ASTM F1111-08a
(Test Method)Standard Test Method for Corrosion of Low-Embrittling Cadmium Plate by Aircraft Maintenance Chemicals
Standard Test Method for Corrosion of Low-Embrittling Cadmium Plate by Aircraft Maintenance Chemicals
SIGNIFICANCE AND USE
The data generated by this test method shall be used to determine whether low embrittling cadmium plated parts are liable to be corroded or damaged by application of the test material during routine maintenance operations.
SCOPE
1.1 This test method is intended as a means of determining the corrosive effects of aircraft maintenance chemicals on low-embrittling cadmium plating used on aircraft high-strength steel, under conditions of total immersion by quantitative measurements of weight change.
1.2 This standard may involve hazardous materials, operations, and equipment. This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. For specific hazard statements see Section 6, 4.1.
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Designation:F 1111 – 08a
Standard Test Method for
Corrosion of Low-Embrittling Cadmium Plate by Aircraft
1
Maintenance Chemicals
This standard is issued under the fixed designation F 1111; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
This standard has been approved for use by agencies of the Department of Defense.
1. Scope 4. Apparatus
1.1 This test method is intended as a means of determining 4.1 Wide Mouth Sealable Glass Jar or Stoppered Flask,
the corrosive effects of aircraft maintenance chemicals on having a capacity so chosen that specimens will remain fully
low-embrittlingcadmiumplatingusedonaircrafthigh-strength immersed in a vertical position and not in contact with other
steel, under conditions of total immersion by quantitative specimens during the test and the ratio of area of immersed
measurements of weight change. metal to the volume of solution will be as prescribed in 9.1.
1.2 This standard may involve hazardous materials, opera- (Warning—Some aircraft maintenance chemicals when
tions, and equipment. This standard does not purport to heated have high vapor pressures or may produce gases during
address all of the safety concerns, if any, associated with its testing. Suitable precautions should be taken to prevent the
use. It is the responsibility of the user of this standard to containing vessel from exploding or the vessel should be so
establish appropriate safety and health practices and deter- chosen as to withstand the resulting pressures.)
mine the applicability of regulatory limitations prior to use. 4.2 Constant Temperature Device—Any suitable regulated
For specific hazard statements see Section 6, 4.1. heating device may be employed for maintaining the solution
at the required temperature.
2. Referenced Documents
4.3 Sandblaster.
2
2.1 ASTM Standards: 4.4 Ampere Meter, capable of measuring 60 65A.
D 329 Specification for Acetone
4.5 Oven, capable of maintaining temperature of 110 6 2°C
D 740 Specification for Methyl Ethyl Ketone (230 6 4°F).
D 1193 Specification for Reagent Water 4.6 Plating Bath, containing the solution specified in MIL-
D 4080 Specification for Trichloroethylene, Technical and
STD-870, Type I, Class 1.
Vapor-Degreasing Grade
5. Reagents
2.2 Industry Standards:
SAE-AMS-6345 Steel Sheet, Strip and Plate (SAE 4130) 5.1 PurityofWater—Unless otherwise indicated, references
3
Normalized or Otherwise Heat Treated to water shall be understood to mean reagent water as defined
by Type III of Specification D 1193.
3. Significance and Use
5.2 Trichloroethylene, in accordance with Specification
3.1 The data generated by this test method shall be used to
D 4080.
determine whether low embrittling cadmium plated parts are 5.3 Methyl Ethyl Ketone, in accordance with Specification
liable to be corroded or damaged by application of the test
D 740.
material during routine maintenance operations. 5.4 Acetone, in accordance with Specification D 329.
5.5 Aluminum Oxide, 180 grit.
1
This test method is under the jurisdiction of ASTM Committee F07 on
6. Safety Precautions
Aerospace and Aircraft and is the direct responsibility of Subcommittee F07.07 on
6.1 The solvents used in cleaning test specimens are flam-
Qualification Testing of Aircraft Cleaning Materials.
Current edition approved Oct. 1, 2008. Published November 2008. Originally
mable or harmful if inhaled, or both. Keep away from sparks
approved in 1988. Last previous edition approved in 2008 as F 1111 – 08.
and open flames. Avoid breathing vapors and prolonged or
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or
repeated contact with skin. Use adequate ventilation.
contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
Standards volume information, refer to the standard’s Document Summary page on
the ASTM website.
3
Available from Society of Automotive Engineers (SAE), 400 Commonwealth
Dr., Warrendale, PA 15096-0001.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, United States.
1
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F 1111 – 08a
6.2 Some materials used for aircraft maintenance may 9.4 Test Duration—Unless otherwise specified, the test
contain flammable solvents, acids or alkalis, or other toxic period shall be 24 h.
compounds. Take suitable precautions to prevent personal
10. Procedure
injury.
10.1 Dry the precleaned specimens at 110°C (230°F) for 1
7. Test Specimens
h, allow to cool to room temperature in a desiccator, then
7.1 The test specimens shall be made of 4130 steel Condi-
weigh to the nearest 0.1 mg.
tion N
...
This document is not anASTM standard and is intended only to provide the user of anASTM standard an indication of what changes have been made to the previous version. Because
it may not be technically possible to adequately depict all changes accurately, ASTM recommends that users consult prior editions as appropriate. In all cases only the current version
of the standard as published by ASTM is to be considered the official document.
Designation:F1111–08 Designation:F 1111 – 08a
Standard Test Method for
Corrosion of Low-Embrittling Cadmium Plate by Aircraft
1
Maintenance Chemicals
This standard is issued under the fixed designation F 1111; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
This standard has been approved for use by agencies of the Department of Defense.
1. Scope
1.1 This test method is intended as a means of determining the corrosive effects of aircraft maintenance chemicals on
low-embrittling cadmium plating used on aircraft high-strength steel, under conditions of total immersion by quantitative
measurements of weight change.
1.2 This standard may involve hazardous materials, operations, and equipment. This standard does not purport to address all
of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate
safety and health practices and determine the applicability of regulatory limitations prior to use. For specific hazard statements
see Section 6, 4.1, and X1.3.
2. Referenced Documents
2
2.1 ASTM Standards:
D 329 Specification for Acetone
D 740 Specification for Methyl Ethyl Ketone
D 1193 Specification for Reagent Water
D 4080 Specification for Trichloroethylene, Technical and Vapor-Degreasing Grade
2.2 Industry Standards:
3
SAE-AMS-6345 Steel Sheet, Strip and Plate (SAE 4130) Normalized or Otherwise Heat Treated
3. Significance and Use
3.1 The data generated by this test method shall be used to determine whether low embrittling cadmium plated parts are liable
to be corroded or damaged by application of the test material during routine maintenance operations.
4. Apparatus
4.1 WideMouthSealableGlassJarorStopperedFlask, having a capacity so chosen that specimens will remain fully immersed
in a vertical position and not in contact with other specimens during the test and the ratio of area of immersed metal to the volume
of solution will be as prescribed in 9.1. (Warning—Some aircraft maintenance chemicals when heated have high vapor pressures
or may produce gases during testing. Suitable precautions should be taken to prevent the containing vessel from exploding or the
vessel should be so chosen as to withstand the resulting pressures.)
4.2 Constant Temperature Device—Any suitable regulated heating device may be employed for maintaining the solution at the
required temperature.
4.3 Sandblaster.
4.4 Ampere Meter, capable of measuring 60 65A.
4.5 Oven, capable of maintaining temperature of 110 6 2°C (230 6 4°F).
4.6 Plating Bath, containing the solution specified in X1.2. , containing the solution specified in MIL-STD-870, Type I, Class
1.
1
This test method is under the jurisdiction ofASTM Committee F07 onAerospace andAircraft and is the direct responsibility of Subcommittee F07.07 on Qualification
Testing of Aircraft Cleaning Materials.
Current edition approved MayOct. 1, 2008. Published JuneNovember 2008. Originally approved in 1988. Last previous edition approved in 20022008 as F 1111 – 028.
2
For referencedASTM standards, visit theASTM website, www.astm.org, or contactASTM Customer Service at service@astm.org. ForAnnualBookofASTMStandards
volume information, refer to the standard’s Document Summary page on the ASTM website.
3
Available from Society of Automotive Engineers (SAE), 400 Commonwealth Dr., Warrendale, PA 15096-0001.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, United States.
1
---------------------- Page: 1 ----------------------
F 1111 – 08a
5. Reagents
5.1 Purity of Water—Unless otherwise indicated, references to water shall be understood to mean reagent water as defined by
Type III of Specification D 1193.
5.2 Trichloroethylene, in accordance with Specification D 4080.
5.3 Methyl Ethyl Ketone, in accordance with Specification D 740.
5.4 Acetone, in accordance with Specification D 329.
5.5 Aluminum Oxide, 180 grit.
6. Safety Precautions
6.1 The solvents used in cleaning test specimens are flammable or harmful if inhaled, or both. Keep away from sparks and open
flames. Avoid breathing vapors and prolonged or repeated contact with skin. Use adequate ventilation.
6.2Cyanides and cadmium oxide are very toxic and corrosive to skin.Take suitable precautions in the handling of them to avoid
personal injury. Use ad
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