Standard Test Method for Density of Adhesives in Fluid Form

SCOPE
1.1 This test method covers the measurement of density (weight per gallon) of adhesives, and components thereof, when in liquid form.
1.2 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

General Information

Status
Historical
Publication Date
31-Dec-1994
Technical Committee
Drafting Committee
Current Stage
Ref Project

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ASTM D1875-95 - Standard Test Method for Density of Adhesives in Fluid Form
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NOTICE: This standard has either been superceded and replaced by a new version or discontinued.
Contact ASTM International (www.astm.org) for the latest information.
Designation: D 1875 – 95
Standard Test Method for
Density of Adhesives in Fluid Form
This standard is issued under the fixed designation D 1875; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (e) indicates an editorial change since the last revision or reapproval.
This standard has been approved for use by agencies of the Department of Defense.
1. Scope (2.81 fl oz) at 25°C (77°F).
1.1 This test method covers the measurement of density
NOTE 1—The use of cups that are factory calibrated eliminates the need
(weight per gallon) of adhesives, and components thereof,
for further calibration. These cups are calibrated with distilled water so
that their proper net weight is obtained at 25°C. A temperature of 25°C is
when in liquid form.
therefore recommended when using these cups. Volume expansion of both
1.2 The values stated in SI units are to be regarded as the
cup and the material to be measured causes erroneous results, if the matter
standard. The values given in parentheses are for information
of temperature is not standardized. However, where less accuracy is
only.
required, consideration of temperature differentials may be ignored.
1.3 This standard does not purport to address all of the
5.2 Thermometer—ASTM Saybolt Viscosity Thermometer
safety concerns, if any, associated with its use. It is the
having a range from 19 to 27°C (66 to 80.5°F) and conforming
responsibility of the user of this standard to establish appro-
to the requirements for Thermometer 17C as prescribed in
priate safety and health practices and determine the applica-
Specification E 1.
bility of regulatory limitations prior to use.
5.3 Constant-Temperature Bath, capable of maintaining a
2. Referenced Documents temperature of 25 6 0.1°C (77 6 0.5°F).
5.4 Laboratory Balance, 200 g (0.44 lb) or greater capacity,
2.1 ASTM Standards:
accurate to 60.1 g (0.0002 lb).
D 907 Terminology of Adhesives
E 1 Specification for ASTM Thermometers
NOTE 2—A hanging pan, triple-beam balance, or overhead-beam type
of balance with scales graduated to 0.1 g has been found to provide results,
3. Terminology
the mean of which was consistent with the over all precision and accuracy
of this test method.
3.1 Definitions—Many terms in this test method are defined
NOTE 3—Fingerprints and smudges on the cup changes the weight and
in Terminology D 907.
is to be avoided. Handle only with tongs and with hands protected by
3.2 Definitions of Terms Specific to This Standard:
clean, dry, absorbent material.
3.2.1 density—the mass (weight in vacuum) of a unit
volume of the liquid at any given temperature expressed as the
6. Sampling
weight in pounds avoirdupois, of a U.S. gallon measure of the
6.1 Take representative samples of the lot to be evaluated
liquid at 25°C, unless otherwise specified.
from three or more separate containers, chosen at random. Do
not take samples from containers that appear to be nonrepre-
4. Significance and Use
sentative. Place the samples in airtight containers, filled to
4.1 This test method is particularly applicable where the
prevent excessive air space above the adhesive, and stored at
fluid has too high a viscosity or where a component is too
room temperature to reduce evaporation or drying to a mini-
volatile for a specific gravity balance determination.
mum. Ensure that the adhesive in the container is thoroughly
mixed if there is a tendency for the materials to separate.
5. Apparatus
5.1 Weight-Per-Gallon Cup—A weight-per-gallon cup of
7. Procedure
plated brass or stainless steel with counterbalance is recom-
7.1 Test three portions of each sample.
mended. The capacity of this cup with cover is exactly 83.2 mL
7.2 Clean and dry the cup with nonresidual solvents.
7.3 Fill the cup with the adhesive at a temperature below
This test method is under the jurisdiction of ASTM Committee D-14 on
25°C. Force down the cap for the cup to the extent of its travel,
Adhesives and is the direct responsibility of Subcommittee D14.10 on Working
leaving the overflow
...

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