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CEN

EN 14333-3:2004

(Main)

Non fatty foods - Determination of benzimidazole fungicides carbendazim, thiabendazole and benomyl (as carbendazim) - Part 3: HPLC method with liquid/liquid-partition clean up

Non fatty foods - Determination of benzimidazole fungicides carbendazim, thiabendazole and benomyl (as carbendazim) - Part 3: HPLC method with liquid/liquid-partition clean up

This draft European Standard specifies a high performance liquid chromatographic (HPLC) method for the determination of the benzimidazole fungicides carbendazim and thiabendazole in fruits, vegetables and processed products.
When benomyl is present, it is completely degraded to carbendazim and is also determined as carbendazim. Thiophanate-methyl is not determined with the method.
The method has been validated for carbendazim and thiabendazole in an interlaboratory test with homogenates of apples, French beans, mushrooms, lemons and fruit based infant food.

Fettarme Lebensmittel - Bestimmung der Benzimidazol-Fungizide Carbendazim, Thiabendazol und Benomyl (als Carbendazim) - Teil 3: HPLC-Verfahren mit Reinigung durch Flüssig/Flüssig-Verteilung

Diese Europäische Norm legt ein hochleistungs-flüssigchromatographisches Verfahren zur Bestimmung der Benzimidazol-Fungizide Carbendazim und Thiabendazol in Obst, Gemüse und deren Verarbeitungsprodukten fest.
Wenn Benomyl anwesend ist, wird es vollständig zu Carbendazim abgebaut und ebenfalls als Carbendazim bestimmt. Thiophanat-methyl wird mit dem Verfahren nicht bestimmt.
Das Verfahren ist für Carbendazim und Thiabendazol durch einen Ringversuch mit Homogenaten von Äpfeln, grünen Bohnen, Pilzen, Zitronen und Kindernahrung aus Fruchtzutaten validiert worden.

Aliments non gras - Détermination des benzimidazoles antifongiques : le carbendazime, le thiabendazole et le bénomyl en tant que carbendazime - Partie 3: Méthode CLHP avec purification par séparation liquide/liquide

Le présent projet de Norme européenne décrit une méthode de chromatographie en phase liquide à haute performance (CLHP) pour la détermination du carbendazime et du thiabendazole, benzimidazoles antifongiques, dans les fruits, les légumes et les produits transformés.
Si du bénomyl est présent, celui-ci est complètement dégradé en carbendazime et dosé en tant que du carbendazime. Le thiophanate-méthyle n'est pas dosé par cette méthode.
La présente méthode a été validée pour le carbendazime et le thiabendazole lors d'un essai interlaboratoires réalisé à l'aide de broyats de pommes, de haricots verts, de champignons et d'aliments pour bébé à base de citrons et de fruits.

Nemastna živila - Določevanje benzimidazolnih fungicidov: karbendazim, tiabendazol in benomil (kot karbendazim) - 3. del: Metoda HPLC s čiščenjem s porazdelitvijo tekoče-tekoče

General Information

Status
Withdrawn
Publication Date
05-Oct-2004
Withdrawal Date
31-Dec-2014
ICS
67.080.01 - Fruits, vegetables and derived products in general
Technical Committee
CEN/TC 275 - Food analysis - Horizontal methods
Drafting Committee
CEN/TC 275/WG 4 - Pesticides in foods of plant origin
Current Stage
9960 - Withdrawal effective - Withdrawal
Start Date
01-Jan-2015
Completion Date
01-Jan-2015
Ref Project
SIST EN 14333-3:2005 - Non fatty foods - Determination of benzimidazole fungicides carbendazim, thiabendazole and benomyl (as carbendazim) - Part 3: HPLC method with liquid/liquid-partition clean up

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2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.D]LPFettarme Lebensmittel - Bestimmung der Benzimidazol-Fungizide Carbendazim, Thiabendazol und Benomyl (als Carbendazim) - Teil 3: HPLC-Verfahren mit Reinigung durch Flüssig/Flüssig-VerteilungAliments non gras - Détermination des benzimidazoles antifongiques : le carbendazime, le thiabendazole et le bénomyl en tant que carbendazime - Partie 3: Méthode CLHP avec purification par séparation liquide/liquideNon fatty foods - Determination of benzimidazole fungicides carbendazim, thiabendazole and benomyl (as carbendazim) - Part 3: HPLC method with liquid/liquid-partition clean up67.050Splošne preskusne in analizne metode za živilske proizvodeGeneral methods of tests and analysis for food productsICS:Ta slovenski standard je istoveten z:EN 14333-3:2004SIST EN 14333-3:2005en01-januar-2005SIST EN 14333-3:2005SLOVENSKI
STANDARD



SIST EN 14333-3:2005



EUROPEAN STANDARDNORME EUROPÉENNEEUROPÄISCHE NORMEN 14333-3October 2004ICS 67.080.01 English versionNon fatty foods - Determination of benzimidazole fungicidescarbendazim, thiabendazole and benomyl (as carbendazim) -Part 3: HPLC method with liquid/liquid-partition clean upAliments non gras - Détermination des benzimidazolesantifongiques : le carbendazime, le thiabendazole et lebénomyl en tant que carbendazime - Partie 3: MéthodeCLHP avec purification par séparation liquide/liquideFettarme Lebensmittel - Bestimmung der Benzimidazol-Fungizide Carbendazim, Thiabendazol und Benomyl (alsCarbendazim) - Teil 3: HPLC-Verfahren mit Reinigungdurch Flüssig/Flüssig-VerteilungThis European Standard was approved by CEN on 29 July 2004.CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this EuropeanStandard the status of a national standard without any alteration. Up-to-date lists and bibliographical references concerning such nationalstandards may be obtained on application to the Central Secretariat or to any CEN member.This European Standard exists in three official versions (English, French, German). A version in any other language made by translationunder the responsibility of a CEN member into its own language and notified to the Central Secretariat has the same status as the officialversions.CEN members are the national standards bodies of Austria, Belgium, Cyprus, Czech Republic, Denmark, Estonia, Finland, France,Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Slovakia,Slovenia, Spain, Sweden, Switzerland and United Kingdom.EUROPEAN COMMITTEE FOR STANDARDIZATIONCOMITÉ EUROPÉEN DE NORMALISATIONEUROPÄISCHES KOMITEE FÜR NORMUNGManagement Centre: rue de Stassart, 36
B-1050 Brussels© 2004 CENAll rights of exploitation in any form and by any means reservedworldwide for CEN national Members.Ref. No. EN 14333-3:2004: ESIST EN 14333-3:2005



EN 14333-3:2004 (E) 2 Contents Page Foreword.3 1 Scope.4 2 Principle.4 3 Reagents.4 4 Apparatus.5 5 Procedure.6 6 Calculation.7 7 Confirmatory tests.7 8 Precision.7 9 Test report.8 Annex A (informative)
Precision data.9 Annex B (informative)
Alternative HPLC operating conditions.12 Bibliography.
...

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