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ASTM E2242-21

(Test Method)

Standard Test Method for Column Percolation Extraction of Mine Rock by the Meteoric Water Mobility Procedure

Standard Test Method for Column Percolation Extraction of Mine Rock by the Meteoric Water Mobility Procedure

SIGNIFICANCE AND USE
5.1 This test method is intended as a means for obtaining an extract from mine rock samples. The extract may be used to estimate the final pH and release of certain constituents of the test sample under the laboratory conditions described in this test method.  
5.2 The pH of the extraction fluid used in this test method should reflect the pH of precipitation in the geographic region in which the mine rock is being evaluated.  
5.3 This test method is designed to mobilize potential contaminants present in the solids, so that the resulting extract can be used to assess leachate that could potentially be produced from mine rock in the field.  
5.4 This test method has not been demonstrated to simulate actual site leaching conditions.  
5.5 This test method produces extracts that are amenable to the determination of both major and minor (trace) constituents. When minor constituents are being determined, it is especially important that precautions be taken in sample preservation, storage, and handling to avoid possible contamination of the extracts.  
5.6 This test method is a comparative method intended for use as a routine method for monitoring mine rock. It is assumed that all who use this method will be trained analysts capable of performing skillfully and safely. It is expected that work will be performed in a properly equipped laboratory under appropriate quality control practices such as those described in Guide E882.
SCOPE
1.1 This test method provides a procedure for the column percolation extraction of mine rock in order to determine the potential for dissolution and mobility of certain constituents by meteoric water.  
1.2 This test method is intended to describe the procedure for performing column percolation extractions only. It does not describe all types of sampling and analytical requirements that may be associated with its application.  
1.3 The values stated in SI units are to be regarded as the standard. The values given in parentheses are provided for information only and are not considered standard.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

General Information

Status
Published
Publication Date
30-Sep-2021
ICS
73.060.01 - Metalliferous minerals in general
Technical Committee
E01 - Analytical Chemistry for Metals, Ores, and Related Materials
Drafting Committee
E01.02 - Ores, Concentrates, and Related Metallurgical Materials
Current Stage
Ref Project

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Standards Content (Sample)

This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the
Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
Designation: E2242 − 21
Standard Test Method for
Column Percolation Extraction of Mine Rock by the
1
Meteoric Water Mobility Procedure
This standard is issued under the fixed designation E2242; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision.Anumber in parentheses indicates the year of last reapproval.A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope CyanidewithFlowInjectionAnalysis(FIA)UtilizingGas
Diffusion Separation and Amperometric Detection
1.1 This test method provides a procedure for the column
E29Practice for Using Significant Digits in Test Data to
percolation extraction of mine rock in order to determine the
Determine Conformance with Specifications
potentialfordissolutionandmobilityofcertainconstituentsby
E50Practices for Apparatus, Reagents, and Safety Consid-
meteoric water.
erations for Chemical Analysis of Metals, Ores, and
1.2 This test method is intended to describe the procedure
Related Materials
forperformingcolumnpercolationextractionsonly.Itdoesnot
E135Terminology Relating to Analytical Chemistry for
describe all types of sampling and analytical requirements that
Metals, Ores, and Related Materials
may be associated with its application.
E389Test Method for Particle Size or Screen Analysis at
1.3 The values stated in SI units are to be regarded as the 4.75mm (No.4) Sieve and Coarser for Metal-Bearing
Ores and Related Materials
standard. The values given in parentheses are provided for
information only and are not considered standard. E691Practice for Conducting an Interlaboratory Study to
Determine the Precision of a Test Method
1.4 This standard does not purport to address all of the
E877Practice for Sampling and Sample Preparation of Iron
safety concerns, if any, associated with its use. It is the
Ores and Related Materials for Determination of Chemi-
responsibility of the user of this standard to establish appro-
cal Composition and Physical Properties
priate safety, health, and environmental practices and deter-
E882Guide for Accountability and Quality Control in the
mine the applicability of regulatory limitations prior to use.
Chemical Analysis Laboratory
1.5 This international standard was developed in accor-
E1601Practice for Conducting an Interlaboratory Study to
dance with internationally recognized principles on standard-
Evaluate the Performance of an Analytical Method
ization established in the Decision on Principles for the
2.2 Other References:
Development of International Standards, Guides and Recom-
Meteoric Water Mobility Procedure,Bureau of Mining
mendations issued by the World Trade Organization Technical
Regulation and Reclamation, Nevada Division of Envi-
Barriers to Trade (TBT) Committee.
ronmental Protection, 9/19/90
2. Referenced Documents
Standard Methods for the Examination of Water and Waste-
2
water,18th edition, APHA/AWWA/WEF, 1992
2.1 ASTM Standards:
D1193Specification for Reagent Water
3. Terminology
D1293Test Methods for pH of Water
D6234Test Method for Shake Extraction of Mining Waste 3.1 Definitions:
by the Synthetic Precipitation Leaching Procedure 3.1.1 For definitions of terms used in this test method, see
D7237Test Method for Free Cyanide and Aquatic Free Terminology E135.
3.1.2 meteoric water, n—rainfall that has the potential to
contact materials and mobilize soluble constituents from mine
1
This test method is under the jurisdiction of ASTM Committee E01 on
rock at a mining or mineral processing site.
Analytical Chemistry for Metals, Ores, and Related Materials and is the direct
responsibility of Subcommittee E01.02 on Ores, Concentrates, and Related Metal- 3.1.3 mine rock, n—ore, waste rock or overburden exca-
lurgical Materials.
vated in order to recover metals or minerals during mining
Current edition approved Oct. 1, 2021. Published October 2021. Originally
operations or coarse processed ore such as heap leach spoils.
approved in 2002. Last previous edition approved in 2013 as E2242–13. DOI:
10.1520/E2242-21.
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or 4. Summary of Test Method
contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
4.1 The test material is placed in a plastic column and
Standards volume information, refer to the standard’s Document Summary page on
the ASTM website. contactedwithwatertoproduceaneffluentcontaininganequal
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
1

---------------------- Page: 1 ----------------------
E2242 − 21
weight of solutio
...

This document is not an ASTM standard and is intended only to provide the user of an ASTM standard an indication of what changes have been made to the previous version. Because
it may not be technically possible to adequately depict all changes accurately, ASTM recommends that users consult prior editions as appropriate. In all cases only the current version
of the standard as published by ASTM is to be considered the official document.
Designation: E2242 − 13 E2242 − 21
Standard Test Method for
Column Percolation Extraction of Mine Rock by the
1
Meteoric Water Mobility Procedure
This standard is issued under the fixed designation E2242; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope
1.1 This test method provides a procedure for the column percolation extraction of mine rock in order to determine the potential
for dissolution and mobility of certain constituents by meteoric water.
1.2 This test method is intended to describe the procedure for performing column percolation extractions only. It does not describe
all types of sampling and analytical requirements that may be associated with its application.
1.3 The values stated in SI units are to be regarded as the standard. The values given in parentheses are provided for information
only and are not considered standard.
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility
of the user of this standard to establish appropriate safety safety, health, and healthenvironmental practices and determine the
applicability of regulatory limitations prior to use.
1.5 This international standard was developed in accordance with internationally recognized principles on standardization
established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued
by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
2. Referenced Documents
2
2.1 ASTM Standards:
D1193 Specification for Reagent Water
D1293 Test Methods for pH of Water
D6234 Test Method for Shake Extraction of Mining Waste by the Synthetic Precipitation Leaching Procedure
D7237 Test Method for Free Cyanide and Aquatic Free Cyanide with Flow Injection Analysis (FIA) Utilizing Gas Diffusion
Separation and Amperometric Detection
E29 Practice for Using Significant Digits in Test Data to Determine Conformance with Specifications
E50 Practices for Apparatus, Reagents, and Safety Considerations for Chemical Analysis of Metals, Ores, and Related Materials
E135 Terminology Relating to Analytical Chemistry for Metals, Ores, and Related Materials
E389 Test Method for Particle Size or Screen Analysis at 4.75 mm (No.4) Sieve and Coarser for Metal-Bearing Ores and Related
Materials
E691 Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method
1
This test method is under the jurisdiction of ASTM Committee E01 on Analytical Chemistry for Metals, Ores, and Related Materials and is the direct responsibility of
Subcommittee E01.02 on Ores, Concentrates, and Related Metallurgical Materials.
Current edition approved Oct. 1, 2013Oct. 1, 2021. Published November 2013October 2021. Originally approved in 2002. Last previous edition approved in 20122013
as E2242 – 12a.E2242 – 13. DOI: 10.1520/E2242-13.10.1520/E2242-21.
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM Standards
volume information, refer to the standard’s Document Summary page on the ASTM website.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
1

---------------------- Page: 1 ----------------------
E2242 − 21
E877 Practice for Sampling and Sample Preparation of Iron Ores and Related Materials for Determination of Chemical
Composition and Physical Properties
E882 Guide for Accountability and Quality Control in the Chemical Analysis Laboratory
E1601 Practice for Conducting an Interlaboratory Study to Evaluate the Performance of an Analytical Method
2.2 Other References:
Meteoric Water Mobility Procedure, Bureau of Mining Regulation and Reclamation, Nevada Division of Environmental
Protection, 9/19/90
Standard Methods for the Examination of Water and Wastewater, 18th edition, APHA/AWWA/WEF, 1992
3. Terminology
3.1 Definitions:
3.1.1 For definitions of terms used in this test method, see Terminology E135.
3.1.2 meteoric water—water, n—rainfall that has the potential to contact materials and mobilize soluble constituents from mine
rock at a mining or mineral processing site.
3.1.3 mine rock—rock, n—ore, waste rock or overburden excavated in order to recover metals or min
...

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SIGNIFICANCE AND USE
4.1 These practices are primarily intended to test materials for compliance with compositional specifications and for monitoring. Partial extraction of ores and related metallurgical materials can provide information on the availability of elements to leaching, water quality changes, or other site conditions.  
4.2 It is assumed that the users of these practices will be trained analysts capable of performing common laboratory procedures skillfully and safely. It is expected that work will be performed in a properly equipped laboratory and that proper waste disposal procedures will be followed. Appropriate quality control practices such as those described in Guide E882 shall be followed.
SCOPE
1.1 These practices cover the digestion of ores and related metallurgical materials, such as mine soil, waste rock and tailings, for subsequent determination of acid-extractable contents of certain elements by such solution analytical techniques as atomic absorption spectrometry (AAS), inductively coupled plasma atomic emission spectrometry (ICP-AES) (see Test Method D1976), and inductively coupled plasma mass spectrometry (ICP-MS) (see Test Method D5673).  
1.1.1 Contents of aluminum, antimony, arsenic, barium, beryllium, bismuth, boron, cadmium, calcium, chromium, cobalt, copper, gallium, iron, lead, lithium, magnesium, manganese, mercury, molybdenum, nickel, phosphorus, potassium, scandium, selenium, silver, sodium, strontium, thallium, tin, titanium, vanadium and zinc can be extracted from ores and related metallurgical materials for determination by analytical methods for elements in solution. Other elements may be determined from extracts produced using this practice.  
1.1.2 Actual element quantification in digested solutions can be accomplished by following the various test methods under other appropriate ASTM standards for element(s) of interest in solution.  
1.1.3 The detection limit and linear content range for each element is dependent on the atomic absorption, mass spectrometry or emission spectrometric technique employed and may be found in the manual accompanying the instrument used or ASTM standard method for analysis of the solutions. Consider the dilution factor in content calculations due to digestion and dilution of solid samples.  
1.1.4 The extent of extraction of elements from ores and related metallurgical materials by these practices is dependent upon the physical and mineralogical characteristics of the prepared sample and the digestion practice used.  
1.2 The digestion practices appear in the following order:    
Sections  
Nitric Acid Microwave Digestion  
7 to 14  
Four-Acid Total Digestion  
15 to 21  
1.3 The values stated SI units are to be regarded as the standard. No other units of measurements are included in this standard.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. For specific hazard statements, see Sections 11 and 20.  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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ASTM
ASTM A370-23(Test Method)
Standard Test Methods and Definitions for Mechanical Testing of Steel Products

SIGNIFICANCE AND USE
4.1 The primary use of these test methods is testing to determine the specified mechanical properties of steel, stainless steel, and related alloy products for the evaluation of conformance of such products to a material specification under the jurisdiction of ASTM Committee A01 and its subcommittees as designated by a purchaser in a purchase order or contract.  
4.1.1 These test methods may be and are used by other ASTM Committees and other standards writing bodies for the purpose of conformance testing.  
4.1.2 The material condition at the time of testing, sampling frequency, specimen location and orientation, reporting requirements, and other test parameters are contained in the pertinent material specification or in a general requirement specification for the particular product form.  
4.1.3 Some material specifications require the use of additional test methods not described herein; in such cases, the required test method is described in that material specification or by reference to another appropriate test method standard.  
4.2 These test methods are also suitable to be used for testing of steel, stainless steel and related alloy materials for other purposes, such as incoming material acceptance testing by the purchaser or evaluation of components after service exposure.  
4.2.1 As with any mechanical testing, deviations from either specification limits or expected as-manufactured properties can occur for valid reasons besides deficiency of the original as-fabricated product. These reasons include, but are not limited to: subsequent service degradation from environmental exposure (for example, temperature, corrosion); static or cyclic service stress effects, mechanically-induced damage, material inhomogeneity, anisotropic structure, natural aging of select alloys, further processing not included in the specification, sampling limitations, and measuring equipment calibration uncertainty. There is statistical variation in all aspects of mechanical testin...
SCOPE
1.1 These test methods2 cover procedures and definitions for the mechanical testing of steels, stainless steels, and related alloys. The various mechanical tests herein described are used to determine properties required in the product specifications. Variations in testing methods are to be avoided, and standard methods of testing are to be followed to obtain reproducible and comparable results. In those cases in which the testing requirements for certain products are unique or at variance with these general procedures, the product specification testing requirements shall control.  
1.2 The following mechanical tests are described:    
Sections  
Tension  
7 to 14  
Bend  
15  
Hardness  
16  
Brinell  
17  
Rockwell  
18  
Portable  
19  
Impact  
20 to 30  
Keywords  
32  
1.3 Annexes covering details peculiar to certain products are appended to these test methods as follows:    
Annex  
Bar Products  
Annex A1  
Tubular Products  
Annex A2  
Fasteners  
Annex A3  
Round Wire Products  
Annex A4  
Significance of Notched-Bar Impact Testing  
Annex A5  
Converting Percentage Elongation of Round Specimens to
Equivalents for Flat Specimens  
Annex A6    
Testing Multi-Wire Strand  
Annex A7  
Rounding of Test Data  
Annex A8  
Methods for Testing Steel Reinforcing Bars  
Annex A9  
Procedure for Use and Control of Heat-cycle Simulation  
Annex A10  
1.4 The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard.  
1.5 When these test methods are referenced in a metric product specification, the yield and tensile values may be determined in inch-pound (ksi) units then converted into SI (MPa) units. The elongation determined in inch-pound gauge lengths of 2 in. or 8 in. may be report...

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ASTM
ASTM F3565-23(Practice)
Standard Practice for Electrofusion Joining Polyethylene (PE) Pipe and Fittings for Pressure Pipe Service

SIGNIFICANCE AND USE
4.1 Using the procedures and apparatus in Sections 8 and 9 and the manufacturer's instructions, pressure-tight joints as strong as the pipe itself can be made between manufacturer-recommended combinations of pipe and fittings. See Specification F1055 for performance requirements of polyethylene electrofusion fittings.
SCOPE
1.1 This practice describes procedures for making joints suitable for pressure service with polyethylene (PE) pipe and fittings by means of electrofusion joining techniques in, but not limited to, a field environment. Other suitable electrofusion joining procedures are available from various sources including fitting manufacturers. This standard does not purport to address all possible electrofusion joining procedures, or to preclude the use of qualified procedures developed by other parties that have been proven to produce reliable electrofusion joints. (Note 1)
Note 1: Reference to the manufacturer in this practice refers to the electrofusion fitting manufacturer.  
1.2 The parameters and procedure are applicable only to joining polyethylene pipe and fittings (Note 2) which are intended for PE fuel gas pipe per Specification D2513 and PE potable water, sewer and industrial pipe manufactured per Specification F714, Specification D3035, Specification F2619, and AWWA C901 and C906.
Note 2: Commercially available materials classified with a thermoplastic pipe material designation code beginning with PE 14, PE 23, PE 24, PE 27, PE 33, PE 34, PE 36, and PE 46, and PE 47 in accordance with Specification D3350 and Terminology F412 are generally acceptable for electrofusion joining using this practice. Consult with the pipe or fitting manufacturer for specific compatibility information.  
1.3 Parts that are within the dimensional tolerances given in present ASTM specifications are required to produce sound joints between polyethylene pipe and fittings when using the joining techniques described in this practice.  
1.4 The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard.  
1.5 The text of this practice references notes, footnotes, and appendices which provide explanatory material. These notes and footnotes (excluding those in tables and figures) shall not be considered as requirements of the practice.  
1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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