Fertilizers - Determination of sulfates content using three different methods

This document specifies three different methods (Methods A, B and C) for the determination of sulfur present in fertilizers extracts in the form of sulfates. Method A specifies the gravimetric method. Method B specifies the method using inductively coupled plasma optical spectrometry (ICP-OES). Method C specifies the method using ion chromatography (IC).

Düngemittel - Bestimmung von Sulfat mit drei verschiedenen Verfahren

Diese Europäische Norm legt drei verschiedene Verfahren (Verfahren A, B und C) für die Bestimmung des in Düngemittelextrakten vorliegenden Schwefels in Form von Sulfaten fest. Als Verfahren A ist das gravimetrische Verfahren festgelegt. Als Verfahren B ist die Bestimmung mittels optischer Emissionsspektro¬metrie mit induktiv gekoppeltem Plasma (ICP OES) festgelegt. Als Verfahren C ist die Vorgehensweise mittels Ionenchromatographie (IC) festgelegt.

Engrais - Dosage des sulfates selon trois méthodes différentes

La présente norme européenne spécifie trois méthodes différentes (méthodes A, B et C) de dosage du soufre présent dans les extraits d’engrais sous forme de sulfate. La méthode A utilise la gravimétrie. La méthode B emploie la spectrométrie d’émission optique à plasma inductif (ICP-OES). La méthode C a recours à la chromatographie ionique (IC).

Gnojila - Določevanje sulfatov s tremi različnimi metodami

Ta evropski standard opredeljuje tri različne metode (Metodo A, B in C) za določanje žvepla, prisotnega v ekstraktih gnojil v obliki sulfatov. Metoda A določa gravimetrično metodo. Metoda B določa metodo z uporabo optične spektrometrije z induktivno sklopljeno plazmo (ICP-OES). Metoda C določa metodo z uporabo ionske kromatografije (IC).

General Information

Status
Withdrawn
Publication Date
27-Oct-2009
Withdrawal Date
09-Aug-2022
Current Stage
9960 - Withdrawal effective - Withdrawal
Completion Date
10-Aug-2022

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2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.Düngemittel - Bestimmung von Sulfat mit drei verschiedenen VerfahrenEngrais - Dosage des sulfates selon trois méthodes différentesFertilizers - Determination of sulfates content using three different methods65.080GnojilaFertilizersICS:Ta slovenski standard je istoveten z:EN 15749:2009SIST EN 15749:2010en,fr,de01-februar-2010SIST EN 15749:2010SLOVENSKI
STANDARDSIST-TS CEN/TS 15749:20081DGRPHãþD



SIST EN 15749:2010



EUROPEAN STANDARD NORME EUROPÉENNE EUROPÄISCHE NORM
EN 15749
October 2009 ICS 65.080 Supersedes CEN/TS 15749:2008English Version
Fertilizers - Determination of sulfates content using three different methods
Engrais - Dosage des sulfates selon trois méthodes différentes
Düngemittel - Bestimmung von Sulfat mit drei verschiedenen Verfahren This European Standard was approved by CEN on 20 September 2009.
CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this European Standard the status of a national standard without any alteration. Up-to-date lists and bibliographical references concerning such national standards may be obtained on application to the CEN Management Centre or to any CEN member.
This European Standard exists in three official versions (English, French, German). A version in any other language made by translation under the responsibility of a CEN member into its own language and notified to the CEN Management Centre has the same status as the official versions.
CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Cyprus, Czech Republic, Denmark, Estonia, Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland and United Kingdom.
EUROPEAN COMMITTEE FOR STANDARDIZATION
COMITÉ EUROPÉEN DE NORMALISATION EUROPÄISCHES KOMITEE FÜR NORMUNG
Management Centre:
Avenue Marnix 17,
B-1000 Brussels © 2009 CEN All rights of exploitation in any form and by any means reserved worldwide for CEN national Members. Ref. No. EN 15749:2009: ESIST EN 15749:2010



EN 15749:2009 (E) 2 Contents Page Foreword .3Introduction .41Scope .52Normative references .53Terms and definitions .54Principle .55Sampling and sample preparation .66Method A – Gravimetric method .67Method B – ICP-OES method .78Method C – IC method . 119Precision of methods A, B and C . 1710Test report . 18Annex A (informative)
Statistical results of the inter-laboratory tests . 19Bibliography . 22 SIST EN 15749:2010



EN 15749:2009 (E) 3 Foreword This document (EN 15749:2009) has been prepared by Technical Committee CEN/TC 260 “Fertilizers and liming materials”, the secretariat of which is held by DIN. This European Standard shall be given the status of a national standard, either by publication of an identical text or by endorsement, at the latest by April 2010, and conflicting national standards shall be withdrawn at the latest by April 2010. Attention is drawn to the possibility that some of the elements of this document may be the subject of patent rights. CEN [and/or CENELEC] shall not be held responsible for id
...

SLOVENSKI STANDARD
kSIST FprEN 15749:2009
01-julij-2009
*QRMLOD'RORþHYDQMHVXOIDWRYVWUHPLUD]OLþQLPLPHWRGDPL
Fertilizers - Determination of sulfates content using three different methods
Düngemittel - Bestimmung von Sulfat mit drei verschiedenen Verfahren
Engrais - Dosage des sulfates selon trois méthodes différentes
Ta slovenski standard je istoveten z: FprEN 15749
ICS:
65.080 Gnojila Fertilizers
kSIST FprEN 15749:2009 en,fr,de
2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.

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kSIST FprEN 15749:2009

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kSIST FprEN 15749:2009
EUROPEAN STANDARD
FINAL DRAFT
FprEN 15749
NORME EUROPÉENNE
EUROPÄISCHE NORM
March 2009
ICS 65.080 Will supersede CEN/TS 15749:2008
English Version
Fertilizers - Determination of sulfates content using three
different methods
Engrais - Dosage des sulfates selon trois méthodes Düngemittel - Bestimmung von Sulfat mit drei
différentes verschiedenen Verfahren
This draft European Standard is submitted to CEN members for unique acceptance procedure. It has been drawn up by the Technical
Committee CEN/TC 260.
If this draft becomes a European Standard, CEN members are bound to comply with the CEN/CENELEC Internal Regulations which
stipulate the conditions for giving this European Standard the status of a national standard without any alteration.
This draft European Standard was established by CEN in three official versions (English, French, German). A version in any other language
made by translation under the responsibility of a CEN member into its own language and notified to the CEN Management Centre has the
same status as the official versions.
CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Cyprus, Czech Republic, Denmark, Estonia, Finland,
France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal,
Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland and United Kingdom.
Warning : This document is not a European Standard. It is distributed for review and comments. It is subject to change without notice and
shall not be referred to as a European Standard.
EUROPEAN COMMITTEE FOR STANDARDIZATION
COMITÉ EUROPÉEN DE NORMALISATION
EUROPÄISCHES KOMITEE FÜR NORMUNG
Management Centre: Avenue Marnix 17, B-1000 Brussels
© 2009 CEN All rights of exploitation in any form and by any means reserved Ref. No. FprEN 15749:2009: E
worldwide for CEN national Members.

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kSIST FprEN 15749:2009
FprEN 15749:2009 (E)
Contents Page
Foreword .3
1 Scope .4
2 Normative references .4
3 Terms and definitions .4
4 Principle .4
5 Sampling and sample preparation .5
6 Method A – Gravimetric method .5
7 Method B – ICP-OES method .6
8 Method C – IC method . 10
9 Precision of methods A, B and C . 16
10 Test report . 18
Annex A (informative) Statistical results of the inter-laboratory tests . 19
Bibliography . 22

2

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kSIST FprEN 15749:2009
FprEN 15749:2009 (E)
Foreword
This document (FprEN 15749:2009) has been prepared by Technical Committee CEN/TC 260 “Fertilizers and
liming materials”, the secretariat of which is held by DIN.
This document is currently
...

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