Standard Test Method for Cohesion/Adhesion of Sprayed Fire-Resistive Materials Applied to Structural Members

SIGNIFICANCE AND USE
The intent of this test method is to determine a property of SFRM that may be used to provide an indication of its in-place serviceability. Satisfactory performance of SFRM applied to structural members and assemblies depends upon its ability to withstand the various influences that may occur during construction and during the life of the structure, as well as upon its satisfactory performance under fire conditions.
SCOPE
1.1 This test method covers a procedure for measuring the cohesion/adhesion or bond strength (tensile) perpendicular to the surface of sprayed fire-resistive material (SFRM) applied to rigid backing. These fire-resistive materials include sprayed fibrous and cementitious materials. The test method is applicable to both laboratory and field procedures as indicated in Section 7.
1.2 The values stated in SI units are to be regarded as the standard. The values in parentheses are for information only.
1.3 This standard does not purport to address all of the safety problems, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

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NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
Designation:E736–00 (Reapproved 2006)
Standard Test Method for
Cohesion/Adhesion of Sprayed Fire-Resistive Materials
Applied to Structural Members
This standard is issued under the fixed designation E736; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
This standard has been approved for use by agencies of the Department of Defense.
1. Scope SFRM with a suitable adhesive. An increasing load, measured
by a scale, is applied manually until failure occurs.
1.1 This test method covers a procedure for measuring the
cohesion/adhesion or bond strength (tensile) perpendicular to
4. Significance and Use
thesurfaceofsprayedfire-resistivematerial(SFRM)appliedto
4.1 The intent of this test method is to determine a property
rigid backing. These fire-resistive materials include sprayed
of SFRM that may be used to provide an indication of its
fibrous and cementitious materials. The test method is appli-
in-place serviceability. Satisfactory performance of SFRM
cable to both laboratory and field procedures as indicated in
applied to structural members and assemblies depends upon its
Section 7.
ability to withstand the various influences that may occur
1.2 The values stated in SI units are to be regarded as the
during construction and during the life of the structure, as well
standard. The values in parentheses are for information only.
as upon its satisfactory performance under fire conditions.
1.3 This standard does not purport to address all of the
safety problems, if any, associated with its use. It is the
5. Apparatus
responsibility of the user of this standard to establish appro-
5.1 Fig. 1 illustrates a suitable apparatus.
priate safety and health practices and determine the applica-
5.2 Bottle Screw Cap, metal or rigid plastic 51 mm to 83
bility of regulatory limitations prior to use.
1 1
mm (2 in. to 3 ⁄4 in.) in diameter and 12 mm ( ⁄2 in.) in nominal
2. Referenced Documents depth. A hook shall be attached at the center. Where deck
2 profile does not allow the use of an 83-mm (3 ⁄4-in.) diameter
2.1 ASTM Standards:
cap due to area restriction, a minimum 51-mm (2-in.) diameter
E84 Test Method for Surface Burning Characteristics of
cap shall be used.
Building Materials
5.3 Adhesive, single or two component, suitable for adher-
E119 Test Methods for Fire Tests of Building Construction
ing cap to SFRM.
and Materials
5.4 Weighing Scale, spring type (fish hook), with a capacity
E605 Test Methods for Thickness and Density of Sprayed
suitable for the SFRM being tested (typically 12 kg to 30 kg
Fire-Resistive Material (SFRM) Applied to Structural
(26 to 66 lb) capacity). The accuracy shall be within 0.1 kg ( ⁄4
Members
lb).
3. Summary of Test Method 5.5 GalvanizedSteelSheet,1.5mm(0.060in.(16ga))thick,
300 mm (12 in.) square, cleaned with solvent to remove any oil
3.1 The cohesion/adhesion is determined using a metal or
from surface to be sprayed.
plastic cap with a hook attached. The cap is attached to the
5.6 Drying Oven, capable of maintaining temperature and
humidity conditions during the specimen curing cycle, in
This test method is under the jurisdiction of ASTM Committee E06 on
accordance with the SFRM manufacturers’ published require-
Performance of Buildings and is the direct responsibility of Subcommittee E06.21
ments.
on Serviceability.
Current edition approved Jan. 1, 2006. Published January 2006. Originally
approved in 1980. Last previous edition approved in 2000 as E736 – 00. DOI:
10.1520/E0736-00R06.
2 3
For referenced ASTM standards, visit the ASTM website, www.astm.org, or Refer to Appendix X1.2 for a list of bottle screw cap supply houses that have
contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM been found satisfactory for this purpose. Many local suppliers are also available.
Standards volume information, refer to the standard’s Document Summary page on Suitable adhesives are commercially available. Refer to Appendix X1.1 for a
the ASTM website. list of adhesive supply houses that have been found satisfactory for this purpose.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, United States.
E736–00 (2006)
8. Procedure
8.1 Apply adhesive sufficient to fill the metal or plastic cap,
and immediately place the cap against the surface of the
SFRM. Refer to Fig. 2.
8.2 Support the cap at the surface until the adhesive has
adequately cured. Wipe away any excess adhesive around the
cap before it cures, or carefully cut it away after it cures.
8.3 Laboratory Tests:
8.3.1 Restrain the specimen with the SFRM facing up to
prevent movement and flexing during testing. The orientation
FIG. 1 Typical Cohesion/Adhesion Testing Apparatus
of the specimen in Fig. 2 shows the SFRM facing down.
8.3.2 Engagethescalewiththehookandexertanincreasing
force at a minimum uniform or incremental rate of approxi-
6. Sampling
mately 5 kg (11 lb)/min perpendicular to the surface.
6.1 This test method requires the application of SFRM in
8.3.3 Force shall be applied until failure occurs, a predeter-
accordance with manufacturers’ published instructions. The
mined value is reached, or until the capacity of the scale is
apparatus, materials, and procedures used to spray apply the
reached.
SFRM for this test shall be representative of application in the
8.3.4 Recordtheforceinnewtons(pounds-force)atthetime
field.
failure occurs or other end point is reached.
6.2 The density of the prepared specimens shall be similar
8.4 Field Tests:
to the density tested and reported during the Test Methods E84
8.4.1 Perform tests as described in 8.3.2-8.3.4.
and E119 fire exposure tests of t
...


This document is not an ASTM standard and is intended only to provide the user of an ASTM standard an indication of what changes have been made to the previous version. Because
it may not be technically possible to adequately depict all changes accurately, ASTM recommends that users consult prior editions as appropriate. In all cases only the current version
of the standard as published by ASTM is to be considered the official document.
An American National Standard Designation: E 736 – 00 (Reapproved 2006)
Designation:E736–00
Standard Test Method for
Cohesion/Adhesion of Sprayed Fire-Resistive Materials
Applied to Structural Members
This standard is issued under the fixed designation E 736; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
This standard has been approved for use by agencies of the Department of Defense.
1. Scope
1.1 This test method covers a procedure for measuring the cohesion/adhesion or bond strength (tensile) perpendicular to the
surface of sprayed fire-resistive material (SFRM) applied to rigid backing. These fire-resistive materials include sprayed fibrous
and cementitious materials. The test method is applicable to both laboratory and field procedures as indicated in Section 7.
1.2 The values stated in SI units are to be regarded as the standard. The values in parentheses are for information only.
1.3 This standard does not purport to address all of the safety problems, if any, associated with its use. It is the responsibility
of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory
limitations prior to use.
2. Referenced Documents
2.1 ASTM Standards:
E84 Test Method for Surface Burning Characteristics of Building Materials
E119 Test Methods for Fire Tests of Building Construction and Materials
E 605 Test Methods for Thickness and Density of Sprayed Fire-Resistive Material (SFRM) Applied to Structural Members
3. Summary of Test Method
3.1 The cohesion/adhesion is determined using a metal or plastic cap with a hook attached. The cap is attached to the SFRM
with a suitable adhesive. An increasing load, measured by a scale, is applied manually until failure occurs.
4. Significance and Use
4.1 The intent of this test method is to determine a property of SFRM that may be used to provide an indication of its in-place
serviceability. Satisfactory performance of SFRM applied to structural members and assemblies depends upon its ability to
withstand the various influences that may occur during construction and during the life of the structure, as well as upon its
satisfactory performance under fire conditions.
5. Apparatus
5.1 Fig. 1 illustrates a suitable apparatus.
1 1
5.2 BottleScrewCap, metal or rigid plastic 51 mm to 83 mm (2 in. to 3 ⁄4 in.) in diameter and 12 mm ( ⁄2 in.) in nominal depth.
A hook shall be attached at the center. Where deck profile does not allow the use of an 83-mm (3 ⁄4-in.) diameter cap due to area
restriction, a minimum 51-mm (2-in.) diameter cap shall be used.
5.3 Adhesive, single or two component, suitable for adhering cap to SFRM.
5.4 Weighing Scale, spring type (fish hook), with a capacity suitable for the SFRM being tested (typically 12 kg to 30 kg (26
to 66 lb) capacity). The accuracy shall be within 0.1 kg ( ⁄4 lb).
5.5 Galvanized Steel Sheet, 1.5 mm (0.060 in. (16 ga)) thick, 300 mm (12 in.) square, cleaned with solvent to remove any oil
from surface to be sprayed.
5.6 Drying Oven, capable of maintaining temperature and humidity conditions during the specimen curing cycle, in accordance
This test method is under the jurisdiction of ASTM Committee E-6 E06 on Performance of Buildings and is the direct responsibility of Subcommittee E06.21 on
Serviceability.
Current edition approved April 10, 2000. Published July 2000. Originally published as E736–80. Last previous edition E736–92.
Current edition approved Jan. 1, 2006. Published January 2006. Originally approved in 1980. Last previous edition approved in 2000 as E 736 – 00.
For referencedASTM standards, visit theASTM website, www.astm.org, or contactASTM Customer Service at service@astm.org. ForAnnualBookofASTMStandards
, Vol 04.07.volume information, refer to the standard’s Document Summary page on the ASTM website.
Refer to Appendix X1.2 for a list of bottle screw cap supply houses that have been found satisfactory for this purpose. Many local suppliers are also available.
Suitable adhesives are commercially available. Refer to Appendix X1.1 for a list of adhesive supply houses that have been found satisfactory for this purpose.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, United States.
E 736 – 00 (2006)
FIG. 1 Typical Cohesion/Adhesion Testing Apparatus
with the SFRM manufacturers’ published requirements.
6. Sampling
6.1 ThistestmethodrequirestheapplicationofSFRMinaccordancewithmanufacturers’publishedinstructions.Theapparatus,
materials, and procedures used to spray apply the SFRM for this test shall be representative of application in the field.
6.2 The density of the prepared specimens shall be similar to the density tested and reported during the Test Methods E119E 84
and E84E 119fire exposure tests of the same material, or as required by the sponsor of the test.
6.3 Determine and report in accordance with Test Methods E 605 the density and thickness of each sample, or of a randomly
selected specimen from the sample lot when a number of identical samples are being tested for the laboratory-prepared samples.
For the field specimens, determine the density from material adjacent to the test specimen.
7. Test Specimen
7.1 Laboratory Tests:
7.1.1 The SFRM shall be applied at a thickness of 12 mm to 25 mm ( ⁄2 in. to 1 in.) to the 300 by 300 mm (12 by 12 in.)
galvanized steel sheet.
7.1.2 Condition the specimen at room temperature (206 10°C (68 6 18°F)).After 72 h, samples may be force dried in a drying
oven at 43 6 6°C (110 6 10°F), and a rel
...

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