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ASTM D6774-22

(Test Method)

Standard Test Method for Crimp and Shrinkage Properties for Textured Yarns Using a Dynamic Textured Yarn Tester

Standard Test Method for Crimp and Shrinkage Properties for Textured Yarns Using a Dynamic Textured Yarn Tester

SIGNIFICANCE AND USE
5.1 Test Method D6774, for determining maximum total contraction, crimp, and residual fiber shrinkage in textured filament yarns is suitable for acceptance testing of commercial shipments.  
5.1.1 If there are differences of practical significance between reported test results for two laboratories (or more), comparative tests should be performed to determine if there is a statistical bias between them, using competent statistical assistance. As a minimum, use the samples for such a comparative tests that are as homogeneous as possible, drawn from the same lot of material as the samples that resulted in disparate results during initial testing and randomly assigned in equal numbers to each laboratory. The test results from the laboratories involved should be compared using a statistical test for unpaired data, a probability level chosen prior to the testing series. If a bias is found, either its cause must be found and corrected, or future test results for that material must be adjusted in consideration of the known bias.  
5.2 The properties and their variability as measured by this method relate to bulk appearance, stretch and recovery of fabrics and dyeability of yarns.  
5.3 For some yarns, elapsed time between processing and testing has a marked effect on the results, of this test, especially during the first 72 h. The effect is caused by stress decay which is known to be minimal beyond the seventh day and after which time the yarn remains relatively stable. Therefore, specimens should only be compared if tested after the same elapsed time. Samples can be tested at-line, thus having little to no elapsed time between processing and testing.
SCOPE
1.1 This test method covers the determination of crimp contraction, residual fiber shrinkage and their variability of all types of filament yarns (partially oriented yarn (POY), fully oriented yarn (FOY), flat yarns, textured and bulked continuous filament (BCF) carpet yarns) using an automated tester.
Note 1: For another method of testing crimp in textured yarns, refer to Test Method D4031.  
1.1.1 This method may also be used for non-textured yarns.  
1.2 This test method is limited to crimped, multi-filament yarns ranging from 22.0 dtex to 890 dtex (15 denier to 800 denier) and for BCF yarns from 890 dtex to 4200 dtex (800 denier to 3800 denier).  
1.3 The values stated in SI units are to be regarded as standard. Inch-pound units in parentheses after SI units are provided for information only and are not considered standard.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

General Information

Status
Published
Publication Date
28-Feb-2022
ICS
59.080.20 - Yarns
Technical Committee
D13 - Textiles
Drafting Committee
D13.58 - Yarns and Fibers
Current Stage
Ref Project

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ASTM D6774-22 - Standard Test Method for Crimp and Shrinkage Properties for Textured Yarns Using a Dynamic Textured Yarn TesterASTM D6774-22 - Standard Test Method for Crimp and Shrinkage Properties for Textured Yarns Using a Dynamic Textured Yarn Tester
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ASTM D6774-22 - Standard Test Method for Crimp and Shrinkage Properties for Textured Yarns Using a Dynamic Textured Yarn Tester
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This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the
Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
Designation: D6774 − 22
Standard Test Method for
Crimp and Shrinkage Properties for Textured Yarns Using a
1
Dynamic Textured Yarn Tester
This standard is issued under the fixed designation D6774; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope D2258 Practice for Sampling Yarn for Testing
D4031 Test Method for Bulk Properties of Textured Yarns
1.1 This test method covers the determination of crimp
D4849 Terminology Related to Yarns and Fibers
contraction, residual fiber shrinkage and their variability of all
types of filament yarns (partially oriented yarn (POY), fully
3. Terminology
oriented yarn (FOY), flat yarns, textured and bulked continu-
3.1 For definitions of textile terms in this test method, refer
ous filament (BCF) carpet yarns) using an automated tester.
to Terminology D4849. For other textile terms used in this test
NOTE 1—For another method of testing crimp in textured yarns, refer to
method, refer to Terminology D123.
Test Method D4031.
1.1.1 This method may also be used for non-textured yarns.
4. Summary of Test Method
1.2 This test method is limited to crimped, multi-filament
4.1 The specimen passes through a pretension device to
yarns ranging from 22.0 dtex to 890 dtex (15 denier to 800
remove crimp. The specimen then passes, at a constant speed,
denier) and for BCF yarns from 890 dtex to 4200 dtex (800
around an input roller, to a calibrated sensor which maintains a
denier to 3800 denier).
specific tension.
4.1.1 Subsequently, the specimen passes through a heating
1.3 The values stated in SI units are to be regarded as
element, at a low tension, where the specimen shrinks and
standard. Inch-pound units in parentheses after SI units are
again is crimped.
provided for information only and are not considered standard.
4.1.2 The crimped specimen then goes to an intermediate
1.4 This standard does not purport to address all of the
roll, at a low tension.
safety concerns, if any, associated with its use. It is the
4.1.3 The specimen then travels to a second sensor, which
responsibility of the user of this standard to establish appro-
maintains a tension equal to the pretension applied, to remove
priate safety, health, and environmental practices and deter-
developed crimp.
mine the applicability of regulatory limitations prior to use.
4.2 Residual fiber shrinkage, crimp developed, and maxi-
1.5 This international standard was developed in accor-
mum total contraction are calculated by the computer software
dance with internationally recognized principles on standard-
using speeds of the input, intermediate and output rolls.
ization established in the Decision on Principles for the
Development of International Standards, Guides and Recom-
5. Significance and Use
mendations issued by the World Trade Organization Technical
Barriers to Trade (TBT) Committee.
5.1 Test Method D6774, for determining maximum total
contraction, crimp, and residual fiber shrinkage in textured
2. Referenced Documents
filament yarns is suitable for acceptance testing of commercial
2
shipments.
2.1 ASTM Standards:
5.1.1 If there are differences of practical significance be-
D123 Terminology Relating to Textiles
tween reported test results for two laboratories (or more),
comparative tests should be performed to determine if there is
1
This test method is under the jurisdiction ofASTM Committee D13 on Textiles
a statistical bias between them, using competent statistical
and is the direct responsibility of Subcommittee D13.58 on Yarns and Fibers.
assistance. As a minimum, use the samples for such a com-
Current edition approved March 1, 2022. Published March 2022. Originally
parative tests that are as homogeneous as possible, drawn from
approved in 2002. Last previous edition approved in 2010 as D6774 – 02 (2010)
thesamelotofmaterialasthesamplesthatresultedindisparate
which was withdrawn January 2019 and reinstated March 2022. DOI: 10.1520/
D6774-22.
results during initial testing and randomly assigned in equal
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or
numbers to each laboratory. The test results from the labora-
contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
tories involved should be compared using a statistical test for
Standards volume information, refer to the standard’s Document Summary page on
the ASTM website. unpaired data, a probability level chosen prior to the testing
Copyright © ASTM Internationa
...

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5.1 This test method is considered satisfactory for acceptance testing of commercial shipments because current estimates of between-laboratory precision are acceptable and the method is used extensively in the trade for acceptance testing.  
5.1.1 If there are differences or practical significance between reported test results for two laboratories (or more), comparative tests should be performed to determine if there is a statistical bias between them, using competent statistical assistance. As a minimum, the test samples to be used are as homogeneous as possible, are drawn from the material from which the disparate test results are obtained, and are assigned randomly in equal numbers to each laboratory for testing. Other materials with established test values may be used for this purpose. The test results from the two laboratories should be compared using a statistical test for unpaired data, at a probability level chosen prior to the testing series. If a bias is found, either its cause must be found and corrected, or future test results must be adjusted in consideration of the known bias.  
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5.3 The extension force of manufactured filament yarns is related to the alignment of the molecules in the yarn filaments, which influences the yarn processing behavior. Knowledge of this property of partially oriented yarn is useful to determine processing conditions.
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Standard Test Method for Yarn Number Based on Short-Length Specimens

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5.1 This is a quick method used for the determination of the approximate yarn number of short-length specimens taken from packages or fabrics.  
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5.1 This test method may be used for the acceptance testing of commercial shipments of yarns and cords. Caution is advised because yarn and cord may contract in length over a period of time due to room temperature retraction. Thermal shrinkage values are reduced proportionately by the amount of room temperature retraction.
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5.1 Test Method D1423 for testing twist in yarns by direct-counting is considered satisfactory for acceptance testing of commercial shipments because current estimates of between-laboratory precision are acceptable and the method has been used extensively in the trade for acceptance testing.  
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1.3 This test method is not intended for yarns that extend more than 5.0 % when tension is increased from 2.5 to 7.5 mN/tex [0.25 to 0.75 gf/tex]. Following the procedures of this test method for such yarns would be independent of the bias and precision determined for this test method. The report from such testing should include the tension used for this testing.  
1.4 Units—The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system are not necessarily exact equivalents; therefore, to ensure conformance with the standard, each system shall be used independently of the other, and values from the two systems shall not be combined.
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ASTM D2258/D2258M-16(2022)(Practice)
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5.1 Assigning a value to any property of the material in a container or in a lot, consignment, or delivery involves a measurement process that includes both sampling and testing procedures. The correctness of the value assigned depends upon the variability due to testing and sampling plan. Even when the variability due to testing is minimized by carefully developed procedures, correct and consistent estimates of the true value of the property are possible only when the sampling procedure avoids systematic bias, minimizes variations due to sampling, and provides a laboratory sample of adequate size.  
5.2 Practice D2258 may not give the most efficient sampling plan that might be devised in special situations but does present a general procedure that gives satisfactory precision with an economical amount of sampling. Many plans that include stratified sampling can be found in textbooks and through the use of statistical software tools and calculators.  
5.2.1 If not specified by the purchaser, the manufacturer will define suitable production lots based on one or more of the following: supply lot, production shift/time segment, production equipment or production line, operator, designated shipment, production run, or a combination herein.  
5.2.2 If not specified by the purchaser, the manufacturer will define sampling and testing frequency based on the following: process capability or capability analysis, historical trends, level of detection rate required, confidence level requirements, known variations or special causes, or both. Every attempt to ensure conforming product is being produced, identify potential nonconforming product or proper isolation and identification, will be carried out by the manufacturer.  
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SCOPE
1.1 This practice describes a procedure for the division of shipments of yarn into test lots and the sampling of such lots for testing.  
1.1.1 This practice can be used for lot sample testing of yarns for both pre-fabric production and post-fabric production.  
1.2 This practice is applicable to single, plied, or cabled yarns, and cords, made of any fiber or mixture of fibers, and supported on any form of package, including beams.  
1.3 This practice also describes procedures for the sampling of yarn(s) removed from woven or knitted fabrics; however, when thus sampled, the yarns are usually not representative of entire shipments, as referred to in 1.1. Consequently, the resultant sampling can only be used to determine the characteristics of the yarn and is usually not used for acceptance testing. Moreover, it should be recognized that the characteristics of yarns from fabrics may be different than the characteristics of the same yarn(s), prior to being entered into the fabric manufacturing process.  
1.4 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system are not necessarily exact equivalents; therefore, to ensure conformance with the standard, each system shall be used independently of the other, and values from the two systems shall not be combined.  
1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical...

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ASTM D6612-00(2022)(Test Method)
Standard Test Method for Yarn Number and Yarn Number Variability Using Automated Tester

SIGNIFICANCE AND USE
5.1 Test Method D6612 for yarn number and yarn number variability is satisfactory for acceptance of commercial shipments and is used in the trade.  
5.1.1 If there are differences of practical significance between the reported test results for two or more laboratories, comparative tests should be performed by those laboratories to determine if there is a statistical bias between them, using competent statistical assistance. As a minimum, samples used for each comparative tests should be as homogeneous as possible, drawn from the same lot of material as the samples that results in disparate results during initial testing, and randomly assigned in equal numbers to each laboratory. Other fabrics with established tests values are used for this purpose. The test results from the laboratories involved should be compared appropriate statistical analysis and a probability level chosen by the two parties before testing begins, at a probability level chosen prior to the testing series. If a bias is found, either its cause must be found and corrected, or future test results adjusted in consideration of the known bias.  
5.1.2 The average results from the two laboratories should be compared using appropriate statistical analysis and a probability level chosen by the two parties before the testing is begun. If a bias is found, either its cause must be found and corrected or the purchaser and the supplier must agree to interpret future test results with consideration to the known bias.  
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1.1 This test method covers the measurement of yarn number up to 4000 dtex (3600 denier) and related variability properties of filament and spun yarns using an automated tester with capability for measuring mass variability characteristics.  
1.2 Yarn number variability properties include percent density spread (%DS), coefficient of variation (%CV), density frequency variation.  
Note 1: For determination of yarn number by use of reel and balance, refer to Test Method D1907. For another method of measuring variability (unevenness) in yarn, refer to Test Method D1425.  
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1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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Standard Test Method for Tensile Properties of Yarns by the Single-Strand Method

SIGNIFICANCE AND USE
5.1 Acceptance Testing—Option A1 of Test Method D2256 is considered satisfactory for acceptance testing of commercial shipments because the test method has been used extensively in the trade for acceptance testing. However, this statement is not applicable to knot and loop breaking force tests, tests on wet specimens, tests on oven-dried specimens, or tests on specimens exposed to low or high temperatures and should be used with caution for acceptance testing because factual information on between-laboratory precision and bias is not available.  
5.1.1 If there are differences of practical significance between reported test results for two laboratories (or more), comparative tests should be performed to determine if there is a statistical bias between them, using competent statistical assistance. As a minimum, use the samples for such a comparative tests that are as homogeneous as possible, drawn from the same lot of material as the samples that resulted in disparate results during initial testing and randomly assigned in equal numbers to each laboratory. The test results from the laboratories involved should be compared using a statistical test for unpaired data, a probability level chosen prior to the testing series. If a bias is found, either its cause must be found and corrected, or future test results for that material must be adjusted in consideration of the known bias.  
5.2 Fundamental Properties—The breaking tenacity, calculated from the breaking force and the linear density, and the elongation are fundamental properties that are widely used to establish limitations on yarn processing or conversion and on their end-use applications. Initial modulus is a measure of the resistance of the yarn to extension at forces below the yield point. The chord modulus is used to estimate the resistance to imposed strain. The breaking toughness is a measure of the work necessary to break the yarn.  
5.3 Comparison to Skein Testing—The single-strand method gives a more a...
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1.1 This test method covers the determination of tensile properties of monofilament, multifilament, and spun yarns, either single, plied, or cabled with the exception of yarns that stretch more than 5.0 % when tension is increased from 0.05 to 1.0 cN/tex [0.5 to 1.0 gf/tex].  
1.2 This test method covers the measurement of breaking force and elongation of yarns and includes directions for the calculation of breaking tenacity, initial modulus, chord modulus, and breaking toughness.  
1.2.1 Options are included for the testing of specimens in: (A) straight, (B) knotted, and (C) looped form.  
1.2.2 Conditions of test are included for the testing of specimens that are: (1) conditioned air, (2) wet, not immersed, (3) wet, immersed, (4) oven-dried, (5) exposed to elevated temperature, or (6) exposed to low temperature.  
Note 1: Special methods for testing yarns made from specific fibers; namely, glass, flax, hemp, ramie, and kraft paper and for specific products; namely, tire cords and rope, have been published: Test Methods D885, and Specification D578.
Note 2: For directions covering the determination of breaking force of yarn by the skein method refer to Test Method D1578.  
1.3 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the two systems may result in non-conformance with the standard.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization estab...

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ASTM
ASTM D2731-21(Test Method)
Standard Test Method for Elastic Properties of Elastomeric Yarns (CRE Type Tensile Testing Machines)

SIGNIFICANCE AND USE
5.1 This test method is considered satisfactory for acceptance testing of commercial shipments since current estimates of between-laboratory precision are acceptable and the method is used extensively in the trade for acceptance testing.  
5.1.1 If there are differences of practical significance between reported test results for two laboratories (or more), comparative tests should be performed to determine if there is a statistical bias between them, using competent statistical assistance. As a minimum, use samples for such comparative tests that are as homogeneous as possible, drawn from the same lot of material as the samples that resulted in disparate results during initial testing, and randomly assigned in equal numbers to each laboratory. The test results from the laboratories involved should be compared using a statistical test for unpaired data, at a probability level chosen prior to the testing series. If bias is found, either its cause must be found and corrected, or future test results for that material must be adjusted in consideration of the known bias.  
5.2 Force at Specified Elongation (FASE) is a measure of the tensile force occurring while extending a textile material within specified limits. This characteristic of elastomeric yarn indicates the resistance that will have to be overcome by the wearer while putting on a garment made of the material and is also an indication of the garment's resistance to deformation caused by normal body movements during wear. The elongations used for these measurements are typically 100 %, 200 % and 300 %.  
5.3 Permanent Deformation (set) is a measure of the increase in length of an elastomeric yarn resulting from cyclic stretching and relaxation. The characteristic is a visible indication of the realignment of intermolecular bonds within the elastic material. As with stress decay, the amount of set increases with yarn extension; however, for any particular extension, little or no additional set takes place after...
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1.1 This test method covers the determination of elastic properties of “as produced” elastomeric yarns made from rubber, spandex or other elastomers. Elastic properties include force at specified elongations, permanent deformation and stress decay. Other hysteresis related properties can be calculated.
Note 1: For a method designed specifically for testing rubber threads, refer to Test Method D2433.  
1.2 This test method is not applicable to covered, wrapped, or core-spun yarns or yarns spun from elastomeric staple.  
1.3 This test method is applicable to elastomeric yarns having a range of 40 to 3200 dtex (36 to 2900 denier).  
1.4 The values stated in either SI units or U.S. Customary units are to be regarded separately as standard. Within the text, the U.S. Customary units are in parentheses. The values stated in each system are not exact equivalents; therefore, each system shall be used independently of the other.  
1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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ASTM
ASTM D204-02(2021)(Test Method)
Standard Test Methods for Sewing Threads

SIGNIFICANCE AND USE
4.1 Acceptance Testing—The test methods in Test Methods D204 for the determination of the properties of sewing thread are considered satisfactory for acceptance testing of commercial shipments of sewing thread, unless specified in the individual test method. These test methods are the best available and are used extensively in the trade.  
4.1.1 If there are differences of practical significance between reported test results for two laboratories (or more) comparative test should be performed to determine if there is a statistical bias between them using competent statistical assistance. As a minimum, use the samples for such a comparative tests that are as homogeneous as possible, drawn from the same lot of material as the samples that resulted in disparate results during initial testing and randomly assigned in equal numbers to each laboratory. The test results from the laboratories involved should be compared using a statistical test for unpaired data, a probability level chosen prior to the testing series. If a bias is found, either its cause must be found and corrected, or future test results for that material must be adjusted in consideration of the known bias.
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1.1 These test methods can be used to evaluate sewing threads of any fiber.  
1.1.1 The test methods in this standard are intended to evaluate only sewing thread taken from thread holders.  
1.2 These test methods only provide for the measurement of sewing thread physical properties. These test methods do not address any other properties that may be important for the satisfactory performance of sewing threads under particular end use conditions.  
1.3 These test methods can be used to measure the following properties:    
Sections  
Colorfastness to Drycleaning  
73 – 83  
Colorfastness to Laundering  
62 – 72  
Colorfastness to Water Migration  
84 – 94  
Diameter  
43 – 50  
Length per Thread Holder  
34 – 42  
Shrinkage, Single Strand  
51 – 61  
Dry Heat  
58.1  
Boiling Water  
58.2  
Strength and Elongation  
15 – 21  
Single Strand—Conditioned  
19.1.1  
Single Strand—Wet  
19.1.2  
Loop Strength  
19.2  
Knot Strength  
19.3  
Twist  
22 – 27  
Twist Balance  
28 – 33  
Yarn Number  
7 – 14
Note 1: For methods covering tests on prepared seams, refer to Test Methods D1683/D1683M and D3940.  
1.4 The values stated in SI units are to be regarded as standard. The values given in parentheses after SI units are provided for information only and are not considered standard.  
1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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