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ASTM C760-90(2020)

(Test Method)

Standard Test Methods for Chemical and Spectrochemical Analysis of Nuclear-Grade Silver-Indium-Cadmium Alloys

Standard Test Methods for Chemical and Spectrochemical Analysis of Nuclear-Grade Silver-Indium-Cadmium Alloys

SIGNIFICANCE AND USE
3.1 Silver-indium-cadmium alloy is used as a control material in nuclear reactors. In order to be suitable for this purpose, the material must meet the specifications for assay and impurity content. These test methods are designed to show whether or not a given material meets the specifications as given in Specification C752.  
3.1.1 An assay is performed to determine whether the material has the chemical composition specified.  
3.1.2 The impurity content is determined to ensure that the maximum concentration limit of impurities is not exceeded.
SCOPE
1.1 These test methods cover procedures for the chemical and spectrochemical analysis of nuclear grade silver-indium-cadmium (Ag-In-Cd) alloys to determine compliance with specifications.  
1.2 The analytical procedures appear in the following order:    
Sections  
Silver, Indium, and Cadmium by a Titration Method  
7 – 15  
Trace Impurities by Carrier-Distillation Spectro-
chemical Method  
16 – 22  
1.3 The values stated in SI units are to be regarded as the standard.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. For specific hazard and precautionary statements, see Section 5 and Practices E50.  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

General Information

Status
Published
Publication Date
31-Dec-2019
ICS
77.040.30 - Chemical analysis of metals
Technical Committee
C26 - Nuclear Fuel Cycle
Drafting Committee
C26.03 - Neutron Absorber Materials Specifications
Current Stage
Ref Project

Relations

Replaces
ASTM C760-90(2015) - Standard Test Methods for Chemical and Spectrochemical Analysis of Nuclear-Grade Silver-Indium-Cadmium Alloys
Effective Date
01-Jan-2020
Refers
ASTM E50-11(2016) - Standard Practices for Apparatus, Reagents, and Safety Considerations for Chemical Analysis of Metals, Ores, and Related Materials
Effective Date
01-Aug-2016
Refers
ASTM E50-17 - Standard Practices for Apparatus, Reagents, and Safety Considerations for Chemical Analysis of Metals, Ores, and Related Materials
Effective Date
01-Sep-2017
Refers
ASTM C752-13(2016) - Standard Specification for Nuclear-Grade Silver-Indium-Cadmium Alloy
Effective Date
01-Apr-2016
Refers
ASTM C752-18 - Standard Specification for Nuclear-Grade Silver-Indium-Cadmium Alloy
Effective Date
01-Jun-2018

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ASTM C760-90(2020) - Standard Test Methods for Chemical and Spectrochemical Analysis of Nuclear-Grade Silver-Indium-Cadmium AlloysASTM C760-90(2020) - Standard Test Methods for Chemical and Spectrochemical Analysis of Nuclear-Grade Silver-Indium-Cadmium Alloys
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ASTM C760-90(2020) - Standard Test Methods for Chemical and Spectrochemical Analysis of Nuclear-Grade Silver-Indium-Cadmium Alloys
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This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the
Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
Designation: C760 − 90 (Reapproved 2020)
Standard Test Methods for
Chemical and Spectrochemical Analysis of Nuclear-Grade
1
Silver-Indium-Cadmium Alloys
This standard is issued under the fixed designation C760; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision.Anumber in parentheses indicates the year of last reapproval.A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope erations for Chemical Analysis of Metals, Ores, and
Related Materials
1.1 These test methods cover procedures for the chemical
E115Practice for Photographic Processing in Optical Emis-
and spectrochemical analysis of nuclear grade silver-indium-
3
sion Spectrographic Analysis (Withdrawn 2002)
cadmium (Ag-In-Cd) alloys to determine compliance with
specifications. 2.2 Other Document:
4
NBS Circular 602
1.2 Theanalyticalproceduresappearinthefollowingorder:
Sections
3. Significance and Use
Silver, Indium, and Cadmium by a Titration Method 7–15
Trace Impurities by Carrier-Distillation Spectro- 16–22
3.1 Silver-indium-cadmium alloy is used as a control mate-
chemical Method
rial in nuclear reactors. In order to be suitable for this purpose,
1.3 The values stated in SI units are to be regarded as the
the material must meet the specifications for assay and impu-
standard.
rity content. These test methods are designed to show whether
1.4 This standard does not purport to address all of the
or not a given material meets the specifications as given in
safety concerns, if any, associated with its use. It is the
Specification C752.
responsibility of the user of this standard to establish appro-
3.1.1 An assay is performed to determine whether the
priate safety, health, and environmental practices and deter-
material has the chemical composition specified.
mine the applicability of regulatory limitations prior to use.
3.1.2 The impurity content is determined to ensure that the
Forspecifichazardandprecautionarystatements,seeSection5
maximum concentration limit of impurities is not exceeded.
and Practices E50.
1.5 This international standard was developed in accor-
4. Purity of Reagents
dance with internationally recognized principles on standard-
ization established in the Decision on Principles for the
4.1 Reagent grade chemicals shall be used in all tests.
Development of International Standards, Guides and Recom-
Unlessotherwiseindicated,itisintendedthatallreagentsshall
mendations issued by the World Trade Organization Technical
conform to the specifications of the Committee on Analytical
5
Barriers to Trade (TBT) Committee.
Reagents of the American Chemical Society, where such
specifications are available. Other grades may be used, pro-
2. Referenced Documents
vided it is first ascertained that the reagent is of sufficiently
2
2.1 ASTM Standards: high purity to permit its use without lessening the accuracy of
the determination.
C752 Specification for Nuclear-Grade Silver-Indium-
Cadmium Alloy
4.2 Purity of Water—Unless otherwise indicated, references
D1193Specification for Reagent Water
towatershallbeunderstoodtomeanreagentwaterconforming
E50Practices for Apparatus, Reagents, and Safety Consid-
to Specification D1193.
1
These test methods are under the jurisdiction of ASTM Committee C26 on
3
Nuclear Fuel Cycle and are the direct responsibility of Subcommittee C26.03 on The last approved version of this historical standard is referenced on
Neutron Absorber Materials Specifications. www.astm.org.
4
Current edition approved Jan. 1, 2020. Published January 2020. Originally Available from National Institute of Standards and Technology (NIST), 100
approved in 1971. Last previous edition approved in 2015 as C760–90(2015). Bureau Dr., Stop 1070, Gaithersburg, MD 20899-1070, http://www.nist.gov.
5
DOI: 10.1520/C0760-90R20. Reagent Chemicals, American Chemical Society Specifications, American
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or Chemical Society, Washington, DC. For suggestions on the testing of reagents not
contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM listed by the American Chemical Society, see Analar Standards for Laboratory
Standards volume information, refer to the standard’s Document Summary page on Chemicals,BDHLtd.,Poole,Dorset,U.K.andthe United States Pharmacopeia and
the ASTM website. National Formulary,U.S.PharmacopeialConvention,Inc.(USPC),Rockville,MD.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
1

---------------------- Page: 1 ----------------------
C760 − 90 (2020)
...

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ASTM E439-23(Test Method)
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4.1 These test methods for the chemical analysis of beryllium metal are primarily intended as referee methods to test such materials for compliance with compositional specifications. It is assumed that all who use these test methods will be trained analysts capable of performing common laboratory procedures skillfully and safely. It is expected that work will be performed in a properly equipped laboratory.
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1.1 These test methods cover the chemical analysis of beryllium having chemical compositions within the following limits:    
Element  
Range, %  
Aluminum  
0.05 to 0.30  
Beryllium  
97.5 to 100    
Beryllium Oxide  
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Carbon  
0.05 to 0.30  
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Iron  
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Magnesium  
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Nickel  
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Silicon  
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Sections  
Chromium by the Diphenylcarbazide Spectrophotometric Test Method
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10 – 19  
Iron by the 1,10-Phenanthroline Spectrophotometric Test Method
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ASTM E363-23(Test Method)
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SIGNIFICANCE AND USE
4.1 These test methods for the chemical analysis of chromium metal and ferrochromium alloy are primarily intended to test such materials for compliance with compositional specifications such as Specifications A101 and A481. It is assumed that all who use these test methods will be trained analysts capable of performing common laboratory procedures skillfully and safely. It is expected that work will be performed in a properly equipped laboratory.
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Element  
Composition, %  
Aluminum  
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Antimony  
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Arsenic  
0.005 max  
Bismuth  
0.005 max  
Boron  
0.005 max  
Carbon  
9.00 max  
Chromium  
51.0 to 99.5  
Cobalt  
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Columbium  
0.05 max  
Copper  
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Lead  
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Molybdenum  
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Nickel  
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Nitrogen  
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Phosphorus  
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Silicon  
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Silver  
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Sulfur  
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Tantalum  
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Tin  
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Titanium  
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Vanadium  
0.50 max  
Zinc  
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Zirconium  
0.05 max  
1.2 The analytical procedures appear in the following order:    
Sections  
Arsenic by the Molybdenum Blue Spectrophotometric Test Method
[0.001 % to 0.005 %]  
10 – 20  
Lead by the Dithizone Spectrophotometric Test Method
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21 – 31  
Chromium by the Sodium Peroxide Fusion-Titrimetric Test Method
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SIGNIFICANCE AND USE
4.1 This practice is intended primarily for the sampling of copper and copper alloys for compliance with compositional specification requirements.  
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SCOPE
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1.2 Cast products may be in the form of cake, billet, wire bar, ingot, ingot bar, or casting.  
1.3 Wrought products may be in the form of flat, pipe, tube, rod, bar, shape, or forging.  
1.4 This practice is not intended to supersede or replace existing specification requirements for the sampling of a particular material.  
1.5 The values stated in SI units are to be regarded as standard. The values in parentheses are given for information only.  
1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. A specific precautionary statement appears in Appendix X4.  
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This practice covers the sampling, for the determination of chemical composition of nonferrous metals and alloys that have been reduced to their final form by mechanical working; that is, by such means as rolling, drawing, and extruding. The portion selection, sample preparation, sampling details, sample size and storage, and resampling are also detailed.
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1.1 This practice covers the sampling, for the determination of chemical composition (Note 1), of nonferrous metals and alloys that have been reduced to their final form by mechanical working; that is, by such means as rolling, drawing, and extruding.  
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5.1 The metallurgical properties of magnesium and its alloys are highly dependant on chemical composition. Precise and accurate analyses are essential to obtaining desired properties, meeting customer specifications and helping to reduce scrap due to off-grade material.  
5.2 This test method is applicable to chill cast specimens as defined in Practice B953 and can also be applied to other types of samples provided that suitable reference materials are available.
SCOPE
1.1 This test method describes the analysis of magnesium and its alloys by atomic emission spectrometry. The magnesium specimen to be analyzed may be in the form of a chill cast disk, casting, sheet, plate, extrusion or some other wrought form or shape. The elements covered in the scope of this method are listed in the table below.    
Element  
Mass Fraction Range (Wt %)  
Aluminum  
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Beryllium  
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0.0001 to 0.01  
Cadmium  
0.0001 to 0.05  
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Erbium  
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Gadolinium  
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Iron  
0.001 to 0.06  
Lanthanum  
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Lithium  
0.001 to 0.05  
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0.001 to 2.0  
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Nickel  
0.0005 to 0.05  
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Praseodymium  
0.01 to 0.5  
Samarium  
0.01 to 1.0  
Silicon  
0.002 to 5.0  
Silver  
0.001 to 0.2  
Sodium  
0.0005 to 0.01  
Strontium  
0.01 to 4.0  
Tin  
0.002 to 0.05  
Titanium  
0.001 to 0.02  
Yttrium  
0.02 to 7.0  
Ytterbium  
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Zinc  
0.001 to 10.0  
Zirconium  
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1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. Specific safety and health statements are given in Section 10.  
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5.1 This test method for the chemical analysis of metals and alloys is primarily intended to test such materials for compliance with compositional specifications. It is assumed that all those who use this test method will be trained analysts capable of performing common laboratory procedures skillfully and safely. It is expected that work will be performed in a properly equipped laboratory.
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1.1 This test method covers the chemical analysis of zinc alloys having chemical compositions within the following limits:    
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0.002 max  
Titanium  
0.02 max  
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0.02 max  
1.2 Units—The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.3 Included are procedures for elements in the following composition ranges:    
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Composition Range, %  
Aluminum  
3.0–8.0  
Cadmium  
0.0016–0.025  
Cerium  
0.005–0.10  
Iron  
0.0015–0.10  
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0.009–0.10  
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0.002–0.026  
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ASTM E1085-22(Test Method)
Standard Test Method for Analysis of Low-Alloy Steels by Wavelength Dispersive X-Ray Fluorescence Spectrometry

SIGNIFICANCE AND USE
5.1 This test method is suitable for manufacturing control and for verifying that a product meets specifications. This test method provides rapid, multi-element determinations with sufficient accuracy to ensure product quality and to minimize production delays. The analytical performance data may be used as a benchmark to determine if similar X-ray spectrometers provide equivalent precision and accuracy, or if the performance of a particular X-ray spectrometer has changed.  
5.2 Calcium is sometimes added to steel to affect inclusion shape which enhances certain mechanical properties of steel. This test method is useful for determining the residual calcium in the steel after such treatment.  
5.2.1 Because calcium occurs primarily in inclusions, the precision of this test method is a function of the distribution of the calcium-bearing inclusions in the steel. The variation of determinations on freshly prepared surfaces will give some indication of the distribution of these inclusions.
SCOPE
1.1 This test method covers the wavelength dispersive X-ray fluorescence analysis of low-alloy steels for the following elements:    
Element  
Mass Fraction
Range, %  
Calcium  
0.001 to 0.007  
Chromium  
0.04 to 2.5  
Cobalt  
0.03 to 0.2  
Copper  
0.03 to 0.6  
Manganese  
0.04 to 2.5  
Molybdenum  
0.005 to 1.5  
Nickel  
0.04 to 3.0  
Niobium  
0.002 to 0.1  
Phosphorus  
0.010 to 0.08  
Silicon  
0.06 to 1.5  
Sulfur  
0.009 to 0.1  
Vanadium  
0.012 to 0.6  
1.1.1 Unless exceptions are noted, mass fraction ranges can be extended and additional elements can be included by the use of suitable reference materials and measurement conditions. Deviations from the published scope must be validated by experimental means. See Guide E2857 for information on validation options.  
1.2 The values stated in the International System of Units (SI) are to be regarded as standard. The values given in parentheses are mathematical conversions to other units that are provided for information only, because they may be used in older software and laboratory procedures.  
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ASTM E3346-22(Guide)
Standard Guide for Combustion, Inert Gas Fusion and Hot Extraction Instruments for use in Analyzing Metals, Ores, and Related Materials

SIGNIFICANCE AND USE
5.1 The chemical measurement processes covered by this guide are used for determination of Carbon, Sulfur, Nitrogen, Oxygen and Hydrogen in metals, ores and related materials. A test method utilizing this guidance is used to test such materials, and also form the basis for quality assurance of these materials. Thus, it is economically and scientifically critical that these instruments be understood by the laboratories that use them.  
5.2 It is assumed that all who use this guide will be trained analysts, capable of performing common laboratory procedures skillfully, and safely. It is expected that any work will be performed in a properly equipped laboratory.  
5.3 It is expected that the laboratory will prepare their own work procedures for any of the information described in this guide.  
5.4 This guide contains numerous references to “manufacturer’s recommendations”. The user of this guide is expected to refer to the instrument operation manual for the specific instrument being used or consult directly with the manufacturer to obtain instructions or recommendations.  
5.5 This guide stresses the conservation of certified reference materials (CRMs). CRMs should not be used for drift checks or conditioning measurments. Other materials should be developed and used for these operations.
SCOPE
1.1 This guide covers information for using Combustion, Inert Gas Fusion and Hot Extraction instruments to determine the mass fraction of the non-metallic elements Carbon, Sulfur, Nitrogen, Oxygen and Hydrogen in metals, ores and related materials.  
1.2 This guide does not specify all the operating conditions because of the differences among different manufacturer’s instruments. Laboratories should follow instructions provided by the manufacturer of the instrument.  
1.3 Units—The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.5 The information in this guide is contained in the sections indicated as follows:    
Sections  
Carbon/Sulfur by Combustion/Infrared Detection  
14 – 19  
Nitrogen/Oxygen by Inert Gas Fusion/Thermal Conductivity and Infrared Detection  
20 – 25  
Hydrogen by Inert Gas Fusion Instrumental Measurement and Hot Extraction/Various Detection Cell Technology  
26 – 31  
1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

  • Guide
    10 pages
    English language
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ASTM
ASTM G47-22(Test Method)
Standard Test Method for Determining Susceptibility to Stress-Corrosion Cracking of 2XXX and 7XXX Aluminum Alloy Products

SIGNIFICANCE AND USE
4.1 The 3.5 % NaCl solution alternate immersion test provides a test environment for detecting materials that would be likely to be susceptible to SCC in natural outdoor environments, especially environments with marine influences.3,4,5 For determining actual serviceability of a material, other stress-corrosion tests should be performed in the intended service environment under conditions relating to the end use, including protective measures.  
4.2 Although this test method is intended for certain alloy types and for testing products primarily in the short-transverse stressing direction, this method is useful for some other types of alloys and stressing directions.
SCOPE
1.1 This test method covers a uniform procedure for characterizing the resistance to stress-corrosion cracking (SCC) of high-strength aluminum alloy wrought products for the guidance of those who perform stress-corrosion tests, for those who prepare stress-corrosion specifications, and for materials engineers.  
1.2 This test method covers method of sampling, type of specimen, specimen preparation, test environment, and method of exposure for determining the susceptibility to SCC of 2XXX (with 1.8 % to 7.0 % copper) and 7XXX (with 0.4 % to 2.8 % copper) aluminum alloy products, particularly when stressed in the short-transverse direction relative to the grain structure.  
1.3 The values stated in SI units are to be regarded as standard. The values given in parentheses after SI units are provided for information only and are not considered standard.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

  • Standard
    7 pages
    English language
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  • Standard
    7 pages
    English language
    sale 15% off