Standard Specification for Nonvulcanized Rubber Sheet Used as Roof Flashing

SCOPE
1.1 This specification covers nonvulcanized rubber sheet made of EPDM (elastomeric terpolymer synthesized from ethylene, propylene and diene monomer) or CR (polychloroprene) intended for use as watertight roof flashing exposed to the weather.
1.2 The tests and property limits used to characterize these flashing materials are specific for each classification.
1.3 SI units shall be used in referee decisions.
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

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Publication Date
09-Jun-1997
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ASTM D4811-97 - Standard Specification for Nonvulcanized Rubber Sheet Used as Roof Flashing
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NOTICE: This standard has either been superceded and replaced by a new version or discontinued.
Contact ASTM International (www.astm.org) for the latest information.
Designation: D 4811 – 97
Standard Specification for
Nonvulcanized Rubber Sheet Used as Roof Flashing
This standard is issued under the fixed designation D 4811; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (e) indicates an editorial change since the last revision or reapproval.
1. Scope D 1204 Test Method for Linear Dimensional Changes on a
Nonrigid Thermoplastic Sheeting or Film at Elevated
1.1 This specification covers nonvulcanized rubber sheet
Temperatures
made of EPDM (ethylene-propylene-diene terpolymer) or CR
D 1418 Practice for Rubber and Rubber Latices—
(polychloroprene) intended for use as watertight roof flashing
Nomenclature
exposed to the weather.
D 2137 Test Methods for Rubber Property—Brittleness
1.2 The tests and property limits used to characterize these
Point of Flexible Polymers and Coated Fabrics
flashing materials are specific for each classification and are
D 3182 Practice for Rubber—Materials, Equipment, and
minimum values to make the product fit for its intended
Procedures for Mixing Standard Compounds and Prepar-
purpose.
ing Standard Vulcanized Sheets
1.3 SI units shall be used in referee decisions.
G 26 Practice for Operating Light-Exposure Apparatus
1.4 In-place roof system design criteria, such as fire resis-
(Xenon-Arc Type) With and Without Water for Exposure
tance, field seaming strength, material compatibility, and uplift
of Nonmetallic Materials
resistance, among others, are beyond the scope of this speci-
G 53 Practice for Operating Light and Water Exposure
fication.
(Fluorescent UV/Condensation Type) for Exposure of
1.5 The following precautionary caveat pertains to the test
Nonmetallic Materials
methods portion only, Section 8, of this specification: This
standard may involve hazardous materials, operations, and
3. Classification
equipment. This standard does not purport to address the
3.1 The following types are used to identify the principal
safety concerns associated with its use. It is the responsibility
polymer components of the flashing material (see Note 1):
of the user of this standard to establish appropriate safety and
3.1.1 Type I—Ethylene-Propylene-Diene Terpolymer
health practices and determine the applicability of regulatory
(EPDM).
limitations prior to use.
3.1.2 Type II—Chloroprene Polymer (CR).
2. Referenced Documents
NOTE 1—For definitions of polymer types, see Practice D 1418. For
2.1 ASTM Standards: definitions of terms related to roofing, see Terminology D 1079.
D 412 Test Methods for Rubber Properties in Tension
4. Materials and Manufacture
D 471 Test Methods for Rubber Property—Effect of Liq-
uids 4.1 The flashing material shall be formulated from the
appropriate polymer type and other compounding ingredients.
D 518 Test Method for Rubber Deterioration—Surface
Cracking The principal polymer in the flashing material shall be one of
those listed in 3.1 in accordance with proportions listed in 3.2
D 573 Test Methods for Rubber—Deterioration in Air
Oven and greater than 95% of the total polymer.
4.2 The flashing material shall be capable of being bonded
D 624 Test Methods for Rubber Property—Tear Resistance
D 1079 Terminology Relating to Roofing, Waterproofing, to itself, to the roofing membrane, and to substrate for making
watertight field splices and repairs. The manufacturer or
and Bituminous Materials
D 1149 Test Method for Rubber Deterioration—Surface fabricator shall recommend suitable bonding methods and
materials.
Ozone Cracking in a Chamber
5. Physical Requirements
5.1 Class V flashing material shall conform to the physical
This specification is under the jurisdiction of ASTM Committee D08 on
Roofing, Waterproofing, and Bituminous Materials and is the direct responsibility of
property requirements prescribed in Table 1 and Table 2. Class
Subcommittee D08.18 on Nonbituminous Organic Roof Coverings.
Current edition approved June 10, 1997. Published January 1998 Originally
published as D 4811 – 90. Last previous edition D 4811 – 90.
2 4
Annual Book of ASTM Standards, Vol 09.01. Annual Book of ASTM Standards, Vol 08.01.
3 5
Annual Book of ASTM Standards, Vol 04.04. Annual Book of ASTM Standards, Vol 14.02.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, United States.
NOTICE: This standard has either been superceded and replaced by a new version or discontinued.
Contact ASTM International (www.astm.org) for the latest information.
D4811–97
TABLE 1 Property Requirements for Flashing Before
7. Workmanship, Finish, and Appearance
Vulcanization
7.1 The flashing material shall be visually free of pinholes,
Type I Type II
particles of foreign matter, undispersed raw materials, or other
Thickness, min,
manufacturing defects that might affect serviceability.
in. (mm) 0.055 (1.4) 0.055 (1.4)
7.2 If the number of irregularities appear excessive on a
Green Strength
Modulus 100 %
sheet (or portion thereof), then its rejection should be negoti-
at 75°F (20°C)
ated between involved parties.
psi (kPa) 25–250 25–75
7.3 Edges of the sheet shall be capable of being seamed to
(172–1725) (172–517)
Elongation (Ultimate),
one another and to other roofing components without fish
min % 400 400
mouthing.
Modulus 100 %
at 122°F (50°C)
psi (kPa) 12 (83) 12 (83)
8. Test Methods
Elongation (Ultimate),
min, % 200 200 8.1 Thickness—Test Methods D 412.
Shelf Stability:
8.2 Green Strength:
Modulus 100 %
8.2.1 Test a fresh sample manufactured within one week.
at 75°F (20°C),
max, psi (kPa) 250 (1725) 250 (1725)
8.2.2 Condition Type I material at 73 6 4°F (23 6 2°C) for
Elongation, min,% 400 400
a minimum of 1 h and a maximum of 8 h before proceeding
Vulcanizability:
with the testing.
Tensile strength,
min, psi (kPa) 406 (2800) 406 (2800) 8.2.3 Decrystallize Type II material by placing in a circu-
Elongation, min % 400 400
lating air oven at 158 6 4°F (70 6 2°C) for 15 min. After
Tensile Set: min, % 80 80
removal from the oven, condition at 73 6 4°F (23 6 2°C) for
Dimensional Stability,
max, % 610 610
a minimum of 1 h and a maximum of 8 h before proceeding
Weatherability, no pass pass
with the testing.
cracks or crazing
8.2.4 After conditioning, die out a 0.5-in. (12.7-mm) dumb-
bell (Die A) and determine the modulus at 100 % extension and
the ultimate elongation at 73 6 4°F (23 6 2°C) in accordance
TABLE 2 Property Requirements for Flashing After Vulcanization
with Test Methods D 412.
Type I Type II
8.2.5 After conditioning, die out a 0.5 in. (12.7 mm)
Vulcanization, at 320°F (160°C), min 20 6220 6 2
dumbbell (Die A), condition in a circulating air oven at 122 6
Tensile Strength, min, psi (MPa) 1305 (9.0) 1205 (8.3)
Elongation, min, % 300 250
4°F (50 6 2°C) for 15 min minimum and 30 min maximum
Tear Resistance, min, lb/in. (kN/M) 125 (22) 125 (22)
and determine the modulus at 100 % extension and the ultimate
Brittle Point, max, °F (°C) −49 (−45) pass −31 (−35) pass
elongation at 1226 4°F (50 6 2°C) in accordance with Test
Tensile Set, max, % 10 10
Ozone Resistance, (73) no cracks no cracks
Methods D 412.
Heat Aging, Air Oven
8.3 Shelf Stability— Determine green strength in accor-
Tensile Strength, min, psi (MPa) 1205 (8.3) 1205 (8.3)
dance with 8.2 after aging in a circulating air oven for 46 h at
Elongation, min, % 200 200
Tear Resistance (Die C), lbf/in. (kN/m), 125 (22) 125 (22)
...

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