ASTM D7116-05
(Specification)Standard Specification for Joint Sealants, Hot Applied, Jet Fuel Resistant Types, for Portland Cement Concrete Pavements (Withdrawn 2012)
Standard Specification for Joint Sealants, Hot Applied, Jet Fuel Resistant Types, for Portland Cement Concrete Pavements (Withdrawn 2012)
ABSTRACT
This specification covers joint and crack sealants of the hot applied, jet fuel resistant type intended for use in sealing joints and cracks in Portland cement concrete in areas that are subject to fuel spillage. Three types of joint sealants are presented: type I - joint sealant which is resilient and capable of maintaining an effective seal in hot to moderate climates, type II - joint sealant capable of maintaining an effective seal in hot to moderate climates, and type III - joint sealant capable of maintaining an effective seal in most climates experiencing moderate to cold temperatures. The specimen conditioning, cone penetration, aged cone penetration retention, and softening point shall be tested to meet the requirements prescribed. Non-immersed bond, water immersed bond, fuel immersed bond, resilience, and oven aged resilience shall be tested to meet the requirements prescribed. The tensile adhesion, artificial weathering, and flexibility of the sealant shall be tested to meet the requirements prescribed.
SCOPE
1.1 This specification covers joint and crack sealants of the hot applied type intended for use in sealing joints and cracks in portland cement concrete in areas that are subject to fuel spillage.
1.2 The values stated in SI units are to be regarded as the standard.
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory requirements prior to use.
WITHDRAWN RATIONALE
Formerly under the jurisdiction of Committee D04 on Road and Paving Materials, this test method was withdrawn in December 2012. This standard is being withdrawn without replacement due to its limited use by industry.
General Information
Standards Content (Sample)
NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
Designation:D7116 −05
StandardSpecification for
Joint Sealants, Hot Applied, Jet Fuel Resistant Types, for
Portland Cement Concrete Pavements
This standard is issued under the fixed designation D7116; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision.Anumber in parentheses indicates the year of last reapproval.A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope 3. General Requirements
1.1 This specification covers joint and crack sealants of the
3.1 The sealant, when in place, shall form a resilient and
hotappliedtypeintendedforuseinsealingjointsandcracksin
cohesivecompoundthatshalleffectivelysealjointsinconcrete
portland cement concrete in areas that are subject to fuel
throughout repeated cycles of expansion and contraction, and
spillage.
againsttheinfiltrationofmoisture,fueland,incompressibles.It
shall not, at ambient temperatures, flow from the joint or be
1.2 The values stated in SI units are to be regarded as the
picked up by vehicle tires. The material shall be capable of
standard.
being brought to a uniform pouring consistency suitable for
1.3 This standard does not purport to address all of the
completelyfillingthejointswithoutinclusionoflargeairholes
safety concerns, if any, associated with its use. It is the
or discontinuities and without damage to the material. It shall
responsibility of the user of this standard to establish appro-
remain relatively unchanged in application characteristics for
priate safety and health practices and determine the applica-
at least6hatthe recommended application temperature in the
bility of regulatory requirements prior to use.
field.
2. Referenced Documents
4. Classification
2.1 ASTM Standards:
D36TestMethodforSofteningPointofBitumen(Ring-and- 4.1 Type I—Ajoint sealant which is resilient and capable of
Ball Apparatus)
maintaining an effective seal in hot to moderate climates.
D3569 Specification for Joint Sealant, Hot-Applied, Material is tested for low temperature performance at -18°C
Elastomeric, Jet-Fuel-Resistant-Type for Portland Cement
using 50% extension (see Specification D3569).
Concrete Pavements (Withdrawn 2006)
4.2 Type II—A joint sealant capable of maintaining an
D5167Practice for Melting of Hot-Applied Joint and Crack
effectivesealinhottomoderateclimates.Materialistestedfor
Sealant and Filler for Evaluation
low temperature performance at -18°C using 50% extension.
D5249Specification for Backer Material for Use with Cold-
Special tests are included (see Federal Spec SS-S-1614A).
and Hot-Applied Joint Sealants in Portland-Cement Con-
crete and Asphalt Joints
4.3 Type III—A joint sealant capable of maintaining an
D5329Test Methods for Sealants and Fillers, Hot-Applied, effective seal in most climates experiencing moderate to cold
for Joints and Cracks in Asphaltic and Portland Cement temperatures. Material is tested for low temperature perfor-
Concrete Pavements mance at -29°C using 50% extension.
2.2 Federal Specification
NOTE 1—It is the responsibility of the user agency to determine which
SS-S-1614A
type is most applicable to their conditions.
5. Physical Requirements
This specification is under the jurisdiction ofASTM Committee D04 on Road
and Paving Materials and is the direct responsibility of Subcommittee D04.33 on
5.1 Maximum Heating Temperature—The maximum heat-
Formed In-Place Sealants for Joints and Cracks in Pavements.
Current edition approved Dec. 1, 2005. Published December 2005. DOI:
ing temperature is the highest temperature to which a sealant
10.1520/D7116-05.
can be heated, and still conform to all the requirements
For referenced ASTM standards, visit the ASTM website, www.astm.org, or
specified herein. For purposes of testing as specified
contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
hereinafter,theapplicationtemperatureshallbethesameasthe
Standards volume information, refer to the standard’s Document Summary page on
the ASTM website.
maximum heating temperature. The maximum heating tem-
The last approved version of this historical standard is referenced on
perature shall be set forth by the manufacturer, shall be shown
www.astm.org.
on all containers and shall be provided to the testing agency
AvailablefromU.S.GovernmentPrintingOfficeSuperintendentofDocuments,
732 N. Capitol St., NW, Mail Stop: SDE, Washington, DC 20401. before any laboratory tests are begun. The maximum heating
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
D7116−05
temperature shall be a minimum of 11°C higher than the D5329priortobeginninganytesting.Thetimeofconditioning
manufacturer’s recommended application temperature. shall be as specified in Table 1.
5.2 The preparation requirements for each sealant are listed
7.2 Cone Penetration—Determine cone penetration accord-
in Table 1.
ing to Test Methods D5329 for Cone Penetration, non-
immersed.
5.3 Sealant shall conform to the requirements prescribed in
Table 2.
7.3 Cone Penetration, Fuel Immersed—Use Test Methods
D5329.
6. Sampling and Heating
7.4 Aged Cone Penetration Retention—Use Test Methods
6.1 Sampling:
D5329 except as stated below.
6.1.1 Samples may be taken at the plant or warehouse prior
7.4.1 After conditioning, the specimen shall be placed in a
to delivery or at the time of delivery, at the option of the
forced draft oven maintained at 70 6 1 C for 72 61h
purchaser. If sampling is done prior to shipment, the inspector
uncovered.
representingthepurchasershallhavefreeaccesstothematerial
7.4.2 The specimen shall then be removed from the oven
to be sampled. The inspector shall be afforded all reasonable
and conditioned at standard laboratory conditions for 1 hour
facilitiesforinspectionandsamplingwhichshallbeconducted
followed by conditioning in a 25 6 0.1 C bath for 1 to 1 ⁄2 h.
so as not to interfere unnecessarily with the operation of the
7.4.3 Test for cone penetration and determine result.This is
works.
the aged cone penetration
6.1.2 Samples shall consist of one of the manufacturer’s
7.4.4 Determine the aged cone penetration retention using
original sealed containers selected at random from the lot or
the following formula:
batch of finished material.Abatch or lot shall be considered as
all finished material that was manufactured simultaneously or
AgedConePenetration
AgedConePenetrationRetention% 5 3100
continuously as a unit between the time of compounding and
ConePenetration
the time of packaging or placing in shipping containers.
(1)
6.1.3 Obtainthesealantportionfortestingfromtheselected
7.5 Determine the Softening PointAccording to Test Meth-
manufacturer’s original sealed container in accordance with
ods D36.
PracticeD5167.Thesampleportionaddedtoandheatedinthe
melter shall weigh as specified in Table 1. Both pots of the
7.6 Bond, Non-Immersed—Determinethebondaccordingto
melter described in Practice D5167 shall be used for samples
Test Methods D 5329D5329 for bond, non-immersed.
exceeding 1250 g and each pot shall contain at least 625 g but
7.6.1 After final scrubbing and blotting specified in Test
not more than 850 g.
Methods D5329, air dry the blocks on their 25.4 mm × 50.8
mm ends at standard laboratory conditions for 1 h 6 10 min.
6.2 Heating—Heat the material in accordance with Practice
prior to pouring bond specimens.
D5167.
6.2.1 The oil bath in the melter shall be heated to a 7.6.2 Immediately after drying the blocks as in 7.6.1,
temperature between the sealant’s maximum heating tempera- assemble the blocks with spacers as specified in Test Methods
ture and 20°C above the sealant’s maximum heating tempera- D5329 so the opening between the blocks will form a cured
ture. (Never allow the oil temperature to exceed 288°C). Add sealant block that is 12.7 6 0.1 mm wide
the sealant to the melter according to the instructions in
7.6.3 After pouring material into the block opening, condi-
PracticeD5167.Afterthesamplehasbeenaddedtothemelter,
tionthespecimenasin7.1.Afterconditioning,removespacers
regulatetheoiltemperaturewithinthelistedtemperaturelimits
and trim off excess material with a hot knife being careful not
while raising the sealant’s temperature to manufacturer’s
topullsealantfromtheblock.Conditionthetestspecimensnot
recommended maximum heating temperature within the re-
less than4hatthe temperature specified in Table 2 for the
quired1houroftime,asstatedinPracticeD5167.Theheating
specific type of sealant. Immediately extend the specimen to
time for each type of sealant as well as the start of the heating
the prescribed percentage in Table 2 using the apparatus and
time shall be as specified in Table 1.
rate described in Test Methods D5329.
7.6.4 Recompress and re-extend according to Test Methods
7. Test Methods
D5329forthetotalnumberofcyclesprescribedinTable2.The
7.1 Specimen Conditioning—Condition all specimens at required cycles shall be completed within a 5 day period from
standard laboratory conditions as specified in Test Method the time of pouring.
TABLE 1 Preparation Requirements
Type I Type II Type III
Sample Size 2550 ± 50 g 1600 ± 50 g 1600 ± 50 g
Start and Duration of 6 h from the start of 3 h fro
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