EN 13075-1:2002

Bitumen and bituminous binders - Determination of breaking behaviour - Part 1: Determination of breaking value of cationic bitumen emulsions, mineral filler method

This European Standard specifies a method for the determination of the breaking value of cationic bitumen emulsions.
WARNING - The use of this standard may involve hazardous materials, operations and equipment. This standard does not purport to address all of the safety problems associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

Bitumen und bitumenhaltige Bindemittel - Bestimmung des Brechverhaltens - Teil 1: Bestimmung des Brechwertes kationischer Bitumenemulsionen, Verfahren mit Feinmineralstoff

Diese Norm legt ein Verfahren zur Bestimmung des Brechwertes kationischer Emulsionen fest. Warnung: Die Anwendung dieser Norm kann gefährliche Substanzen, Arbeitsgänge und Ausrüstung einschließen. In der Norm werden nicht alle Sicherheitsprobleme angesprochen, die mit ihrer Anwendung verbunden sind. Es liegt in der Verantwortung des Anwenders dieser Norm, geeignete Sicherheits- und Gesundheitsschutzmaßnahmen vorzusehen und vorher zu klären, ob einschränkende Vorschriften zu berücksichtigen sind.

Bitumes et liants bitumineux - Détermination du comportement à la rupture - Partie 1: Détermination de l'indice de rupture des émulsions cationiques de bitume, méthode des fines minérales

La présente norme européenne prescrit une méthode de détermination du comportement à la rupture des émulsions cationiques  AVERTISSEMENT : L'utilisation de la présente norme européenne implique l'intervention de produits, d'opérations et d'équipements à caractère dangereux. La présente norme européenne n'a pas la prétention d'aborder tous les problèmes de sécurité concernés par son usage. Il est de la responsabilité de l'utilisateur de consulter et d'établir des règles de sécurité et d'hygiène appropriées et de déterminer l'applicabilité des restrictions réglementaires avant l'utilisation.

Bitumen in bitumenska veziva - Določevanje stopnje stabilnosti - 1. del: Določevanje hitrosti razpada kationskih bitumenskih emulzij, metoda z mineralnim polnilom

General Information

• Status: Withdrawn
• Publication Date: 09-Jul-2002
• Withdrawal Date: 17-Mar-2009
• ICS: 75.140 - Waxes, bituminous materials and other petroleum products
• ICS: 91.100.50 - Binders. Sealing materials
• Technical Committee: CEN/TC 336 - Bituminous binders
• Drafting Committee: CEN/TC 336/WG 2 - Emulsions and fluxed bitumens
• Current Stage: 9960 - Withdrawal effective - Withdrawal
• Start Date: 18-Mar-2009
• Completion Date: 18-Mar-2009
• Directive: 305/2011 - Regulation (eu) No 305/2011 of the European Parliament and of the Council of 9 march 2011 laying down harmonised conditions for the marketing of construction products and repealing council directive 89/106/eec
• Directive: 89/106/EEC - Construction products
• Mandate: M/124 - Mandate to CEN/CENELEC concerning the execution of standardization work for harmonized standards on road construction products
• Ref Project: SIST EN 13075-1:2003 - Bitumen and bituminous binders - Determination of breaking behaviour - Part 1: Determination of breaking value of cationic bitumen emulsions, mineral filler method

Relations

• Replaced By: EN 13075-1:2009 - Bitumen and bituminous binders - Determination of breaking behaviour - Part 1: Determination of breaking value of cationic bituminous emulsions, mineral filler method
• Effective Date: 23-Mar-2009

Standards Content (Sample)

SLOVENSKI STANDARD
SIST EN 13075-1:2003
01-januar-2003
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'RORþHYDQMHKLWURVWLUD]SDGDNDWLRQVNLKELWXPHQVNLKHPXO]LMPHWRGD]PLQHUDOQLP
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Bitumen and bituminous binders - Determination of breaking behaviour - Part 1:
Determination of breaking value of cationic bitumen emulsions, mineral filler method
Bitumen und bitumenhaltige Bindemittel - Bestimmung des Brechverhaltens - Teil 1:
Bestimmung des Brechwertes kationischer Bitumenemulsionen, Verfahren mit
Feinmineralstoff
Bitumes et liants bitumineux - Détermination du comportement a la rupture - Partie 1:
Détermination de l'indice de rupture des émulsions cationiques de bitume, méthode des
fines minérales
Ta slovenski standard je istoveten z: EN 13075-1:2002
ICS:
75.140 Voski, bitumni in drugi naftni Waxes, bituminous materials
proizvodi and other petroleum products
91.100.50 Veziva. Tesnilni materiali Binders. Sealing materials
SIST EN 13075-1:2003 en
2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.

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EUROPEAN STANDARD
EN 13075-1
NORME EUROPÉENNE
EUROPÄISCHE NORM
July 2002
ICS 75.140; 91.100.50
English version
Bitumen and bituminous binders - Determination of breaking
behaviour - Part 1: Determination of breaking value of cationic
bitumen emulsions, mineral filler method
Bitumes et liants bitumineux - Détermination du Bitumen und bitumenhaltige Bindemittel - Bestimmung des
comportement à la rupture - Partie 1: Détermination de Brechverhaltens - Teil 1: Bestimmung des Brechwertes
l'indice de rupture des émulsions cationiques de bitume, kationischer Bitumenemulsionen, Verfahren mit
méthode des fines minérales Feinmineralstoff
This European Standard was approved by CEN on 14 March 2002.
CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this European
Standard the status of a national standard without any alteration. Up-to-date lists and bibliographical references concerning such national
standards may be obtained on application to the Management Centre or to any CEN member.
This European Standard exists in three official versions (English, French, German). A version in any other language made by translation
under the responsibility of a CEN member into its own language and notified to the Management Centre has the same status as the official
versions.
CEN members are the national standards bodies of Austria, Belgium, Czech Republic, Denmark, Finland, France, Germany, Greece,
Iceland, Ireland, Italy, Luxembourg, Malta, Netherlands, Norway, Portugal, Spain, Sweden, Switzerland and United Kingdom.
EUROPEAN COMMITTEE FOR STANDARDIZATION
COMITÉ EUROPÉEN DE NORMALISATION
EUROPÄISCHES KOMITEE FÜR NORMUNG
Management Centre: rue de Stassart, 36  B-1050 Brussels
© 2002 CEN All rights of exploitation in any form and by any means reserved Ref. No. EN 13075-1:2002 E
worldwide for CEN national Members.

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EN 13075-1:2002 (E)
Foreword
This document EN 13075-1:2002 has been prepared by Technical Committee CEN/TC 336 "Bituminous binders",
the secretariat of which is held by AFNOR.
This European Standard shall be given the status of a national standard, either by publication of an identical text or
by endorsement, at the latest by January 2003, and conflicting national standards shall be withdrawn at the latest
by January 2003.
This European Standard is part of a package including 14 standards: EN 1428, EN 1429, EN 1430, EN 1431,
EN 12846, EN 12847, EN 12848, EN 12849, EN 12850, EN 13074, EN 13075-1, EN 13075-2, EN 13614 and
EN 13808.
Annex A is normative and annex B is informative.
This European Standard EN 13075 consists of the following parts under the general title Bitumen and bituminous
binders – Determination of breaking behaviour:
Part 1 – Determination of breaking value of cationic bitumen emulsions, mineral filler method;
Part 2 – Determination of fines mixing time of cationic bitumen emulsions.
According to the CEN/CENELEC Internal Regulations, the national standards organizations of the following
countries are bound to implement this European Standard: Austria, Belgium, Czech Republic, Denmark, Finland,
France, Germany, Greece, Iceland, Ireland, Italy, Luxembourg, Malta, Netherlands, Norway, Portugal, Spain,
Sweden, Switzerland and the United Kingdom.
2

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EN 13075-1:2002 (E)
1 Scope
This European Standard specifies a method for the determination of the breaking value of cationic bitumen
emulsions.
WARNING – The use of this standard may involve hazardous materials, operations and equipment. This
standard does not purport to address all of the safety problems associated with its use. It is the
responsibility of the user of this standard to establish appropriate safety and health practices and
determine the applicability of regulatory limitations prior to use.
2 Normative references
This European Standard incorporates by dated or undated reference, provisions from other publications. These
normative references are cited at the appropriate places in the text, and the publications are listed hereafter. For
dated references, subsequent amendments to or revisions of any of these publications apply to this European
Standard only when incorporated in it by amendment or revision. For undated references the latest edition of the
publication referred to applies (including amendments).
1)
EN 58 , Bitumen and bituminous binders - Sampling bituminous binders.
EN 12594, Bitumen and bituminous binders – Preparation of test samples.
3 Terms and definitions
For the purposes of this European Standard, the following term and definition apply.
3.1
breaking value
dimensionless number corresponding to the amount of reference filler, in grams, needed to coagulate 100 g of
bitumen emulsion
4 Principle
A reference filler is added at a uniform rate to a specified quantity of stirred cationic bitumen emulsion. When the
emulsion has broken completely, the amount of added filler is determined by weighing. The mass of filler (in grams)
multiplied by 100 and divided by the amount of emulsion (in grams) is the breaking value.
NOTE The cationic or anionic nature of an emulsion can be determined with EN 1430 [1].
5 Reagents and materials
2)
5.1 Filler, Forshammer SE filler , reference is given in annex A.
The filler shall be dried before use.
NOTE For information, the round robin test showed good correlation with Sikaisol filler (described in annex B).

1) In course of revision.
2) This information is given for the convenience of users of this European Standard and does not constitute an endorsement
by CEN of the product name. Equivalent products may be used if they can be shown to lead to the same results, or if a
correlation between the products has been established.
3

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EN 13075-1:2002 (E)
In case of dispute, the Forshammer SE filler shall be used.
5.2 Cleaning agents, as used conventionally in laboratories.
6 Apparatus
Usual laboratory apparatus and glassware, together with the following:
6.1 Equipment for semi-automatic procedure, as shown in Figure 1, consisting of the following:
6.1.1 Stirrer motor, with an output power of at least 25 W, and a speed of 260 r/min – 60 r/min.
6.1.2 Stirrer, having the dimensions given in Figures 3, 4 and 5. In Figure 3, the dimensions are given as an
example.
6.1.3 Adjustable filler feeder, capable of feeding the filler at a rate of 0,3 g/s - 0,4 g/s. This equipment shall be
calibrated. The calibration shall be achieved by weighing the amount of the filler poured during a period of time
between 100 s and 200 s measured with an accuracy of 0,2 s.
NOTE For the manual procedure, the feeding rate, , in grams per second, should be calculated, using the following
q
equation:
m
f
q =
t
where
m is the mass of filler in grams;
f
is the analysis time in seconds.
t
6.1.4 Metal cans, cylindrical, of approximate capacity 500 ml, height 95 mm and diameter
...