Standard Specification for Crosslinked and Noncrosslinked Poly(Vinyl Chloride) Heat-Shrinkable Tubing for Electrical Insulation

ABSTRACT
This specification applies to two types of flexible, crosslinked (Type II) and noncrosslinked (Type I) poly(vinyl chloride) heat-shrinkable tubing for electrical insulating purposes. It is supplied in an expanded form and will shrink to its extruded diameter when heated. Besides dimensional requirements such as inside diameter and wall thickness, the tubing shall also adhere to the following chemical and physical property requirements: restricted shrinkage; longitudinal change; dielectric strength; color and color stability; water absorption; specific gravity; volume resistivity; flammability; heat shock; low-temperature flexibility; tensile strength; elongation; heat resistance; resistance to fluids such as hydraulic fluid, JP-4 fuel, lubricating oils, de-icing fluid, and NaCl solution; copper corrosion; behavior during copper dust humidity test; and shelf life.
SCOPE
1.1 This specification applies to flexible, crosslinked and noncrosslinked poly(vinyl chloride) heat-shrinkable tubing for electrical insulating purposes. It is supplied in an expanded form and will shrink to its extruded diameter when heated.
Note 1—This standard is similar but not identical to IEC 60684-3-201.
1.2 The values stated in inch-pound units are to be regarded as the standard except temperature, which shall be stated in degrees Celsius. Values in parentheses are for information only.

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ASTM D3150-00(2006) - Standard Specification for Crosslinked and Noncrosslinked Poly(Vinyl Chloride) Heat-Shrinkable Tubing for Electrical Insulation
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NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
An American National Standard
Designation: D3150 – 00 (Reapproved 2006)
Standard Specification for
Crosslinked and Noncrosslinked Poly(Vinyl Chloride) Heat-
Shrinkable Tubing for Electrical Insulation
This standard is issued under the fixed designation D3150; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope SS-S-550 Sodium Chloride, Technical, for Water-Softening
Units
1.1 This specification applies to flexible, crosslinked and
2.4 IEC Standards:
noncrosslinked poly(vinyl chloride) heat-shrinkable tubing for
60684–3–201 Flexible insulating sleeving, Part 3, Sheet
electrical insulating purposes. It is supplied in an expanded
201: Heat shrinkable sleeving, general purpose, flexible,
form and will shrink to its extruded diameter when heated.
cross-linked PVC, shrink ratio 2:1
NOTE 1—This standard is similar but not identical to IEC
60684–3–201.
3. Terminology
1.2 The values stated in inch-pound units are to be regarded
3.1 Definitions:
as the standard except temperature, which shall be stated in
3.1.1 For definitions pertaining to electrical insulation, refer
degreesCelsius.Valuesinparenthesesareforinformationonly.
to Terminology D1711.
3.1.2 For definitions pertaining to fire standards, refer to
2. Referenced Documents
Terminology E176.
2.1 ASTM Standards:
4. Classification
D1711 Terminology Relating to Electrical Insulation
D2671 Test Methods for Heat-Shrinkable Tubing for Elec-
4.1 Type I—Flexible, noncrosslinked poly(vinyl chloride)
trical Use
tubing capable of being shrunk at 135 °C (275 °F) in 15 min.
D3636 Practice for Sampling and Judging Quality of Solid
4.2 Type II—Flexible, crosslinked poly(vinyl chloride) tub-
Electrical Insulating Materials
ing capable of being shrunk at 175 °C (347 °F) in 15 min.
E176 Terminology of Fire Standards
5. Ordering Information
2.2 Military Standards:
MIL-STD-104 Limits for Electrical Insulation Color 5.1 When tubing is ordered to this specification, the pur-
MIL-H-5606 Hydraulic Fluid, Petroleum Base, Aircraft,
chaser should define the size, color, and type of the required
Missile, and Ordnance tubing.
MIL-T-5624 Turbine Fuel, Aviation, Grades JP-4 and JP-5
6. Materials and Manufacture
MIL-L-7808 Lubricating Oil, Aircraft, Turbine Engine,
Synthetic Base 6.1 The polymers used in the manufacture of heat-
MIL-L-23699 Lubricating Oil, Aircraft, Turbine Engines, shrinkable tubing shall be modified poly(vinyl chloride) and
Synthetic Base the finished compound shall be free of all foreign matter other
MIL-A-8243 Anti-Icing and De-Icing Defrosting Fluid than intended formulation additives as appropriate.
2.3 Federal Standards: 6.2 The tubing shall be extruded, crosslinked (Type II only),
and then expanded to the required dimensions.
This specification is under the jurisdiction of ASTM Committee D09 on
7. Chemical and Physical Property Requirements Chemical
Electrical and Electronic Insulating Materials and is the direct responsibility of
and Physical Property Requirements
Subcommittee D09.07 on Flexible and Rigid Insulating Materials.
Current edition approved Oct. 1, 2006. Published October 2006. Originally
7.1 The material shall conform to the chemical and physical
approved in 1973. Last previous edition approved in 2000 as D3150 – 00. DOI:
property requirements specified in Table 1.
10.1520/D3150-00R06.
For referenced ASTM standards, visit the ASTM website, www.astm.org, or
contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
Standards volume information, refer to the standard’s Document Summary page on May be obtained from Superintendent of Documents, U.S. Government
the ASTM website. Printing Office, Washington, DC 20402.
3 5
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Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, United States.
D3150 – 00 (2006)
TABLE 1 Chemical and Physical Property Requirements
Requirements
Property
Type I Type II
Restricted shrinkage, Procedure A:
Type I—30 min, 135 6 2°C(275 6 4 °F) no cracks
Type II—30 min, 175 6 2°C(374 6 4 °F) no cracks
2000-V proof voltage no failures no failures
Longitudinal change, max, % 0, − 25 + 1, − 10
Dielectric strength, V/mil (kV/mm) 400 (15.75) 400 (15.75)
Color MIL-STD-104 MIL-STD-104
Color stability, 24 h at 130 6 2°C(266 6 4 °F) MIL-STD-104 MIL-STD-104
Water absorption, 24 h at 25 6 2°C(77 6 4 °F), max, % 1.0 1.0
Specific gravity, max 1.40 1.40
11 11
Volume resistivity, min, ohm·cm 10 10
Flammability, max, s, Procedure A 15 15
Heat shock:
Type I—4 h at 180 6 2°C(236 6 4 °F) no dripping, flowing, or cracking
Type II—4 h at 200 6 2°C(392 6 4 °F) no dripping, flowing, or cracking
Low-temperature flexibility, Procedure B, all sizes1hat no cracking no cracking
− 10 °C (14 °F) on as-received specimens
Tensile strength, min, psi (MPa) 2000 (13.8) 2000 (13.8)
Elongation, min, % 200 200
Heat resistance, 168 h at 136 6 2°C(277 6 4 °F), followed
by tests for:
Elongation, min, % 150 130
Elongation, % of original, min 65 65
Fluid resistance, 24 h at 25 6 2°C(77 6 4 °F):
Hydraulic Fluid, MIL-H-5606
JP-4 Fuel, MIL-T-5624
Lubricating Oil, MIL-L-7808
Lubricating Oil, MIL-L-23699
De-icing Fluid, MIL-A-8243
5 % NaCl, SS-S-550
Followed by tests for:
Dielectric strength, V/mil (kV/mm) 280 (11.0) 280 (11.0)
Tensile strength, min, psi (MPa) 1800 (12.4) 2000 (13.8)
Copper corrosion, Procedure B:
168 h at 136 °C (277 °F) no blackening or pitting of copper no blackening or pitting of copper
Copper dust humidity test, Procedure C no corrosion or discoloration of copper dust no corrosion or discoloration of copper dust
Shelf life
The required shelf life is 2 weeks at 40 6 2°C(104 6 4 °F). The supplier must advise and caution the customer if special storage and handling precautions must
be observed to maintain required product dimensions and characteristics.
TABLE 2 Type I Dimensions
7.2 Every lot of material shall be tested for dimensional
As Supplied After Unrestricted Shrinkage
requirements, restricted shrinkage, tensile strength, elongation,
Nominal Inside Diameter, Inside Diameter,
longitudinal change, and dielectric breakdown. Other require-
Wall Thickness, in. (mm)
Size, in. min, in. (mm) max, in. (mm)
ments may be tested less frequently or at a frequency agreed
⁄16 0.063 (1.60) 0.037 (0.94) 0.014 6 0.003 (0.35 6 0.08)
upon between the supplier and the purchaser.
⁄32 0.093 (2.34) 0.055 (1.41) 0.014 6 0.003 (0.35 6 0.08)
⁄8 0.125 (3.18) 0.075 (1.91) 0.014 6 0.003 (0.35 6 0.08)
8. Dimensional Requirements 3
⁄16 0.187 (4.75) 0.110 (2.80) 0.018 6 0.003 (0.45 6 0.08)
⁄4 0.250 (6.35) 0.150 (3.81) 0.022 6 0.004 (0.56 6 0.12)
8.1 Type I material shall conform to the applicable require-
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