Standard Practice for Evaluation of Limestone or Lime Uniformity From a Single Source

SIGNIFICANCE AND USE
4.1 This practice is designed to present in a standardized format information on the variability of limestone or lime from a single source over a period of time. It can be applied to all materials covered in Test Methods C25, C110, C1271, and C1301, and Specification C141.
SCOPE
1.1 This practice is intended for use in instances where the purchaser desires information on the uniformity of limestone or lime produced at a single source. It is intended that this test method normally be used for the predominant material manufactured at a plant. Guidelines for sampling, testing and presentation of results (Table 1) are given.  
1.2 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.3 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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Publication Date
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This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the
Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
Designation: C1164 − 22
Standard Practice for
Evaluation of Limestone or Lime Uniformity From a Single
1
Source
This standard is issued under the fixed designation C1164; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope Lime and Limestone
C1301 Test Method for Major and Trace Elements in Lime-
1.1 This practice is intended for use in instances where the
stone and Lime by Inductively Coupled Plasma-Atomic
purchaserdesiresinformationontheuniformityoflimestoneor
Emission Spectroscopy (ICP) and Atomic Absorption
lime produced at a single source. It is intended that this test
(AA)
method normally be used for the predominant material manu-
factured at a plant. Guidelines for sampling, testing and
3. Terminology
presentation of results (Table 1) are given.
3.1 Definitions:
1.2 This standard does not purport to address all of the
3.1.1 Fordefinitionsoftermsrelatingtothispracticereferto
safety concerns, if any, associated with its use. It is the
Terminology C51.
responsibility of the user of this standard to establish appro-
priate safety, health, and environmental practices and deter-
4. Significance and Use
mine the applicability of regulatory limitations prior to use.
4.1 This practice is designed to present in a standardized
1.3 This international standard was developed in accor-
format information on the variability of limestone or lime from
dance with internationally recognized principles on standard-
a single source over a period of time. It can be applied to all
ization established in the Decision on Principles for the
materials covered in Test Methods C25, C110, C1271, and
Development of International Standards, Guides and Recom-
C1301, and Specification C141.
mendations issued by the World Trade Organization Technical
Barriers to Trade (TBT) Committee.
5. Sampling
2. Referenced Documents
5.1 The sampling shall be done in accordance with Methods
2
C50.
2.1 ASTM Standards:
C25 Test Methods for Chemical Analysis of Limestone,
5.2 All sampling shall be performed by personnel qualified
Quicklime, and Hydrated Lime
by specific training for this purpose.
C50 Practice for Sampling, Sample Preparation, Packaging,
5.3 Datapointsshallbeanaverageofthreeormoreseparate
and Marking of Lime and Limestone Products
determinationsrelativetoaspecifiedunitoftime.Forexample:
C51 Terminology Relating to Lime and Limestone (as Used
(1) n determinations for daily average, (2) daily determinations
by the Industry)
for weekly average.
C110 Test Methods for Physical Testing of Quicklime,
5.4 The samples shall be identified by the date or dates that
Hydrated Lime, and Limestone
the represented material was obtained.
C141 Specification for Hydrated Hydraulic Lime for Struc-
tural Purposes
6. Procedure
C1271 Test Method for X-ray Spectrometric Analysis of
6.1 The minimum amount of testing (see 5.3) and the type
of test(s) to be performed should be agreed upon by the
1
This practice is under the jurisdiction of ASTM Committee C07 on Lime and
purchaser and producer.
Limestone and is the direct responsibility of Subcommittee C07.02 on Specifica-
tions and Guidelines. NOTE 1—A single daily analysis does not necessarily characterize a
Current edition approved July 1, 2022. Published July 2022. Originally approved product. A minimum of three analyses is more reasonable.
in 1990. Last previous edition approved in 2014 as C1164 – 14. DOI: 10.1520/
6.2 It is desirable that all tests used in a single evaluation be
C1164-22.
2
performed in the same laboratory, preferably by the same
For referenced ASTM standards, visit the ASTM website, www.astm.org, or
contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
person, in order for the results to be comparable.
Standards volume information, refer to the standard’s Document Summary page on
the ASTM website. NOTE 2—In order to obtain comparable results when exchanging
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
1

---------------------- Page: 1 ----------------------
C1164 − 22
TABLE 1 High Calcium Quicklime January 1989
7.2 The physical analysis of quicklime, hydrated lime, and
limestoneshallbedeterminedinaccordancewithTestMethods
NOTE 1—This data is presented only as a sample of the correct method
for presentation. Other tests can be substituted and others omitted. C110.
Test
7.3 The analysis of hydraulic hydrated lime shall be deter-
Day
% Acid %
...

This document is not an ASTM standard and is intended only to provide the user of an ASTM standard an indication of what changes have been made to the previous version. Because
it may not be technically possible to adequately depict all changes accurately, ASTM recommends that users consult prior editions as appropriate. In all cases only the current version
of the standard as published by ASTM is to be considered the official document.
Designation: C1164 − 14 C1164 − 22
Standard Practice for
Evaluation of Limestone or Lime Uniformity From a Single
1
Source
This standard is issued under the fixed designation C1164; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope*Scope
1.1 This practice is intended for use in instances where the purchaser desires information on the uniformity of limestone or lime
produced at a single source. It is intended that this test method normally be used for the predominant material manufactured at a
plant. Guidelines for sampling, testing and presentation of results (Table 1) are given.
1.2 The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical
conversions to SI units that are provided for information only and are not considered standard.
1.2 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility
of the user of this standard to establish appropriate safety safety, health, and healthenvironmental practices and determine the
applicability of regulatory limitations prior to use.
1.3 This international standard was developed in accordance with internationally recognized principles on standardization
established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued
by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
2. Referenced Documents
2
2.1 ASTM Standards:
C25 Test Methods for Chemical Analysis of Limestone, Quicklime, and Hydrated Lime
C50 Practice for Sampling, Sample Preparation, Packaging, and Marking of Lime and Limestone Products
C51 Terminology Relating to Lime and Limestone (as Used by the Industry)
C110 Test Methods for Physical Testing of Quicklime, Hydrated Lime, and Limestone
C141 Specification for Hydrated Hydraulic Lime for Structural Purposes
C1271 Test Method for X-ray Spectrometric Analysis of Lime and Limestone
C1301 Test Method for Major and Trace Elements in Limestone and Lime by Inductively Coupled Plasma-Atomic Emission
Spectroscopy (ICP) and Atomic Absorption (AA)
3. Terminology
3.1 Definitions:
3.1.1 For definitions of terms relating to this practice refer to Terminology C51.
1
This practice is under the jurisdiction of ASTM Committee C07 on Lime and Limestone and is the direct responsibility of Subcommittee C07.02 on Specifications and
Guidelines.
Current edition approved Dec. 1, 2014July 1, 2022. Published December 2014July 2022. Originally approved in 1990. Last previous edition approved in 20092014 as
C1164 – 92 (2009).C1164 – 14. DOI: 10.1520/C1164-14.10.1520/C1164-22.
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM Standards
volume information, refer to the standard’s Document Summary page on the ASTM website.
*A Summary of Changes section appears at the end of this standard
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
1

---------------------- Page: 1 ----------------------
C1164 − 22
TABLE 1 High Calcium Quicklime January 1989
NOTE 1—This data is presented only as a sample of the correct method
for presentation. Other tests can be substituted and others omitted.
Test
Day
% Acid % Available
% CaO % MgO
Insoluble CaO
1 0.66 95.85 2.27 94.90
2 0.84 95.03 2.87 94.08
3 1.24 95.85 1.57 94.90
4 1.22 96.67 1.49 95.71
5 1.22 96.26 1.32 95.31
8 0.68 95.85 2.06 94.69
9 0.96 95.54 2.27 94.89
10 1.26 96.15 1.74 95.20
11 1.04 96.04 2.00 95.11
13 1.26 96.26 1.51 95.31
15 1.34 95.23 2.09 94.28
16 1.28 95.44 2.34 94.69
19 0.68 96.15 1.46 95.20
20 1.42 95.85 1.27 94.90
22 1.06 95.85 1.86 94.90
23 0.58 96.15 2.09 95.31
24 0.84 95.03 2.61 94.08
26 1.28 95.64 1.39 94.69
27 1.48 95.54 1.58 94.39
29 0.98 94.82 2.71 93.67
30 1.24 94.41 3.42 93.67
Avg 1.07 95.70 2.00 94.76
Range 0.90 2.26 2.15 2.04
Std Dev 0.26 0.54 0.56 0.54
4. Significance and Use
4.1 This practice is designed to present in a standardized format information on the variability of limestone or lime from a single
source over a period of time. It can be applied to all materials covered in Test Methods C25, C110, C1271, and C1301, and
Specification C141.
5. Sampling
5.1 Th
...

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