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ASTM D2494-13(2020)

(Test Method)

Standard Test Method for Commercial Mass of a Shipment of Yarn or Manufactured Staple Fiber or Tow

Standard Test Method for Commercial Mass of a Shipment of Yarn or Manufactured Staple Fiber or Tow

SIGNIFICANCE AND USE
5.1 This test method is considered satisfactory as a referee method for acceptance testing of commercial shipments of yarn or manufactured staple fibers.  
5.1.1 If there are differences of practical significance between reported test results for two laboratories (or more), comparative tests should be performed to determine if there is a statistical bias between them, using competent statistical assistance. As a minimum, use the samples for such a comparative test that are as homogeneous as possible, drawn from the same lot of material as the samples that resulted in disparate results during initial testing and randomly assigned in equal numbers to each laboratory. The test results from the laboratories involved should be compared using a statistical test for unpaired data, a probability level chosen prior to the testing series. If a bias is found, either its casuse must be found and corrected, or future test results for that material must be adjusted in consideration of the known bias.  
5.2 Option I is in common use in other countries, particularly in Europe.4  
5.3 Option II is used to calculate the commercial mass of as-produced manufactured filament yarns (except some producer-textured yarns), manufactured staple fibers, and tows. This option is intended to reflect the mass of fiber remaining after fiber lubricants and processing aids are removed.  
5.4 Option III is used to calculate the commercial mass of spun yarns, textured yarns, tops, and slivers. When materials are sold on a CMRU basis, the purchaser pays for the fiber lubricant or other removable processing aids.  
5.5 Option IV is in common use with impregnated aramids.  
5.6 When it can be shown that solvent extraction or another method of testing gives the same results, or results that have a constant ratio to those obtained by the scour procedure, that method may be used for routine testing of known production but should not be substituted for a scour on new or unknown material. For the determ...
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1.1 This test method provides a measurement of the commercial mass of a shipment of yarn or manufactured staple fiber or tow. This test method applies to (1) yarn of all fiber types except silk, glass, asbestos, and bast; (2) tops and slivers of all fiber types except wool, silk, glass, asbestos, and bast; and (3) manufactured fibers or tow, except glass and other fibers used for special purposes such as flock (Note 1).  
Note 1: For other test methods for measuring mass of fibrous materials, refer to Practice D2720.  
1.1.1 Sampling in this test method is primarily for use in acceptance testing rather than production control. manufactured fiber producers usually sample for the commercial “mass” of product on an on-going basis rather than each shipment to a customer.  
1.2 Commercial mass has been traditionally based on one of three options depending on the state of the material: (1) dried, unscoured yarn, staple fiber, tow, and so forth, using commercial moisture regain in the calculations; (2) dried, scoured yarn, staple fiber, tow, and so forth, using commercial moisture regain values in the calculations; and (3) dried, scoured yarn, staple fiber, tow, and so forth, using a defined allowance in the calculations.  
1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization ...

General Information

Status
Published
Publication Date
31-Jan-2020
ICS
59.080.20 - Yarns
Technical Committee
D13 - Textiles
Drafting Committee
D13.58 - Yarns and Fibers
Current Stage
Ref Project

Relations

Referred By
ASTM D4849-21 - Standard Terminology Related to Yarns and Fibers
Effective Date
01-Feb-2020
Referred By
ASTM D2654-22 - Standard Test Methods for Moisture in Textiles
Effective Date
01-Feb-2020

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ASTM D2494-13(2020) - Standard Test Method for Commercial Mass of a Shipment of Yarn or Manufactured Staple Fiber or TowASTM D2494-13(2020) - Standard Test Method for Commercial Mass of a Shipment of Yarn or Manufactured Staple Fiber or Tow
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ASTM D2494-13(2020) - Standard Test Method for Commercial Mass of a Shipment of Yarn or Manufactured Staple Fiber or Tow
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This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the
Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
Designation: D2494 − 13 (Reapproved 2020)
Standard Test Method for
Commercial Mass of a Shipment of Yarn or Manufactured
1
Staple Fiber or Tow
This standard is issued under the fixed designation D2494; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope mendations issued by the World Trade Organization Technical
Barriers to Trade (TBT) Committee.
1.1 This test method provides a measurement of the com-
mercial mass of a shipment of yarn or manufactured staple
2. Referenced Documents
fiber or tow. This test method applies to (1) yarn of all fiber
2
2.1 ASTM Standards:
types except silk, glass, asbestos, and bast; (2) tops and slivers
of all fiber types except wool, silk, glass, asbestos, and bast; D123 Terminology Relating to Textiles
D629 Test Methods for Quantitative Analysis of Textiles
and (3) manufactured fibers or tow, except glass and other
fibers used for special purposes such as flock (Note 1). D1909 Standard Tables of Commercial Moisture Regains
and Commercial Allowances for Textile Fibers
NOTE 1—For other test methods for measuring mass of fibrous
D2257 Test Method for Extractable Matter in Textiles
materials, refer to Practice D2720.
D2258 Practice for Sampling Yarn for Testing
1.1.1 Sampling in this test method is primarily for use in
D2720 Practice for Calculation of Commercial Weight and
acceptance testing rather than production control. manufac-
Yield of Scoured Wool, Top, and Noil for Various Com-
tured fiber producers usually sample for the commercial
mercial Compositions
“mass” of product on an on-going basis rather than each
D3333 Practice for Sampling Manufactured Staple Fibers,
shipment to a customer.
Sliver, or Tow for Testing
1.2 Commercialmasshasbeentraditionallybasedononeof
D3888 Terminology for Yarn Spinning Systems
three options depending on the state of the material: (1) dried,
D3990 Terminology Relating to Fabric Defects
unscoured yarn, staple fiber, tow, and so forth, using commer-
D4849 Terminology Related to Yarns and Fibers
cialmoistureregaininthecalculations;(2)dried,scouredyarn,
2.2 AATCC Standard:
staple fiber, tow, and so forth, using commercial moisture
150 Dimensional Changes in Automatic Home Laundering
regain values in the calculations; and (3) dried, scoured yarn, 3
of Woven Garments
staple fiber, tow, and so forth, using a defined allowance in the
calculations.
3. Terminology
1.3 The values stated in SI units are to be regarded as
3.1 Definitions:
standard. No other units of measurement are included in this
3.1.1 commercial mass, n—billed mass (weight) as deter-
standard.
mined by a generally accepted method or as agreed upon
1.4 This standard does not purport to address all of the
between the purchaser and the seller.
safety concerns, if any, associated with its use. It is the 3.1.1.1 Discussion—The basis for determining the commer-
responsibility of the user of this standard to establish appro-
cial mass of a shipment of yarn or manufactured fibers is
priate safety, health, and environmental practices and deter- generally one of the following:
mine the applicability of regulatory limitations prior to use.
(1) CAS Basis (commercial allowance with scoured
1.5 This international standard was developed in accor- material)—themassofoven-dryfiberoryarnafterscouringby
dance with internationally recognized principles on standard-
definite prescribed methods plus the mass corresponding to its
ization established in the Decision on Principles for the commercial allowance.
Development of International Standards, Guides and Recom-
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or
1
This test method is under the jurisdiction ofASTM Committee D13 on Textiles contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
and is the direct responsibility of Subcommittee D13.58 on Yarns and Fibers. Standards volume information, refer to the standard’s Document Summary page on
Current edition approved Feb. 1, 2020. Published March 2020. Originally the ASTM website.
3
published as D2494 – 66 T. Last previous edition approved in 2013 as D2494 – 13. Available from the American Association of Textile Chemists and Colorists,
DOI: 10.1520/D2494-13R20. P.O. Box 12215, Research Triangle Park, NC 27709.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
1

---------------------- Page: 1 ----------------------
D2494 − 13 (2020)
(2) CMRS
...

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5.3 The extension force of manufactured filament yarns is related to the alignment of the molecules in the yarn filaments, which influences the yarn processing behavior. Knowledge of this property of partially oriented yarn is useful to determine processing conditions.
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5.1 This is a quick method used for the determination of the approximate yarn number of short-length specimens taken from packages or fabrics.  
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5.1 Test Method D6612 for yarn number and yarn number variability is satisfactory for acceptance of commercial shipments and is used in the trade.  
5.1.1 If there are differences of practical significance between the reported test results for two or more laboratories, comparative tests should be performed by those laboratories to determine if there is a statistical bias between them, using competent statistical assistance. As a minimum, samples used for each comparative tests should be as homogeneous as possible, drawn from the same lot of material as the samples that results in disparate results during initial testing, and randomly assigned in equal numbers to each laboratory. Other fabrics with established tests values are used for this purpose. The test results from the laboratories involved should be compared appropriate statistical analysis and a probability level chosen by the two parties before testing begins, at a probability level chosen prior to the testing series. If a bias is found, either its cause must be found and corrected, or future test results adjusted in consideration of the known bias.  
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1.2 Yarn number variability properties include percent density spread (%DS), coefficient of variation (%CV), density frequency variation.  
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1.3 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system are not necessarily exact equivalents; therefore to ensure conformance with this standard, each system shall be used independently of the other, and values from the two systems shall not be combined.  
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ASTM D2258/D2258M-16(2022)(Practice)
Standard Practice for Sampling Yarn for Testing

SIGNIFICANCE AND USE
5.1 Assigning a value to any property of the material in a container or in a lot, consignment, or delivery involves a measurement process that includes both sampling and testing procedures. The correctness of the value assigned depends upon the variability due to testing and sampling plan. Even when the variability due to testing is minimized by carefully developed procedures, correct and consistent estimates of the true value of the property are possible only when the sampling procedure avoids systematic bias, minimizes variations due to sampling, and provides a laboratory sample of adequate size.  
5.2 Practice D2258 may not give the most efficient sampling plan that might be devised in special situations but does present a general procedure that gives satisfactory precision with an economical amount of sampling. Many plans that include stratified sampling can be found in textbooks and through the use of statistical software tools and calculators.  
5.2.1 If not specified by the purchaser, the manufacturer will define suitable production lots based on one or more of the following: supply lot, production shift/time segment, production equipment or production line, operator, designated shipment, production run, or a combination herein.  
5.2.2 If not specified by the purchaser, the manufacturer will define sampling and testing frequency based on the following: process capability or capability analysis, historical trends, level of detection rate required, confidence level requirements, known variations or special causes, or both. Every attempt to ensure conforming product is being produced, identify potential nonconforming product or proper isolation and identification, will be carried out by the manufacturer.  
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1.1 This practice describes a procedure for the division of shipments of yarn into test lots and the sampling of such lots for testing.  
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1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
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ASTM D1423/D1423M-16(2022)(Test Method)
Standard Test Method for Twist in Yarns by Direct-Counting

SIGNIFICANCE AND USE
5.1 Test Method D1423 for testing twist in yarns by direct-counting is considered satisfactory for acceptance testing of commercial shipments because current estimates of between-laboratory precision are acceptable and the method has been used extensively in the trade for acceptance testing.  
5.1.1 If there are differences of practical significance between reported test results for two laboratories (or more), comparative tests should be performed to determine if there is a statistical bias between them, using competent statistical assistance. As a minimum use the samples for such comparative tests as homogeneous as possible, drawn from the same lot of material that resulted in the disparate test results and randomly in equal numbers to each laboratory. The test results from the laboratories involved should be compared using a statistical test for unpaired data, at a probability level chosen prior to the testing series. If a bias is found, either its cause must be found and corrected, or future test results for that material must be adjusted in consideration of the known bias.  
5.2 The determination of twist in a straight section of a yarn is not the simple straightforward operation it appears to be, for the test results may be greatly influenced by variations in test procedures and techniques. In all manipulations, extreme care is necessary to prevent specimen rotation altering the twist level before testing begins.  
5.3 The twist in a yarn before it is packaged may be different from that of the yarn after it has been withdrawn from the package because of changes in tension and the effect of the method of withdrawal. If the yarn is withdrawn over-end, a slight increase or decrease in twist will take place, depending upon the direction of the twist in the yarn, the direction of winding on the package, and the length of the wrap on the package.  
5.4 When a yarn is incorporated into or removed from a more complex structure, alterations may occur as a result of ...
SCOPE
1.1 This test method covers the determination of the amount and direction of twist at the completion of any stage of twisting in single (spun or filament), plied, cabled, or novelty (exclusive of long-term repeat patterns) yarns. The procedures are designed primarily for yarns in packages, but, with special precautions, they are applicable to yarns taken from fabrics. The procedure for spun yarn in 9.2 is also applicable to rovings.  
1.2 For plied yarns, this test method covers the determination of the twist of the plied yarns and the twist of the single yarn before plying. For cabled yarns, the test method covers the determination of the cable or hawser twist; the twist of the plied yarn after plying, but prior to the last twisting operation; and the twist of the single yarn before plying. Procedures are also included for the determination of the twists of the single and plied yarn components as they lie in the final structure. Also, directions are included for the determination of twist in plied yarn made with direct cabling technology.  
1.3 This test method is not intended for yarns that extend more than 5.0 % when tension is increased from 2.5 to 7.5 mN/tex [0.25 to 0.75 gf/tex]. Following the procedures of this test method for such yarns would be independent of the bias and precision determined for this test method. The report from such testing should include the tension used for this testing.  
1.4 Units—The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system are not necessarily exact equivalents; therefore, to ensure conformance with the standard, each system shall be used independently of the other, and values from the two systems shall not be combined.
Note 1: For a more rapid but less accurate method of determining twist in single spun yarns, refer to Test Method D1422.
Note 2: This test method has been evaluated for use in de...

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ASTM
ASTM D2731-21(Test Method)
Standard Test Method for Elastic Properties of Elastomeric Yarns (CRE Type Tensile Testing Machines)

SIGNIFICANCE AND USE
5.1 This test method is considered satisfactory for acceptance testing of commercial shipments since current estimates of between-laboratory precision are acceptable and the method is used extensively in the trade for acceptance testing.  
5.1.1 If there are differences of practical significance between reported test results for two laboratories (or more), comparative tests should be performed to determine if there is a statistical bias between them, using competent statistical assistance. As a minimum, use samples for such comparative tests that are as homogeneous as possible, drawn from the same lot of material as the samples that resulted in disparate results during initial testing, and randomly assigned in equal numbers to each laboratory. The test results from the laboratories involved should be compared using a statistical test for unpaired data, at a probability level chosen prior to the testing series. If bias is found, either its cause must be found and corrected, or future test results for that material must be adjusted in consideration of the known bias.  
5.2 Force at Specified Elongation (FASE) is a measure of the tensile force occurring while extending a textile material within specified limits. This characteristic of elastomeric yarn indicates the resistance that will have to be overcome by the wearer while putting on a garment made of the material and is also an indication of the garment's resistance to deformation caused by normal body movements during wear. The elongations used for these measurements are typically 100 %, 200 % and 300 %.  
5.3 Permanent Deformation (set) is a measure of the increase in length of an elastomeric yarn resulting from cyclic stretching and relaxation. The characteristic is a visible indication of the realignment of intermolecular bonds within the elastic material. As with stress decay, the amount of set increases with yarn extension; however, for any particular extension, little or no additional set takes place after...
SCOPE
1.1 This test method covers the determination of elastic properties of “as produced” elastomeric yarns made from rubber, spandex or other elastomers. Elastic properties include force at specified elongations, permanent deformation and stress decay. Other hysteresis related properties can be calculated.
Note 1: For a method designed specifically for testing rubber threads, refer to Test Method D2433.  
1.2 This test method is not applicable to covered, wrapped, or core-spun yarns or yarns spun from elastomeric staple.  
1.3 This test method is applicable to elastomeric yarns having a range of 40 to 3200 dtex (36 to 2900 denier).  
1.4 The values stated in either SI units or U.S. Customary units are to be regarded separately as standard. Within the text, the U.S. Customary units are in parentheses. The values stated in each system are not exact equivalents; therefore, each system shall be used independently of the other.  
1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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ASTM
ASTM D204-02(2021)(Test Method)
Standard Test Methods for Sewing Threads

SIGNIFICANCE AND USE
4.1 Acceptance Testing—The test methods in Test Methods D204 for the determination of the properties of sewing thread are considered satisfactory for acceptance testing of commercial shipments of sewing thread, unless specified in the individual test method. These test methods are the best available and are used extensively in the trade.  
4.1.1 If there are differences of practical significance between reported test results for two laboratories (or more) comparative test should be performed to determine if there is a statistical bias between them using competent statistical assistance. As a minimum, use the samples for such a comparative tests that are as homogeneous as possible, drawn from the same lot of material as the samples that resulted in disparate results during initial testing and randomly assigned in equal numbers to each laboratory. The test results from the laboratories involved should be compared using a statistical test for unpaired data, a probability level chosen prior to the testing series. If a bias is found, either its cause must be found and corrected, or future test results for that material must be adjusted in consideration of the known bias.
SCOPE
1.1 These test methods can be used to evaluate sewing threads of any fiber.  
1.1.1 The test methods in this standard are intended to evaluate only sewing thread taken from thread holders.  
1.2 These test methods only provide for the measurement of sewing thread physical properties. These test methods do not address any other properties that may be important for the satisfactory performance of sewing threads under particular end use conditions.  
1.3 These test methods can be used to measure the following properties:    
Sections  
Colorfastness to Drycleaning  
73 – 83  
Colorfastness to Laundering  
62 – 72  
Colorfastness to Water Migration  
84 – 94  
Diameter  
43 – 50  
Length per Thread Holder  
34 – 42  
Shrinkage, Single Strand  
51 – 61  
Dry Heat  
58.1  
Boiling Water  
58.2  
Strength and Elongation  
15 – 21  
Single Strand—Conditioned  
19.1.1  
Single Strand—Wet  
19.1.2  
Loop Strength  
19.2  
Knot Strength  
19.3  
Twist  
22 – 27  
Twist Balance  
28 – 33  
Yarn Number  
7 – 14
Note 1: For methods covering tests on prepared seams, refer to Test Methods D1683/D1683M and D3940.  
1.4 The values stated in SI units are to be regarded as standard. The values given in parentheses after SI units are provided for information only and are not considered standard.  
1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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