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ASTM D5136-17

(Specification)

Standard Specification for High Purity p-Xylene

Standard Specification for High Purity <emph type="ital">p</emph>-Xylene

ABSTRACT
This specification establishes the requirements for p-Xylene. Sampled specimens shall conform to the following physical and chemical properties: minimum purity; maximum m-Xylene content; maximum o-Xylene content; maximum sulfur content; maximum toluene content; maximum ethylbenzene content; maximum nonaromatic hydrocarbons content; appearance; color (Pt/Co scale); distillation range; and maximum pressure.
SCOPE
1.1 This specification covers high purity p-Xylene.  
1.2 The following applies to all specified limits in this specification: for purposes of determining conformance with this specification, an observed value or a calculated value shall be rounded off “to the nearest unit” in the last right-hand digit used in expressing the specification limit, in accordance with the rounding-off method of Practice E29.  
1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.4 Consult current OSHA regulations, supplier’s Safety Data Sheets, and local regulations for all materials used in this specification.  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

General Information

Status
Historical
Publication Date
31-May-2017
ICS
71.080.15 - Aromatic hydrocarbons
Technical Committee
D16 - Aromatic, Industrial, Specialty and Related Chemicals
Drafting Committee
D16.01 - Benzene, Toluene, Xylenes, Cyclohexane and Their Derivatives
Current Stage
Ref Project

Relations

Replaces
ASTM D5136-09(2013) - Standard Specification for High Purity <emph type="ital">p</emph>-Xylene
Effective Date
01-Jun-2017
Replaced By
ASTM D5136-17a - Standard Specification for High Purity <emph type="ital">p</emph>-Xylene
Effective Date
01-Jul-2017
Referred By
ASTM D7504-23 - Standard Test Method for Trace Impurities in Monocyclic Aromatic Hydrocarbons by Gas Chromatography and Effective Carbon Number
Effective Date
01-Jun-2017
Referred By
ASTM D5917-15(2019) - Standard Test Method for Trace Impurities in Monocyclic Aromatic Hydrocarbons by Gas Chromatography and External Calibration
Effective Date
01-Jun-2017

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Standards Content (Sample)

NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
Designation:D5136 −17
Standard Specification for
1
High Purity p-Xylene
This standard is issued under the fixed designation D5136; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope Aromatic Hydrocarbons by Gas Chromatography and
External Calibration
1.1 This specification covers high purity p-Xylene.
D7183 Test Method for Determination of Total Sulfur in
1.2 The following applies to all specified limits in this
Aromatic Hydrocarbons and Related Chemicals by Ultra-
specification: for purposes of determining conformance with
violet Fluorescence
this specification, an observed value or a calculated value shall
D7504 Test Method for Trace Impurities in Monocyclic
be rounded off “to the nearest unit” in the last right-hand digit
Aromatic Hydrocarbons by Gas Chromatography and
used in expressing the specification limit, in accordance with
Effective Carbon Number
the rounding-off method of Practice E29.
E29 Practice for Using Significant Digits in Test Data to
Determine Conformance with Specifications
1.3 The values stated in SI units are to be regarded as
standard. No other units of measurement are included in this E2680 Test Method for Appearance of Clear, Transparent
Liquids (Visual Inspection Procedure)
standard.
2.2 Other Document:
1.4 Consult current OSHA regulations, supplier’s Safety
OSHA Regulations, 29 CFR paragraphs 1910.1000 and
Data Sheets, and local regulations for all materials used in this
3
1910.1200
specification.
1.5 This international standard was developed in accor-
3. Properties
dance with internationally recognized principles on standard-
ization established in the Decision on Principles for the 3.1 High purity p-Xylene shall conform to the following
Development of International Standards, Guides and Recom- requirements:
mendations issued by the World Trade Organization Technical
ASTM
Property Specification
A
Test Method
Barriers to Trade (TBT) Committee.
B
Purity, min, weight % 99.7 D5917 or D7504
m-Xylene, max, weight % 0.20 D5917 or D7504
2. Referenced Documents
o-Xylene, max, weight % 0.10 D5917 or D7504
2
Sulfur, max, mg/kg 1.0 D7183
2.1 ASTM Standards:
Toluene, max, weight % 0.10 D5917 or D7504
D850 Test Method for Distillation of Industrial Aromatic
Ethylbenzene, max, weight % 0.20 D5917 or D7504
Hydrocarbons and Related Materials Nonaromatic hydrocarbons, max, weight % 0.20 D5917 or D7504
Appearance, free of haze, particulates pass E2680
D1209 Test Method for Color of Clear Liquids (Platinum-
or suspended matter particles
Cobalt Scale)
Color, max, Pt/Co scale 10 D1209 or D5386
Distillation range, including the temperature 1.0 D850
D3437 Practice for Sampling and Handling Liquid C
...

This document is not an ASTM standard and is intended only to provide the user of an ASTM standard an indication of what changes have been made to the previous version. Because
it may not be technically possible to adequately depict all changes accurately, ASTM recommends that users consult prior editions as appropriate. In all cases only the current version
of the standard as published by ASTM is to be considered the official document.
Designation: D5136 − 09 (Reapproved 2013) D5136 − 17
Standard Specification for
1
High Purity p-Xylene
This standard is issued under the fixed designation D5136; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope*Scope
1.1 This specification covers high purity p-Xylene.
1.2 The following applies to all specified limits in this specification: for purposes of determining conformance with this
specification, an observed value or a calculated value shall be rounded off “to the nearest unit” in the last right-hand digit used
in expressing the specification limit, in accordance with the rounding-off method of Practice E29.
1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.4 Consult current OSHA regulations, supplier’s Material supplier’s Safety Data Sheets, and local regulations for all materials
used in this specification.
1.5 This international standard was developed in accordance with internationally recognized principles on standardization
established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued
by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
2. Referenced Documents
2
2.1 ASTM Standards:
D850 Test Method for Distillation of Industrial Aromatic Hydrocarbons and Related Materials
D1209 Test Method for Color of Clear Liquids (Platinum-Cobalt Scale)
D3437 Practice for Sampling and Handling Liquid Cyclic Products
D5386 Test Method for Color of Liquids Using Tristimulus Colorimetry
D5917 Test Method for Trace Impurities in Monocyclic Aromatic Hydrocarbons by Gas Chromatography and External
Calibration
D7183 Test Method for Determination of Total Sulfur in Aromatic Hydrocarbons and Related Chemicals by Ultraviolet
Fluorescence
D7504 Test Method for Trace Impurities in Monocyclic Aromatic Hydrocarbons by Gas Chromatography and Effective Carbon
Number
E29 Practice for Using Significant Digits in Test Data to Determine Conformance with Specifications
E2680 Test Method for Appearance of Clear, Transparent Liquids (Visual Inspection Procedure)
2.2 Other Document:
3
OSHA Regulations, 29 CFR paragraphs 1910.1000 and 1910.1200
3. Properties
3.1 High purity p-Xylene shall conform to the following requirements:
ASTM
A
Property Specification Test Method
B
Purity, min, weight % 99.7 D5917 or D7504
m-Xylene, max, weight % 0.20 D5917 or D7504
o-Xylene, max, weight % 0.10 D5917 or D7504
1
This specification is under the jurisdiction of ASTM Committee D16 on Aromatic Hydrocarbons Aromatic, Industrial, Specialty and Related Chemicals and is the direct
responsibility of Subcommittee D16.01 on Benzene, Toluene, Xylenes, Cyclohexane and Their Derivatives.
Current edition approved July 1, 2013June 1, 2017. Published July 2013June 2017. Originally approved in 1990. Last previous edition approved in 20092013 as
D5136 – 09.D5136 – 09 (2013). DOI: 10.1520/D5136-09R13.10.1520/D5136-17.
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM Standards
volume information, refer to the standard’sstandard’s Document Summary page on the ASTM website.
3
Available from U.S. Government Printing Office Superintendent of Documents, 732 N. Capitol St., NW, Mail Stop: SDE, Washington, DC 20401, http://
www.access.gpo.gov.
*A Summary of Changes section appears at the end of this standard
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
1

---------------------- Page: 1 ----------------------
D5136 − 17
Sulfur, max, mg/kg 1.0 D7183
Toluene, max, weight % 0.10 D5917 or D7504
Ethylbenzene, max, weight % 0.20 D5917 or D7504
Nonaromatic hydrocarbons, max, weight % 0.20 D5917 or D7504
C
Appearance .
Color, max, Pt/Co scale 10 D1209 or D5386
Distillation range, including the temperature 1.0 D850
138.3°C at 101.3 kPa (760 mm Hg)
pressure, max, °C
ASTM
Property Specification
A
Test Method
B
Purity, min, weight % 99.7 D5917 or D7504
m-Xylene, max, weight % 0.20 D5917 or D7504
o-Xylene, max, weight % 0.10 D5917 or D7504
Sulfur, max, mg/kg 1.0 D7183
Toluene, max, weight % 0.10 D5917 or D7504
Ethylbenzene, max, weight % 0.20 D5917 or D7504
Nonaromatic hydro
...

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