Standard Specification for Zirconium and Zirconium Alloy Forgings

ABSTRACT
This specification covers three grades of zirconium and zirconium alloy forgings. The forgings shall be formed with conventional forging equipment normally found in primary ferrous and nonferrous metal plants. The forgings are furnished in three grades as Grade R60702, Grade R60702, and Grade R60705. Forgings shall be furnished in the annealed conditions. The material shall conform to the requirements as to chemical composition and tensile properties prescribed. Two tension tests shall be made from each lot. Two chemistry tests for hydrogen and nitrogen content shall be made from each lot of finished product. If the results of any tests of any lot do not conform to the requirements specified, retests shall be made on additional forgings of double the original number of the same lot, each of which shall conform to the requirements specified.
SCOPE
1.1 This specification2 covers three grades of zirconium and zirconium alloy forgings (see 4.1).  
1.2 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the two systems may result in non-conformance with the standard.  
1.3 The following safety hazards caveat pertains only to the test method portion, Section 12, of this specification: This standard does not purport to address all of the safety problems, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

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NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
Designation:B493/B493M −14
Standard Specification for
1
Zirconium and Zirconium Alloy Forgings
This standard is issued under the fixed designation B493/B493M; the number immediately following the designation indicates the year
of original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval.
A superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope 4. Classification
2
1.1 This specification covers three grades of zirconium and 4.1 The forgings are furnished in three grades as follows:
zirconium alloy forgings (see 4.1). 4.1.1 Grade R60702—Unalloyed zirconium.
4.1.2 Grade R60704—Zirconium-tin alloy.
1.2 The values stated in either SI units or inch-pound units
4.1.3 Grade R60705—Zirconium-niobium alloy.
are to be regarded separately as standard. The values stated in
each system may not be exact equivalents; therefore, each
5. Ordering Information
system shall be used independently of the other. Combining
5.1 Orders for material under this specification shall include
values from the two systems may result in non-conformance
the following information:
with the standard.
5.1.1 Quantity (weight and number of pieces),
1.3 The following safety hazards caveat pertains only to the
5.1.2 Name of material (zirconium forgings),
test method portion, Section 12, of this specification:This
5.1.3 Finish (Section 9),
standard does not purport to address all of the safety problems,
5.1.4 Dimension (diameter, thickness, length, width, or as
if any, associated with its use. It is the responsibility of the user
specified in appropriate drawings),
of this standard to establish appropriate safety and health
5.1.5 ASTM designation and year of issue,
practices and determine the applicability of regulatory limita-
5.1.6 Grade number (see 4.1), and
tions prior to use.
5.1.7 Additions to the specification and supplementary
requirements, if required, including, but not limited to: product
2. Referenced Documents
marking (see 17.1), check analysis (see 7.3), inspection (see
3
2.1 ASTM Standards:
13.1), lot definition (see 3.1.1), internal soundness (see S1.1),
E8 Test Methods for Tension Testing of Metallic Materials
and surface quality (see S2.1) requirements.
3. Terminology
NOTE 1—A typical ordering description is as follows: 8000-lb zirco-
nium forgings, mechanically descaled, 100 mm by 120 mm by 1.2 m.
3.1 Lot Definition:
rectangular bar, ASTM B493/ 493M - 08, Grade R60702.
3.1.1 forgings, n—parts, including semi-finished products,
or complex shapes, produced by hot mechanical work using
6. Materials and Manufacture
hammers, presses, or forging machines; a lot shall consist of a
6.1 The forgings shall be formed with conventional forging
materialofthesamesize,shape,condition,andfinishproduced
equipment normally found in primary ferrous and nonferrous
from the same ingot or powder blend by the same reduction
metal plants.
schedule and the same heat treatment parameters. Unless
6.2 Forgings shall be furnished in the annealed conditions.
otherwise agreed between manufacturer and purchaser, a lot
shall be limited to the product of an 8 h period for final
7. Chemical Composition
continuous anneal, or to a single furnace load for final batch
anneal. 7.1 The material shall conform to the requirements as to
chemical composition prescribed in Table 1.
1
This specification is under the jurisdiction of ASTM Committee B10 on
7.2 Themanufacturersingotanalysisshallbeconsideredthe
Reactive and Refractory Metals and Alloys and is the direct responsibility of
chemical analysis for forgings, except for hydrogen and
Subcommittee B10.02 on Zirconium and Hafnium.
nitrogen, which shall be determined on the finished product.
Current edition approved May 1, 2014. Published June 2014. Originally
ε1
approved in 1969. Last previous edition approved in 2008 as B493 – 08 . DOI:
7.3 When requested by the purchaser and stated in the
10.1520/B0493_B0493M-14.
2
purchase order, a check analysis for any elements listed in
For ASME Boiler and Pressure Vessel Code applications see related Specifi-
cation SB-493 in Section II of that Code.
Table 1 shall be made on the finished product.
3
For referenced ASTM standards, visit the ASTM website, www.astm.org, or
7.3.1 The manufacturer’s analysis shall be considered as
contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
verified if the check analysis confirms the manufacturer’s
Standards volume information, refer to the standard’s Document Summary page on
the ASTM website. reported values within the tolerances prescribed in Table 2.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
1

---------------------- Page: 1 ----------------------
B493/B493M−14
A
TABLE 1 Chemical Requirem
...

This document is not an ASTM standard and is intended only to provide the user of an ASTM standard an indication of what changes have been made to the previous version. Because
it may not be technically possible to adequately depict all changes accurately, ASTM recommends that users consult prior editions as appropriate. In all cases only the current version
of the standard as published by ASTM is to be considered the official document.
´1
Designation: B493/B493M − 08 B493/B493M − 14
Standard Specification for
1
Zirconium and Zirconium Alloy Forgings
This standard is issued under the fixed designation B493/B493M; the number immediately following the designation indicates the year
of original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval.
A superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1
ε NOTE—An editorial correction was made in 12.1 in February 2010.
1. Scope
2
1.1 This specification covers three grades of zirconium and zirconium alloy forgings.forgings (see 4.1).
1.2 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each
system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the
two systems may result in non-conformance with the standard.
1.3 The following safety hazards caveat pertains only to the test method portion, Section 12, of this specification:This standard
does not purport to address all of the safety problems, if any, associated with its use. It is the responsibility of the user of this
standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.
2. Referenced Documents
3
2.1 ASTM Standards:
E8 Test Methods for Tension Testing of Metallic Materials
3. Terminology
3.1 Lot Definition:
3.1.1 forgings, n—parts, including semi-finished products, or complex shapes, produced by hot mechanical work using
hammers, presses, or forging machines; a lot shall consist of a material of the same size, shape, condition, and finish produced from
the same ingot or powder blend by the same reduction schedule and the same heat treatment parameters. Unless otherwise agreed
between manufacturer and purchaser, a lot shall be limited to the product of an 8 h period for final continuous anneal, or to a single
furnace load for final batch anneal.
4. Classification
4.1 The forgings are furnished in three grades as follows:
4.1.1 Grade R60702—Unalloyed zirconium.
4.1.2 Grade R60704—Zirconium-tin alloy.
4.1.3 Grade R60705—Zirconium-niobium alloy.
5. Ordering Information
5.1 Orders for material under this specification shall include the following information:
5.1.1 Quantity (weight and number of pieces),
5.1.2 Name of material (zirconium forgings),
5.1.3 Finish (Section 9),
5.1.4 Dimension (diameter, thickness, length, width, or as specified in appropriate drawings),
5.1.5 ASTM designation and year of issue,
5.1.6 Grade number (see 3.14.1), and
1
This specification is under the jurisdiction of ASTM Committee B10 on Reactive and Refractory Metals and Alloys and is the direct responsibility of Subcommittee
B10.02 on Zirconium and Hafnium.
Current edition approved Nov. 1, 2008May 1, 2014. Published December 2008June 2014. Originally approved in 1969. Last previous edition approved in 20032008 as
ε1
B493 – 01 (2003).B493 – 08 . DOI: 10.1520/B0493_B0493M-08E01.10.1520/B0493_B0493M-14.
2
For ASME Boiler and Pressure Vessel Code applications see related Specification SB-493 in Section II of that Code.
3
For referenced ASTM standards, visit the ASTM website, www.astm.org, or contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM Standards
volume information, refer to the standard’s Document Summary page on the ASTM website.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
1

---------------------- Page: 1 ----------------------
B493/B493M − 14
5.1.7 Additions to the specification and supplementary requirements, if required, including, but not limited to: product marking
(see 17.1), check analysis (see 7.3), inspection (see 13.1), lot definition (see 3.1.1), internal soundness (see S1.1), and surface
quality (see S2.1) requirements.
NOTE 1—A typical ordering description is as follows: 8000-lb zirconium forgings, mechanically descaled, 100 mm by 120 mm by 1.2 m. rectangular
bar, ASTM B493/ 493M - 08, Grade R60702.
6. Materials and Manufacture
6.1 The forgings shall be formed with conventional forging equipment normally found in primary ferrous and nonferrous metal
plants.
6.2 Forgings shall be furnished in the annealed conditions.
7. Chemical Composition
7.1 The material shall conform to the requirements as to chemical composition prescribed in Table 1.
7.2 The manufacturer’smanufacturers ingot analysis shall be considered the
...

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