced Documents
2
2.1 ASTM Standards:
D850 Test Method for Distillation of Industrial Aromatic Hydrocarbons and Related Materials
D1209 Test Method for Color of Clear Liquids (Platinum-Cobalt Scale)
D1492 Test Method for Bromine Index of Aromatic Hydrocarbons by Coulometric Titration
D3437 Practice for Sampling and Handling Liquid Cyclic Products
D3797 Test Method for Analysis of o-Xylene by Gas Chromatography
D5386 Test Method for Color of Liquids Using Tristimulus Colorimetry
D5776 Test Method for Bromine Index of Aromatic Hydrocarbons by Electrometric Titration
D7504 Test Method forTrace Impurities in MonocyclicAromatic Hydrocarbons by Gas Chromatography and Effective Carbon
Number
E29 Practice for Using Significant Digits in Test Data to Determine Conformance with Specifications
3
2.2 Other Document:
OSHA Regulations 29CFR, Paragraphs 1910.1000 and 1910.1200 OSHA Regulations, 29 CFR Paragraphs 1910.1000 and
1910.1200
3. Properties
3.1 O-Xylene 980 shall conform to the following requirements:
ASTM Test
Property Specification
A
Method
Purity, min, wt % 98.0 D3797
Purity, min, wt % 98.0 D3797 or D7504
Nonaromatic hydrocarbons, max, wt % 0.5 D3797
Nonaromatic hydrocarbons, max, wt % 0.5 D3797 or D7504
p-Xylene plus m-Xylene, max, wt % 1.3 D3797
1
This specification is under the jurisdiction ofASTM Committee D16 onAromatic Hydrocarbons and Related Chemicals and is the direct responsibility of Subcommittee
D16.01 on Benzene, Toluene, Xylenes, Cyclohexane, and Their Derivatives.
Current edition approved Dec. 1, 2004. Published January 2005. Originally approved in 1993. Last previous edition approved in 2003 as D5471–97(2003). DOI:
10.1520/D5471-04E01.on Benzene, Toluene, Xylenes, Cyclohexane and Their Derivatives.
´1
Current edition approved Feb. 15, 2010. Published April 2010. Originally approved in 1993. Last previous edition approved in 2004 as D5471 – 0
...

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