iTeh StandardsiTeh Standards
EURUSD
Your shopping cart is empty.
ASTM

ASTM G127-15

(Guide)

Standard Guide for the Selection of Cleaning Agents for Oxygen-Enriched Systems

Standard Guide for the Selection of Cleaning Agents for Oxygen-Enriched Systems

SIGNIFICANCE AND USE
3.1 The purpose of this guide is to provide information that may be considered when selecting and qualifying a cleaning agent for oxygen-enriched systems.  
3.2 Insufficient cleanliness can result in the ignition of contaminants or components by a variety of mechanisms. Therefore, an acceptable level of contamination for each condition of use in oxygen-enriched service should be defined. The acceptable level of contamination may depend on various factors, such as:  
3.2.1 The nature and type of the contaminants,  
3.2.2 The location and degree of contamination,  
3.2.3 The type of substrate material,  
3.2.4 The configuration and end use of the equipment or part to be cleaned, and  
3.2.5 The operating parameters of the oxygen-enriched system (pressure, temperature, phase, concentration, fluid velocity, etc.).
SCOPE
1.1 The purpose of this guide is to establish a procedure to select cleaning agents, both solvents and water-based detergents, for oxygen-enriched systems. This includes laboratory-scale tests for cleaning effectiveness, materials compatibility, and oxygen compatibility.  
1.2 The effectiveness of a particular cleaning agent depends upon the method by which it is used, the nature and type of the contaminants, and the characteristics of the article being cleaned, such as size, shape, and material. Final evaluation of the cleaning agent should include testing of actual products and production processes.  
1.3 Different cleaning agents may be required for different cleaning activities, such as aqueous ultrasonic cleaning, spray cleaning, hand wiping, and flushing of oxygen lines in field applications.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

General Information

Status
Historical
Publication Date
30-Sep-2015
ICS
71.100.40 - Surface active agents
Technical Committee
G04 - Compatibility and Sensitivity of Materials in Oxygen Enriched Atmospheres
Drafting Committee
G04.02 - Recommended Practices
Current Stage
Ref Project

Buy Standard

ASTM G127-15 - Standard Guide for the Selection of Cleaning Agents for Oxygen-Enriched SystemsASTM G127-15 - Standard Guide for the Selection of Cleaning Agents for Oxygen-Enriched Systems
PreviousNext
Guide
ASTM G127-15 - Standard Guide for the Selection of Cleaning Agents for Oxygen-Enriched Systems
English language
6 pages
sale 15% off
Preview
sale 15% off
Preview
REDLINE ASTM G127-15 - Standard Guide for the Selection of Cleaning Agents for Oxygen-Enriched SystemsREDLINE ASTM G127-15 - Standard Guide for the Selection of Cleaning Agents for Oxygen-Enriched Systems
PreviousNext
Guide
REDLINE ASTM G127-15 - Standard Guide for the Selection of Cleaning Agents for Oxygen-Enriched Systems
English language
6 pages
sale 15% off
Preview
sale 15% off
Preview

Standards Content (Sample)

NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
Designation: G127 − 15
Standard Guide for the
1
Selection of Cleaning Agents for Oxygen-Enriched Systems
This standard is issued under the fixed designation G127; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope D2863 Test Method for Measuring the Minimum Oxygen
Concentration to Support Candle-Like Combustion of
1.1 The purpose of this guide is to establish a procedure to
Plastics (Oxygen Index)
select cleaning agents, both solvents and water-based
D4809 Test Method for Heat of Combustion of Liquid
detergents, for oxygen-enriched systems. This includes
Hydrocarbon Fuels by Bomb Calorimeter (Precision
laboratory-scale tests for cleaning effectiveness, materials
Method)
compatibility, and oxygen compatibility.
F483 Practice for Total Immersion Corrosion Test for Air-
1.2 The effectiveness of a particular cleaning agent depends
craft Maintenance Chemicals
upon the method by which it is used, the nature and type of the
G5 Reference Test Method for Making Potentiodynamic
contaminants, and the characteristics of the article being
Anodic Polarization Measurements
cleaned, such as size, shape, and material. Final evaluation of
G31 Guide for Laboratory Immersion Corrosion Testing of
the cleaning agent should include testing of actual products and
Metals
production processes.
G59 Test Method for Conducting Potentiodynamic Polariza-
1.3 Different cleaning agents may be required for different tion Resistance Measurements
G63 Guide for Evaluating Nonmetallic Materials for Oxy-
cleaning activities, such as aqueous ultrasonic cleaning, spray
cleaning, hand wiping, and flushing of oxygen lines in field gen Service
G72 Test Method for Autogenous Ignition Temperature of
applications.
Liquids and Solids in a High-Pressure Oxygen-Enriched
1.4 This standard does not purport to address all of the
Environment
safety concerns, if any, associated with its use. It is the
G74 Test Method for Ignition Sensitivity of Nonmetallic
responsibility of the user of this standard to establish appro-
Materials and Components by Gaseous Fluid Impact
priate safety and health practices and determine the applica-
G86 Test Method for Determining Ignition Sensitivity of
bility of regulatory limitations prior to use.
Materials to Mechanical Impact in Ambient Liquid Oxy-
gen and Pressurized Liquid and Gaseous Oxygen Envi-
2. Referenced Documents
ronments
2
2.1 ASTM Standards:
G93 Practice for Cleaning Methods and Cleanliness Levels
D471 Test Method for Rubber Property—Effect of Liquids
for Material and Equipment Used in Oxygen-Enriched
D543 Practices for Evaluating the Resistance of Plastics to
Environments
Chemical Reagents
G94 Guide for Evaluating Metals for Oxygen Service
D1193 Specification for Reagent Water
G121 Practice for Preparation of Contaminated Test Cou-
D1460 Test Method for Rubber Property—Change in
pons for the Evaluation of Cleaning Agents
Length During Liquid Immersion
G122 Test Method for Evaluating the Effectiveness of
D2512 Test Method for Compatibility of Materials with
Cleaning Agents
Liquid Oxygen (Impact Sensitivity Threshold and Pass-
2.2 CGA Document:
Fail Techniques)
CGA Pamphlet G-4.1 Cleaning Equipment for Oxygen Ser-
vice
1
2.3 Other ASTM Documents:
This guide is under the jurisdiction of ASTM Committee G04 on Compatibility
and Sensitivity of Materials in Oxygen Enriched Atmospheres and is the direct
MNL36 Safe Use of Oxygen and Oxygen Systems: Hand-
2
responsibility of Subcommittee G04.02 on Recommended Practices.
book for Design, Operation, and Maintenance
Current edition approved Oct. 1, 2015. Published October 2015. Originally
approved in 1995. Last previous edition approved in 2008 as G127 – 95 (2008).
3. Significance and Use
DOI: 10.1520/G0127-15.
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or
3.1 The purpose of this guide is to provide information that
contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
may be considered when selecting and qualifying a cleaning
Standards volume information, refer to the standard’s Document Summary page on
the ASTM website. agent for oxygen-enriched systems.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
1

---------------------- Page: 1 ----------------------
G127 − 15
3.2 Insufficient cleanliness can result in the ignition of are expected to come in contact with the candidate cleaning
contaminants or components by a variety of mechanisms. agent. As a minimum, materials representative of each family
Therefore, an acceptable level of contaminati
...

This document is not an ASTM standard and is intended only to provide the user of an ASTM standard an indication of what changes have been made to the previous version. Because
it may not be technically possible to adequately depict all changes accurately, ASTM recommends that users consult prior editions as appropriate. In all cases only the current version
of the standard as published by ASTM is to be considered the official document.
Designation: G127 − 95 (Reapproved 2008) G127 − 15
Standard Guide for the
Selection of Cleaning Agents for OxygenOxygen-Enriched
1
Systems
This standard is issued under the fixed designation G127; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope
1.1 The purpose of this guide is to establish a procedure to select cleaning agents, both solvents and water-based detergents, for
oxygen service.oxygen-enriched systems. This includes of laboratory-scale tests for cleaning effectiveness, materials compatibility,
and oxygen compatibility.
1.2 The effectiveness of a particular cleaning agent depends upon the method by which it is used, the nature and type of the
contaminants, and the characteristics of the article being cleaned, such as size, shape, and material. Final evaluation of the cleaning
agent should include testing of actual products and production processes.
1.3 Different cleaning agents may be required for different cleaning activities, such as aqueous ultrasonic cleaning, spray
cleaning, hand wiping, and flushing of oxygen lines in field applications.
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility
of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory
limitations prior to use.
2. Referenced Documents
2
2.1 ASTM Standards:
D471 Test Method for Rubber Property—Effect of Liquids
D543 Practices for Evaluating the Resistance of Plastics to Chemical Reagents
D1193 Specification for Reagent Water
D1460 Test Method for Rubber Property—Change in Length During Liquid Immersion
D2512 Test Method for Compatibility of Materials with Liquid Oxygen (Impact Sensitivity Threshold and Pass-Fail Techniques)
D2863 Test Method for Measuring the Minimum Oxygen Concentration to Support Candle-Like Combustion of Plastics
(Oxygen Index)
3
D2934 Test Method for Compatibility of Vulcanized Rubber Seals--Compatibility with Service Fluids (Withdrawn 1993)
D4809 Test Method for Heat of Combustion of Liquid Hydrocarbon Fuels by Bomb Calorimeter (Precision Method)
F483 Practice for Total Immersion Corrosion Test for Aircraft Maintenance Chemicals
G5 Reference Test Method for Making Potentiodynamic Anodic Polarization Measurements
G31 Guide for Laboratory Immersion Corrosion Testing of Metals
G59 Test Method for Conducting Potentiodynamic Polarization Resistance Measurements
G63 Guide for Evaluating Nonmetallic Materials for Oxygen Service
G72 Test Method for Autogenous Ignition Temperature of Liquids and Solids in a High-Pressure Oxygen-Enriched Environment
G74 Test Method for Ignition Sensitivity of Nonmetallic Materials and Components by Gaseous Fluid Impact
G86 Test Method for Determining Ignition Sensitivity of Materials to Mechanical Impact in Ambient Liquid Oxygen and
Pressurized Liquid and Gaseous Oxygen Environments
G93 Practice for Cleaning Methods and Cleanliness Levels for Material and Equipment Used in Oxygen-Enriched Environments
G94 Guide for Evaluating Metals for Oxygen Service
G121 Practice for Preparation of Contaminated Test Coupons for the Evaluation of Cleaning Agents
1
This guide is under the jurisdiction of ASTM Committee G04 on Compatibility and Sensitivity of Materials in Oxygen Enriched Atmospheres and is the direct
responsibility of Subcommittee G04.02 on Recommended Practices.
Current edition approved April 1, 2008Oct. 1, 2015. Published July 2008October 2015. Originally approved in 1995. Last previous edition approved in 20002008 as
G127 – 95 (2000).(2008). DOI: 10.1520/G0127-95R08.10.1520/G0127-15.
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM Standards
volume information, refer to the standard’s Document Summary page on the ASTM website.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
1

---------------------- Page: 1 ----------------------
G127 − 15
G122 Test Method for Evaluating the Effectiveness of Cleaning Agents
2.2 CGA Document:
CGA Pamphlet G-4.1 Cleaning Equipment for Oxygen Service
2.3 Other ASTM Documents:
2
MNL36 Safe Use of Oxygen and Oxygen Systems: Handbook for Design, Operation,
...

Questions, Comments and Discussion

Ask us and Technical Secretary will try to provide an answer. You can facilitate discussion about the standard in here.

This May Also Interest You

ASTM
ASTM G127-15(2023)(Guide)
Standard Guide for the Selection of Cleaning Agents for Oxygen-Enriched Systems

SIGNIFICANCE AND USE
3.1 The purpose of this guide is to provide information that may be considered when selecting and qualifying a cleaning agent for oxygen-enriched systems.  
3.2 Insufficient cleanliness can result in the ignition of contaminants or components by a variety of mechanisms. Therefore, an acceptable level of contamination for each condition of use in oxygen-enriched service should be defined. The acceptable level of contamination may depend on various factors, such as:  
3.2.1 The nature and type of the contaminants,  
3.2.2 The location and degree of contamination,  
3.2.3 The type of substrate material,  
3.2.4 The configuration and end use of the equipment or part to be cleaned, and  
3.2.5 The operating parameters of the oxygen-enriched system (pressure, temperature, phase, concentration, fluid velocity, etc.).
SCOPE
1.1 The purpose of this guide is to establish a procedure to select cleaning agents, both solvents and water-based detergents, for oxygen-enriched systems. This includes laboratory-scale tests for cleaning effectiveness, materials compatibility, and oxygen compatibility.  
1.2 The effectiveness of a particular cleaning agent depends upon the method by which it is used, the nature and type of the contaminants, and the characteristics of the article being cleaned, such as size, shape, and material. Final evaluation of the cleaning agent should include testing of actual products and production processes.  
1.3 Different cleaning agents may be required for different cleaning activities, such as aqueous ultrasonic cleaning, spray cleaning, hand wiping, and flushing of oxygen lines in field applications.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

  • Guide
    6 pages
    English language
    sale 15% off
ASTM
ASTM G122-20(Test Method)
Standard Test Method for Evaluating the Effectiveness of Cleaning Agents and Processes

SIGNIFICANCE AND USE
5.1 The purpose of these test methods is to define a procedure for evaluating the capability and effectiveness of cleaning agents to remove residues of a compound/product from surrogate surfaces (that is, coupons or beakers) of Materials of Construction. This test method also provides a procedure for determining the compatibility of cleaning agents with the Material of Construction prior to starting tests. Based on the outcome of the testing, suitable cleaning agents may be selected for further cleaning process development (see Guide D6361/D6361M).  
5.2 The potential critical cleaning parameters related to the cleaning agent(s) under study may also be examined using these tests. Potentially critical cleaning parameters include cleaning agent concentration, temperature, time, pH, foaming, type and strength of ultrasonic energy or agitation (if used), and others. These parameters may be varied (for example, using Design of Experiments) to determine their potential optimal settings for actual use.
SCOPE
1.1 This test method covers a procedure for evaluating the effectiveness and capability of cleaning agents to remove contamination to the desired level. This includes removing drug residues from manufacturing equipment and residues from medical devices (Guide E3106), as well as systems for oxygen service.  
1.2 The test coupons/beakers described in this standard provide a representative surface to which contamination can be applied and tested for the ability of a cleaning agent to remove it.  
1.3 This test method is a laboratory scale approximation and the actual effectiveness of a particular cleaning agent depends upon the method (temperature, agitation, concentration, etc.) in which it is used and the characteristics of the article being cleaned, such as size, shape, and material. Final evaluation of the cleaning agent should include testing of actual products and cleaning processes.  
1.4 Units—The values stated in SI units are to be regarded as standard. The values given in parentheses after SI units are provided for information only and are not considered standard.  
1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the safety of each compound on a case-by-case basis.  
1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

  • Standard
    6 pages
    English language
    sale 15% off
  • Standard
    6 pages
    English language
    sale 15% off
ASTM
ASTM G121-18(Practice)
Standard Practice for Preparation of Contaminated Test Coupons for the Evaluation of Cleaning Agents

SIGNIFICANCE AND USE
5.1 This practice will be suitable to direct the preparation of test coupons with a known amount of contaminant on the surface. A standard test coupon is described and a list of contaminants that have typically been found in oxygen-enriched systems and components is provided.  
5.2 These test coupons shall be used in the evaluation of cleaning agents for oxygen-enriched systems and components. This will permit direct comparison within and between test facilities.  
5.3 Materials used in other fluid handling systems such as nitrogen, helium, hydrogen, gasoline, etc. may also be prepared for evaluation by this practice.
SCOPE
1.1 This practice describes the procedure for the preparation of single- and double-sided contaminated test coupons for the evaluation of cleaning agents. It is applicable for the evaluation of cleaning agents proposed for the cleaning of oxygen equipment, pharmaceutical manufacturing equipment, and medical devices (see Test Method G122 and Guide G127). It also is applicable to other systems where contamination is a concern.  
1.2 Several classes of contaminants/residues most likely to be found in oxygen equipment, pharmaceutical manufacturing equipment, and medical devices are identified. However, if the user of this practice has identified contaminants not included in these classes, such identified contaminants may be substituted for the preparation of the test coupons if appropriate for this test method.  
1.3 Solvent and cleaning agent compatibility with nonmetallic substrates should be verified prior to the preparation of the test coupons. Typical nonmetallic materials utilized in oxygen systems are contained in Guide G63.  
1.4 This practice may involve hazardous materials, operations, and equipment. This practice does not purport to address all of the safety concerns associated with its use. It is the responsibility of whomever uses this practice to consult and establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

  • Standard
    5 pages
    English language
    sale 15% off
  • Standard
    5 pages
    English language
    sale 15% off
ASTM
ASTM D4009-92(2023)(Guide)
Standard Guide for Foam Stability of Hand Dishwashing Detergents

SIGNIFICANCE AND USE
3.1 The guide, as now constituted, is not suitable for ranking of hand dishwashing products, since no basis is available at this time for correlation of the foam stability of these products using any particular food soil or combination of soils with consumers' ranking of performance.  
3.2 The relative foam stability ranking of hand dishwashing detergent products will vary greatly depending on the type of food soils used in the test. Therefore, selection of the standard food soil to be used in a test shall be made by agreement between the interested parties on the basis of experience.  
3.3 This laboratory screening guide includes flexibility in several areas so as to allow its use by the maximum number of laboratories, without purchase of significant additional equipment. It should be recognized, therefore, that differences in specific equipment may result in a reduced level of interlaboratory and inter-operator precision, and such results must be evaluated with caution.
SCOPE
1.1 This guide provides guidelines for several techniques of measuring the foam stability of light-duty hand dishwashing detergent products in the presence of artificially applied test-food soils. It is intended as a laboratory screening test to aid in the formulation of products, for quality control and as a basis between the formulator and supplier in standardizing foam stability of the detergents.  
1.2 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.
This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.3 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

  • Guide
    4 pages
    English language
    sale 15% off
ASTM
ASTM D501-03(2023)(Test Method)
Standard Test Methods of Sampling and Chemical Analysis of Alkaline Detergents

ABSTRACT
These test methods cover procedures for the sampling and chemical analysis of inorganic alkaline detergents. These detergents include caustic soda, soda ash, modified soda (sequicarbonate type), sodium bicarbonate, sodium metasilicate, trisodium phosphate, tetrasodium pyrophosphate, borax, and sodium triphosphate. Different tests shall be conducted in order to determine the following properties of the detergents: total alkalinity, matter insoluble in water content, apparent density, ignition loss, pH level, turbidity, temperature rise, and particle size. Chemical analysis of the samples shall be performed by using either reverse-flow ion-exchange chromatography or paper chromatography.
SCOPE
1.1 These test methods cover procedures for the sampling and chemical analysis of inorganic alkaline detergents.  
1.2 The procedures appear in the following order:    
Sections  
Caustic Soda:  
Sampling  
5  
Total Alkalinity as Sodium Oxide (Na2O)  
6 – 8  
Sodium Hydroxide (NaOH)  
9 – 11  
Carbonate as Sodium Carbonate (Na2CO3)  
12  
Carbon Dioxide (CO2) by the Evolution Method  
13 – 16  
Soda Ash:  
Sampling  
17  
Matter Volatile at 150 °C to 155 °C  
18 and 19  
Total Alkalinity as Sodium Carbonate (Na2CO3 )  
20 – 22  
Sodium Bicarbonate (NaHCO3)  
23 – 25  
Sodium Bicarbonate (NaHCO3) by Potentiometric Titration  
26 – 28  
Matter Insoluble in Water  
29 and 30  
Apparent Density  
31 and 32  
Modified Soda (Sequicarbonate Type):  
Sampling  
33  
Total Alkalinity as Sodium Oxide (Na2O)  
34 – 36  
Sodium Bicarbonate (NaHCO3) and Sodium Carbonate (Na2CO3)  
37 – 39  
Matter Insoluble in Water  
40  
Sodium Bicarbonate:  
Sampling  
41  
Sodium Bicarbonate, Sodium Carbonate, and Free Moisture  
42 – 45  
Matter Insoluble in Water  
46  
Sodium Metasilicate, Sodium Sesquisilicate and Sodium Orthosil- icate:  
Sampling  
47  
Total Alkalinity as Sodium Oxide (Na2O)  
48 – 50  
Total Silica as SiO2  
51 – 53  
Sodium Metasilicate (Na2SiO3·5H2O)  
54  
Sodium Sesquisilicate (3Na2O·2SiO2·11H2O)  
55  
Matter Insoluble in Water  
56 and 57  
Loss on Ignition of Sodium Sesquisilicate (3Na2O·2SiO2 ·11H2O)  
58 and 59  
Sodium Orthosilicate (Na4SiO4)  
60  
Trisodium Phosphate:  
Sampling  
61  
Trisodium Phosphate (Na3PO4) Content and Phosphorus Pentoxide (P2O5)  
62 – 64  
Trisodium Phosphate Calculated as Na3PO4·12H2O, Na3PO4· H2O, Na3PO4, and as P2O5  
65 – 68  
Total Alkalinity as Sodium Oxide (Na2O)  
69 – 71  
Matter Insoluble in Water  
72 and 73  
Tetrasodium Pyrophosphate:  
Sampling  
74  
Tetrasodium Pyrophosphate
(Na4P2O7)  
75 – 79  
Matter Insoluble in Water  
80 and 81  
Loss on Ignition  
82 and 83  
Borax:  
Sampling  
84  
Total Borate and Excess Alkalinity or Acidity  
85 – 87  
Matter Insoluble in Water  
88 and 89  
Sodium Triphosphate:  
Sampling  
90  
Tritratable Na2O  
91 – 94  
Total P2O5:  
Preferred Method  
95 – 97  
Alternative Method  
98 – 101  
pH Titration  
102 – 107  
Quantitative Separation and Measurement of Various Phosphates:  
Reverse-Flow Ion-Exchange Chromatography (Preferred Method)  
108 – 119  
Paper Chromatographic Method  
120 – 127  
pH of 1 percent Solution  
128  
Turbidity  
129  
Temperature Rise  
130 – 134  
Sulfate  
135 – 137  
Ignition Loss  
140 and 141  
Matter Insoluble in Water  
142 – 144  
Particle Size  
145  
Orthophosphate  
146 – 151  
1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of th...

  • Standard
    27 pages
    English language
    sale 15% off
ASTM
ASTM D500-95(2023)(Test Method)
Standard Test Methods of Chemical Analysis of Sulfonated and Sulfated Oils

ABSTRACT
These test methods cover the chemical analysis of sulfonated and sulfated oils. Water by distillation with volatile solvent and moisture and volatile matter by hot-plate shall be tested to meet the requirements prescribed. Titration test, extraction-titration test, and ash-gravimetric test shall be performed to meet the requirements specified. Total desulfated fatty matter, total active ingredients, unsaponifiable non-volatile matter, inorganic salts, total alkalinity, and total ammonia shall be tested to meet the requirements prescribed. In the absence of ammonium or triethanolamine soaps test method, brine test method, and in the presence of ammonium or triethanolamine soaps test method shall be performed to meet the requirements prescribed. Water-immiscible organic solvents volatile with steam shall be tested to meet the requirements prescribed.
SCOPE
1.1 These test methods cover the chemical analysis of sulfonated and sulfated oils. The analytical procedures appear in the following order:    
Section  
Moisture:  
Test Method A. Water by Distillation with Volatile Solvent  
4 – 9  
Test Method B. Moisture and Volatile Matter by Hot-Plate Method  
10 – 14  
Organically Combined Sulfuric Anhydride:  
Test Method A. Titration Test  
15 – 19  
Test Method B. Extraction-Titration Test  
20 – 24  
Test Method C. Ash-Gravimetric Test (in the Presence of True
Sulfonates)  
25 – 28  
Total Desulfated Fatty Matter  
29 – 32  
Total Active Ingredients  
33 – 36  
Unsaponifiable Nonvolatile Matter  
37 – 41  
Inorganic Salts  
42 – 46  
Total Alkalinity  
47 – 49  
Total Ammonia  
50 – 52  
Acidity as Free Fatty Acids or Acid Number:  
Test Method A. In the Absence of Ammonium or Triethanolamine Soaps  
53 – 56  
Test Method B. In the Presence of Dark Colored Oils but in the
Absence of Ammonium or Triethanolamine Soaps (Brine Test)  
57 – 60  
Test Method C. In the Presence of Ammonium or Triethanolamine Soaps  
61 – 63  
Water-Immiscible Organic Solvents Volatile with Steam  
64 – 70  
1.2 The values stated in inch-pound units are to be regarded as the standard. The metric equivalents of inch-pound units may be approximate.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. Material Safety Data Sheets are available for reagents and materials. Review them for hazards prior to usage.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

  • Standard
    12 pages
    English language
    sale 15% off
ASTM
ASTM D1570-95(2023)(Test Method)
Standard Test Methods for Sampling and Chemical Analysis of Fatty Alkyl Sulfates

ABSTRACT
These test methods cover the sampling and chemical analysis of paste, powder, or liquid detergent fatty alkyl sulfates. The different procedure for sampling and chemical analysis of past, powder, or liquid detergent are presented and discussed in details. Distillation test, titration test, and gravimetric test shall be performed to meet the requirements prescribed. The calculations methods for chlorides as sodium chloride are presented in details.
SCOPE
1.1 These test methods cover the sampling and chemical analysis of paste, powder, or liquid detergent fatty alkyl sulfates.  
1.2 The procedures for sampling and analysis appear in the following order:    
Sections  
Sampling:  
Powders and Flakes Packed in Cans or Cartons  
4  
Powders and Flakes in Bulk  
5  
Liquids  
6  
Pastes  
7  
Preparation of Sample  
8  
Moisture by the Distillation Test Method  
11 – 14  
pH  
15  
Alkalinity  
16 – 19  
Alcohol-Soluble Matter  
20 – 22  
Alcohol-Insoluble Matter  
23 and 24  
Unsulfated Material  
25 – 28  
Combined Alcohols  
29 – 32  
Ester SO3:  
Method A. Titration Test Method  
36 and 37    
Sections  
Ester SO3:  
Method B. Gravimetric Test Method  
38 and 39  
Sodium Sulfate  
40 – 43  
Chlorides Calculated as Sodium Chloride (NaCl)  
44 – 47  
1.3 The values stated in either inch-pound or SI units are to be regarded separately as the standard. The values given in parentheses are for information only.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. Material Safety Data Sheets are available for reagents and materials. Review them for hazards prior to usage.  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

  • Standard
    10 pages
    English language
    sale 15% off
ASTM
ASTM D820-93(2023)(Test Method)
Standard Test Methods for Chemical Analysis of Soaps Containing Synthetic Detergents

ABSTRACT
These test methods detail the standard procedures for the chemical analysis of soaps containing synthetic detergents. The analytical procedures include the determination of the following chemical properties and substances: moisture and other matter volatile at a specified temperature; free alkali or free acid; anhydrous, salt-free soda soap; alcohol-soluble matter; matter insoluble in water; total alkalinity of matter insoluble in alcohol (alkaline salts); sodium silicate; phosphates; phosphates by colorimetric method using molybdenum blue); unsaponified and unsaponifiable matter; free fatty matter; chlorides in alcohol-soluble matter; rosin by McNicoll method; synthetic detergent by difference; and neutral inorganic salts.
SCOPE
1.1 These test methods cover procedures for the chemical analysis of soaps containing synthetic detergents.  
1.2 The analytical procedures appear in the following order:    
Sections  
Moisture and Other Matter Volatile at 105°C (Oven Method)  
5 and 6  
Free Alkali or Free Acid  
7 and 8  
Anhydrous, Salt-Free, Soda Soap  
9 – 12  
Alcohol-Soluble Matter  
13 and 14  
Matter Insoluble in Water  
15 and 15  
Total Alkalinity of Matter Insoluble in Alcohol (Alkaline Salts)  
16 and 17  
Sodium Silicate  
18 – 20  
Phosphates  
21 – 28  
Phosphate (Colorimetric Method Using Molybdenum Blue)  
29 – 34  
Unsaponified and Unsaponifiable Matter  
35 – 39  
Free Fatty Matter  
40  
Chlorides in Alcohol-Soluble Matter  
41 – 43  
Rosin (McNicoll Method)  
44 – 47  
Synthetic Detergent (by Difference)  
48  
Neutral, Inorganic Salts  
49  
1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.4 This standard does not purport to address all of the safety problems, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

  • Standard
    10 pages
    English language
    sale 15% off
ASTM
ASTM D1173-23(Test Method)
Standard Test Method for Foaming Properties of Surface-Active Agents

ABSTRACT
This test method covers the determination of foaming properties of surface-active agents. Glass tubing apparatus for this test method shall include pipet and a receiver. Apparatus requirements like dimensions, shape, calibration marks, rubber stoppers, etc., shall conform to the specifications as indicated in this standard method. Test solution preparation shall include water preheating, adding the surface-active agent while stirring, and solution aging. Test procedure for foaming properties determination shall be done while surface-active solution is aging as indicated in this standard test method. Report shall include test solution concentration, temperature, water hardness, and foam height.
SCOPE
1.1 This test method covers the determination of the foaming properties of surface-active agents as defined in Terminology D459. This test method is applicable under limited and controlled conditions, but does not necessarily yield information correlating with specific end uses. This method is subjected to the operator of the method as the foam heights are not always level and an average height is determined by the user so it is more of a qualitative measurement in these instances. However, for foam measurements results taken on more flat uniform samples this method has more of a quantitative quality.  
1.2 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.3 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

  • Standard
    3 pages
    English language
    sale 15% off
  • Standard
    3 pages
    English language
    sale 15% off
ASTM
ASTM D502-89(2023)(Test Method)
Standard Test Method for Particle Size of Soaps and Other Detergents

SIGNIFICANCE AND USE
3.1 This test method assures that the particle size of soaps and detergents conforms to specifications having to do with density and packaging, among others. It also offers a means of controlling the amount of potentially hazardous very low particle size material.
SCOPE
1.1 This test method covers the determination of the particle size of soaps and other detergents by hand sieving and machine sieving methods.  
1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. Material Safety Data Sheets are available for reagents and materials. Review them for hazards prior to usage.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

  • Standard
    2 pages
    English language
    sale 15% off