Standard Practice for Evaluation of Limestone or Lime Uniformity From a Single Source

SIGNIFICANCE AND USE
4.1 This practice is designed to present in a standardized format information on the variability of limestone or lime from a single source over a period of time. It can be applied to all materials covered in Test Methods C25, C110, C1271, and C1301, and Specification C141.
SCOPE
1.1 This practice is intended for use in instances where the purchaser desires information on the uniformity of limestone or lime produced at a single source. It is intended that this test method normally be used for the predominant material manufactured at a plant. Guidelines for sampling, testing and presentation of results (Table 1) are given.  
1.2 The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

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NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
Designation: C1164 − 14
Standard Practice for
Evaluation of Limestone or Lime Uniformity From a Single
1
Source
This standard is issued under the fixed designation C1164; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope* stone and Lime by Inductively Coupled Plasma-Atomic
Emission Spectroscopy (ICP) and Atomic Absorption
1.1 This practice is intended for use in instances where the
(AA)
purchaserdesiresinformationontheuniformityoflimestoneor
lime produced at a single source. It is intended that this test
3. Terminology
method normally be used for the predominant material manu-
factured at a plant. Guidelines for sampling, testing and 3.1 Definitions:
presentation of results (Table 1) are given. 3.1.1 Fordefinitionsoftermsrelatingtothispracticereferto
Terminology C51.
1.2 The values stated in inch-pound units are to be regarded
as standard. The values given in parentheses are mathematical
4. Significance and Use
conversions to SI units that are provided for information only
4.1 This practice is designed to present in a standardized
and are not considered standard.
format information on the variability of limestone or lime from
1.3 This standard does not purport to address all of the
a single source over a period of time. It can be applied to all
safety concerns, if any, associated with its use. It is the
materials covered in Test Methods C25, C110, C1271, and
responsibility of the user of this standard to establish appro-
C1301, and Specification C141.
priate safety and health practices and determine the applica-
bility of regulatory limitations prior to use.
5. Sampling
2. Referenced Documents
5.1 The sampling shall be done in accordance with Methods
2
C50.
2.1 ASTM Standards:
C25 Test Methods for Chemical Analysis of Limestone,
5.2 All sampling shall be performed by personnel qualified
Quicklime, and Hydrated Lime
by specific training for this purpose.
C50 Practice for Sampling, Sample Preparation, Packaging,
5.3 Datapointsshallbeanaverageofthreeormoreseparate
and Marking of Lime and Limestone Products
determinationsrelativetoaspecifiedunitoftime.Forexample:
C51 Terminology Relating to Lime and Limestone (as used
(1) n determinations for daily average, (2) daily determinations
by the Industry)
for weekly average.
C110 Test Methods for Physical Testing of Quicklime,
5.4 The samples shall be identified by the date or dates that
Hydrated Lime, and Limestone
the represented material was obtained.
C141 Specification for Hydraulic Hydrated Lime for Struc-
tural Purposes
6. Procedure
C1271 Test Method for X-ray Spectrometric Analysis of
Lime and Limestone
6.1 The minimum amount of testing (see 5.3) and the type
C1301 Test Method for Major and Trace Elements in Lime-
of test(s) to be performed should be agreed upon by the
purchaser and producer.
1
NOTE 1—A single daily analysis does not necessarily characterize a
This practice is under the jurisdiction of ASTM Committee C07 on Lime and
product. A minimum of three analyses is more reasonable.
Limestone and is the direct responsibility of Subcommittee C07.02 on Specifica-
tions and Guidelines.
6.2 It is desirable that all tests used in a single evaluation be
Current edition approved Dec. 1, 2014. Published December 2014. Originally
performed in the same laboratory, preferably by the same
approved in 1990. Last previous edition approved in 2009 as C1164 – 92 (2009).
DOI: 10.1520/C1164-14.
person, in order for the results to be comparable.
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or
NOTE 2—In order to obtain comparable results when exchanging
contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
Standards volume information, refer to the standard’s Document Summary page on samples between laboratories, methods used in preparation, handling and
the ASTM website. storage of those samples must be uniform.
*A Summary of Changes section appears at the end of this standard
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
1

---------------------- Page: 1 ----------------------
C1164 − 14
TABLE 1 High Calcium Quicklime January 1989
7.2 The physical analysis of quicklime, hydrated lime, and
limestoneshallbedeterminedinaccordancewithTestMethods
NOTE 1—This data is presented only as a sample of the correct method
C110.
for presentation. Other tests can be substituted and others omitted.
Test
7.3 The analysis of hydraulic hydrated lime shall be deter-
Day
Acid Insoluble % CaO % MgO Available CaO
mined in accordance with Specification C141.
1 0.66 95.85 2.
...

This document is not an ASTM standard and is intended only to provide the user of an ASTM standard an indication of what changes have been made to the previous version. Because
it may not be technically possible to adequately depict all changes accurately, ASTM recommends that users consult prior editions as appropriate. In all cases only the current version
of the standard as published by ASTM is to be considered the official document.
Designation: C1164 − 92 (Reapproved 2009) C1164 − 14
Standard Practice for
Evaluation of Limestone or Lime Uniformity From a Single
1
Source
This standard is issued under the fixed designation C1164; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope Scope*
1.1 This practice is intended for use in instances where the purchaser desires information on the uniformity of limestone or lime
produced at a single source. It is intended that this test method normally be used for the predominant material manufactured at a
plant. Guidelines for sampling, testing and presentation of results (Table 1) are given.
1.2 The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical
conversions to SI units that are provided for information only and are not considered standard.
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility
of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory
limitations prior to use.
2. Referenced Documents
2
2.1 ASTM Standards:
C25 Test Methods for Chemical Analysis of Limestone, Quicklime, and Hydrated Lime
C50 Practice for Sampling, Sample Preparation, Packaging, and Marking of Lime and Limestone Products
C51 Terminology Relating to Lime and Limestone (as used by the Industry)
C110 Test Methods for Physical Testing of Quicklime, Hydrated Lime, and Limestone
C141 Specification for Hydraulic Hydrated Lime for Structural Purposes
C1271 Test Method for X-ray Spectrometric Analysis of Lime and Limestone
C1301 Test Method for Major and Trace Elements in Limestone and Lime by Inductively Coupled Plasma-Atomic Emission
Spectroscopy (ICP) and Atomic Absorption (AA)
3. Terminology
3.1 Definitions:
3.1.1 For definitions of terms relating to this practice refer to Terminology C51.
4. Significance and Use
4.1 This practice is designed to present in a standardized format information on the variability of limestone or lime from a single
source over a period of time. It can be applied to all materials covered in Test Methods C25 and , C110, C1271, and C1301, and
Specification C141.
5. Sampling
5.1 The sampling shall be done in accordance with Methods C50.
5.2 All sampling shall be performed by personnel qualified by specific training for this purpose.
5.3 Data points shall be an average of three or more separate determinations relative to a specified unit of time. For example:
(1) n determinations for daily average, (2) daily determinations for weekly average.
1
This practice is under the jurisdiction of ASTM Committee C07 on Lime and Limestone and is the direct responsibility of Subcommittee C07.02 on Specifications and
Guidelines.
Current edition approved Dec. 1, 2009Dec. 1, 2014. Published May 2010December 2014. Originally approved in 1990. Last previous edition approved in 20032009 as
C1164 – 92 (2003).(2009). DOI: 10.1520/C1164-92R09.10.1520/C1164-14.
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM Standards
volume information, refer to the standard’s Document Summary page on the ASTM website.
*A Summary of Changes section appears at the end of this standard
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
1

---------------------- Page: 1 ----------------------
C1164 − 14
TABLE 1 High Calcium Quicklime January 1989
NOTE 1—This data is presented only as a sample of the correct method
for presentation. Other tests can be substituted and others omitted.
Test
Day
Acid Insoluble % CaO % MgO Available CaO
1 0.66 95.85 2.27 94.90
2 0.84 95.03 2.87 94.08
3 1.24 95.85 1.57 94.90
4 1.22 96.67 1.49 95.71
5 1.22 96.26 1.32 95.31
8 0.68 95.85 2.06 94.69
9 0.96 95.54 2.27 94.89
10 1.26 96.15 1.74 95.20
11 1.04 96.04 2.00 95.11
13 1.26 96.26 1.51 95.31
15 1.34 95.23 2.09 94.28
16 1.28 95.44 2.34 94.69
19 0.68 96.15 1.46 95.20
20 1.42 95.85 1.27 94.90
22 1.06 95.85 1.86 94.90
23 0.58 96.15 2.09 95.31
24 0.84 95.03 2.61 94.08
26 1.28 95.64 1.39 94.69
27 1.48 95.54 1.58 94.39
29 0.98 94.82 2.71 93.67
30 1.24 94.41 3.42 93.67
Avg 1.07 95.70 2.00 94.76
Range 0.90 2.26 2.15 2.
...

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