Standard Specification for Reclaimed Methylene Chloride <a href="#fn00002"></a>

ABSTRACT
This specification covers reclaimed methylene chloride used in various industries for noncritical applications. Tests for specific gravity, acidity, water content, appearance, color, nonvolatile residue, chloride content, assay, and 1,1,1-trichloroethane content shall be performed and shall conform to the requirements specified.
SCOPE
1.1 This specification covers the grade of methylene chloride typically needed in various industries for noncritical applications, such as in paint stripping formulations. It may be used as a reference document by purchasers or by persons establishing in-house methylene chloride recovery programs.

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Publication Date
31-Dec-2007
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ASTM D5395-03(2008) - Standard Specification for Reclaimed Methylene Chloride <a href="#fn00002"></a>
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NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
Designation:D5395 −03(Reapproved 2008)
Standard Specification for
1,2
Reclaimed Methylene Chloride
This standard is issued under the fixed designation D5395; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope D2989 Test Method for Acidity-Alkalinity of Halogenated
Organic Solvents and Their Admixtures
1.1 This specification covers the grade of methylene chlo-
D3401 Test Methods for Water in Halogenated Organic
ride typically needed in various industries for noncritical
Solvents and Their Admixtures
applications, such as in paint stripping formulations. It may be
D3741 Test Methods for Appearance of Admixtures Con-
used as a reference document by purchasers or by persons
taining Halogenated Organic Solvents
establishing in-house methylene chloride recovery programs.
D6806 Practice for Analysis of Halogenated Organic Sol-
vents and Their Admixtures by Gas Chromatography
2. Referenced Documents
E1064 Test Method for Water in Organic Liquids by Coulo-
2.1 ASTM Standards:
metric Karl Fischer Titration
D2108 Test Method for Color of Halogenated Organic
2.2 U.S. Governmnet Documents:
Solvents and Their Admixtures (Platinum-Cobalt Scale)
49 CFR 100 to 199 Department ofTransportation Hazardous
D2109 Test Methods for Nonvolatile Matter in Halogenated
Materials Regulations
Organic Solvents and Their Admixtures
29 CFR 1910.1200 Department of Labor, OSHA Regula-
D2111 Test Methods for Specific Gravity and Density of
tions on Hazard Communications
Halogenated Organic Solvents and Their Admixtures
D2988 Test Methods for Water-Soluble Halide Ion in Halo-
3. Properties
genated Organic Solvents and Their Admixtures
3.1 Reclaimed methylene chloride shall meet the require-
ments of Table 1.
This specification is under the jurisdiction of ASTM Committee D26 on
4. Packaging and Package Marking
Halogenated Organic Solvents and Fire Extinguishing Agents and is the direct
4.1 Package and label industrial or commercial quantities in
responsibility of Subcommittee D26.02 on Vapor Degreasing.
Current edition approved Jan. 1, 2008. Published March 2008. Originally
accordance with DOT regulations as found in 49 CFR 100 to
approved in 1993. Last previous edition approved in 2003 as D5395 – 03. DOI:
199, and in accordance with state and local regulations, and
10.1520/D5395-03R08.
2 with OSHA re
...


This document is not an ASTM standard and is intended only to provide the user of an ASTM standard an indication of what changes have been made to the previous version. Because
it may not be technically possible to adequately depict all changes accurately, ASTM recommends that users consult prior editions as appropriate. In all cases only the current version
of the standard as published by ASTM is to be considered the official document.
Designation:D5395–97 Designation: D 5395 – 03 (Reapproved 2008)
Standard Specification for
,
1 2
Reclaimed Methylene Chloride
This standard is issued under the fixed designation D 5395; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (e) indicates an editorial change since the last revision or reapproval.
1. Scope
1.1 This specification covers the grade of methylene chloride typically needed in various industries for noncritical applications,
such as in paint stripping formulations. It may be used as a reference document by purchasers or by persons establishing in-house
methylene chloride recovery programs.
2. Referenced Documents
2.1 ASTM Standards:
D2108Test Method for Color of Halogenated Organic Solvents and Their Admixtures (Platinum-Cobalt Scale)
D2109Test Methods for Nonvolatile Matter in Halogenated Organic Solvents and Their Admixtures
D2111Test Methods for Specific Gravity of Halogenated Organic Solvents and Their Admixtures
D2988Test Method for Water-Soluble Halide Ion in Halogenated Organic Solvents and Their Admixtures
D2989Test Method for Acidity-Alkalinity of Halogenated Organic Solvents and Their Admixtures
D3401Test Methods for Water in Halogenated Organic Solvents and Their Admixtures
D3447Test Method for Purity of Trichlorotrifluoroethane
D3741Test Method for Appearance of Admixtures Containing Halogenated Organic Solvents
E1064Test Method for Water in Organic Liquids by Coulometric Karl Fischer Titration
D 2108 Test Method for Color of Halogenated Organic Solvents and Their Admixtures (Platinum-Cobalt Scale)
D 2109 Test Methods for Nonvolatile Matter in Halogenated Organic Solvents and Their Admixtures
D 2111 Test Methods for Specific Gravity and Density of Halogenated Organic Solvents and Their Admixtures
D 2988 Test Methods for Water-Soluble Halide Ion in Halogenated Organic Solvents and Their Admixtures
D 2989 Test Method for Acidity-Alkalinity of Halogenated Organic Solvents and Their Admixtures
D 3401 Test Methods for Water in Halogenated Organic Solvents and Their Admixtures
D 3741 Test Methods for Appearance of Admixtures Containing Halogenated Organic Solvents
D 6806 Practice for Analysis of Halogenated Organic Solvents and Their Admixtures by Gas Chromatography
E 1064 Test Method for Water in Organic Liquids by Coulometric Karl Fischer Titration
2.2 U.S. Governmnet Documents:
49 CFR 100 to 199 Department of Transportation Hazardous Materials Regulations
29 CFR 1910.1200 Department of Labor, OSHA Regulations on Hazard Communications
3. Properties
3.1 Reclaimed methylene chloride shall meet the requirements of Table 1.
4. Packaging and Package Marking
4.1Industrial or commercial quantities shall be packaged and labeled in accordance with DOT regulations as found in 49 CFR
100 to 199 and state and local regulations with above usage in mind.
4.2Department of Defense procurements
...

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