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ASTM C1250-93(2005)

(Test Method)

Standard Test Method for Nonvolatile Content of Cold Liquid-Applied Elastomeric Waterproofing Membranes

Standard Test Method for Nonvolatile Content of Cold Liquid-Applied Elastomeric Waterproofing Membranes

SCOPE
1.1 This test method describes a laboratory procedure for determining the average nonvolatile content for one- or two-component cold liquid-applied elastomeric waterproofing membranes.
1.2 The values stated in SI units are to be regarded as the standard. The values in parentheses are for information only.
1.3 This standard does not purport to address all of the safety problems, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

General Information

Status
Historical
Publication Date
31-Dec-2004
ICS
83.060 - Rubber
91.100.50 - Binders. Sealing materials
Technical Committee
D08 - Roofing and Waterproofing
Drafting Committee
D08.22 - Waterproofing and Dampproofing Systems
Current Stage
Ref Project

Relations

Replaces
ASTM C1250-93(1998) - Standard Test Method for Nonvolatile Content of Cold Liquid-Applied Elastomeric Waterproofing Membranes
Effective Date
01-Jan-2005
Replaced By
ASTM C1250-05 - Standard Test Method for Nonvolatile Content of Cold Liquid-Applied Elastomeric Waterproofing Membranes (Withdrawn 2015)
Effective Date
01-Jul-2005
Referred By
ASTM C1522-05(2021) - Standard Test Method for Extensibility After Heat Aging of Cold Liquid-Applied Elastomeric Waterproofing Membranes
Effective Date
01-Jan-2005

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ASTM C1250-93(2005) - Standard Test Method for Nonvolatile Content of Cold Liquid-Applied Elastomeric Waterproofing MembranesASTM C1250-93(2005) - Standard Test Method for Nonvolatile Content of Cold Liquid-Applied Elastomeric Waterproofing Membranes
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ASTM C1250-93(2005) - Standard Test Method for Nonvolatile Content of Cold Liquid-Applied Elastomeric Waterproofing Membranes
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NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
Designation: C 1250 – 93 (Reapproved 2005)
Standard Test Method for
Nonvolatile Content of Cold Liquid-Applied Elastomeric
Waterproofing Membranes
This standard is issued under the fixed designation C 1250; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (e) indicates an editorial change since the last revision or reapproval.
1. Scope 6. Apparatus
1.1 This test method describes a laboratory procedure for 6.1 Forced-draft Oven, controlled to 70 6 2°C (158 6
determining the average nonvolatile content for one- or two- 3.6°F).
component cold liquid-applied elastomeric waterproofing 6.2 Balance, sensitive to 0.01 g.
membranes. 6.3 Two Aluminum Weighing Dishes,57by18mm.
1.2 The values stated in SI units are to be regarded as the
7. Conditioning/Mixing
standard. The values in parentheses are for information only.
1.3 This standard does not purport to address all of the 7.1 Unless otherwise specified by those authorizing the
tests, standard conditions for all tests are 23 6 2°C (73.4 6
safety concerns, if any, associated with its use. It is the
responsibility of the user of this standard to establish appro- 3.6°F) and 50 6 5 % relative humidity.
7.2 Store all membrane materials to be tested in an un-
priate safety and health practices and determine the applica-
bility of regulatory limitations prior to use. opened container at standard conditions for at least 24 h before
any test specimens are prepared.
2. Referenced Documents
7.3 Follow the manufacturer’s instructions for mixing and
2.1 ASTM Standards: preparing membrane materials for testing. Thoroughly mix
C 717 Terminology of Building Seals and Sealants one-component materials before using. Mix two-component
compounds in the ratio recommended by the manufacturer.
3. Terminology
8. Procedure
3.1 Definitions—Refer toTerminology C 717 for definitions
of compound, elastomeric, and waterproofing, used in this test 8.1 For each test sample, prepare two test specimens as
method. follows:
8.1.1 Mark each aluminum weighing dish for identification.
4. Summary of Test Method
Accurately weigh each aluminum weighing dish to the nearest
4.1 This test method consists of preparing duplicate
0.01 g. Record each mass.
samples, each of known mass, and aging these samples for 72 8.1.2 Place an aluminum weighing dish on the balance and
hat70 6 2°C (158 6 3.6°F) in an air-circulating oven.
tare. Add 5.06 0.2 g of compound and spread evenly over the
interior surface area of the dish.
5. Significance and Use
8.1.3 Reweigh the test specimen, combination membrane,
5.1 This test method is used to determine the nonvolatile
and dish, and record the mass.
content of cold liquid-applied elastomeric waterproofing mem-
8.1.4 Repeat 8.
...

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1.3 There is no known ISO equivalent to this test method.  
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This specification covers nonvulcanized (uncured) rubber sheet made of ethylene-propylene-diene terpolymer (EPDM) or polychloroprene (CR) intended for use as watertight roof flashing exposed to the weather. In-place roof system design criteria such as fire resistance, field seaming strength, material compatibility, and uplift resistance, among others, are beyond the scope of this specification. The flashing material shall be formulated from the appropriate polymer type and other compounding ingredients, and shall be capable of being bonded to itself, to the roofing membrane, and to substrate for making watertight field splices and repairs. Property requirements for flashing before vulcanization include thickness, Green strength modulus, ultimate elongation, shelf stability, vulcanizability, tensile strength and set, dimensional stability, and weatherability. Consequently, the property requirements for flashing after vulcanization includes tensile strength and set, elongation, tear resistance, brittle point, ozone resistance, air oven heat aging, water absorption and weight change, linear dimension change, and weatherability.
SCOPE
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1.3 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the two systems may result in nonconformance with the standard.  
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5.1 There are differences in opinion among those concerned with sealant technology whether or not this adhesion-in-peel test simulates the type of strain and e-tensile stresses encountered by a sealant in normal use. Nevertheless, this test provides a valuable measurement of the ability of the cured sealant to maintain a bond to the substrate under severe peel conditions.  
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5.3 This test method alone is not appropriate for comparing the overall performance of different sealants in a given application. The adhesive force that determines if a given sealant is useful in a given application also depends on the modulus of elasticity and the degree to which the sealant will be strained. This test, as it exists, does not consider the modulus of elasticity, nor amount of stress that will be produced by a given strain in an actual sealant in a moving joint. No known correlations are given to relate and apply modulus values to the peel values.  
5.4 This test requires that the results indicate whether the failure mode is primarily adhesive or cohesive. It is important to note that a cohesive failure is not necessarily better than an adhesive failure, if the adhesive value is sufficient for the application. Having adhesive failure allows one to study the change of adhesion with time and with the various stress conditions.
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1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
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