prEN 18032

Foodstuff - Quick Method for the Analysis of Multiple Highly Polar Pesticides and their Metabolites in Foodstuff Involving Extraction with Acidified Methanol and Measurement by LC- or IC-MS/MS (QuPPe-Method)

This document specifies a procedure for the analysis of residues of highly polar pesticides and metabolites, which are not amenable to common multiresidue methods, in various food commodities of plant and animal origin, including fruits, vegetables, cereals, pulses, oily seeds, nuts, milk, liver and honey. The method was developed at the EURL-SRM hosted at CVUA Stuttgart and has been collaboratively studied on a large number of commodity/pesticide combinations. Guidelines for calibration are outlined in CEN/TS 17061:2019.

Lebensmittel - Schnellmethode zur Bestimmung mehrerer hochpolarer Pestizide und ihrer Metaboliten in Lebensmitteln nach Extraktion mit angesäuertem Methanol und Messung mittels LC- oder IC-MS/MS (QuPPe-Methode)

Dieses Dokument legt ein Verfahren zur Bestimmung von Rückständen hochpolarer Pestizide und ihrer Meta boliten in verschiedenen Arten von Lebensmitteln pflanzlichen und tierischen Ursprungs, einschließlich Obst, Gemüse, Getreide, Hülsenfrüchte, Ölsaaten, Nüsse, Milch, Leber und Honig, fest, die mit üblichen Multiverfahren nicht untersucht werden können. Das Verfahren wurde in dem beim CVUA Stuttgart ansässigen EURL-SRM wickelt[1],[2],[3] und ist in Ringversuchen an einer großen Zahl von Lebensmittel-Pestizid-Kombinationen näher untersucht worden. Leitlinien für die Kalibrierung sind in CEN/TS17061:2019 dargelegt.

Produits alimentaires - Méthode rapide pour l'analyse de plusieurs pesticides hautement polaires et de leurs métabolites dans les aliments impliquant une extraction avec du méthanol acidifié et une analyse par LC- ou CI-SM/SM (méthode QuPPe)

Le présent document spécifie un mode opératoire pour l'analyse des résidus de pesticides et de métabolites hautement polaires, qui ne se prêtent pas aux méthodes multirésidus courantes, dans de nombreux produits alimentaires d'origine végétale et animale, notamment les fruits, les légumes, les céréales, les légumineuses, les graines oléagineuses, les noix, le lait, le foie et le miel. La méthode a été élaborée par le laboratoire de référence de l'Union Européen selon des méthodes monorésidus (EURL SRM) au CVUA de Stuttgart [1], [2], [3] et a fait l'objet d'une étude collaborative sur un grand nombre de combinaisons de produits/pesticides. Les lignes directrices concernant l'étalonnage sont décrites dans la CEN/TS 17061:2019.

Živila - Hitra metoda za analizo več visokopolarnih pesticidov in njihovih metabolitov v živilih z ekstrakcijo s kislim metanolom in merjenjem z LC- ali IC-MS/MS (QuPPe-Metoda)

General Information

• Status: Not Published
• Publication Date: 25-Aug-2025
• ICS: 67.050 - General methods of tests and analysis for food products
• Technical Committee: CEN/TC 275 - Food analysis - Horizontal methods
• Drafting Committee: CEN/TC 275/WG 3 - Pesticides and PCB's in foods of animal origin
• Current Stage: 4060 - Closure of enquiry - Enquiry
• Start Date: 14-Mar-2024
• Due Date: 02-Jul-2024
• Completion Date: 14-Mar-2024
• Ref Project: oSIST prEN 18032:2024 - Foodstuff - Quick Method for the Analysis of Multiple Highly Polar Pesticides and their Metabolites in Foodstuff Involving Extraction with Acidified Methanol and Measurement by LC- or IC-MS/MS (QuPPe-Method)

Standards Content (Sample)

SLOVENSKI STANDARD
oSIST prEN 18032:2024
01-marec-2024
Živila - Hitra metoda za analizo več visokopolarnih pesticidov in njihovih
metabolitov v živilih z ekstrakcijo s kislim metanolom in merjenjem z LC- ali IC-
MS/MS (QuPPe-Metoda)
Foodstuff - Quick Method for the Analysis of Multiple Highly Polar Pesticides and their
Metabolites in Foodstuff Involving Extraction with Acidified Methanol and Measurement
by LC- or IC-MS/MS (QuPPe-Method)
Lebensmittel - Schnellmethode zur Bestimmung mehrerer hochpolarer Pestizide und
ihrer Metaboliten in Lebensmitteln nach Extraktion mit angesäuertem Methanol und
Messung mittels LC- oder IC-MS/MS (QuPPe-Methode)
Produit alimentaire - Méthode rapide pour l'analyse de plusieurs pesticides hautement
polaires et de leurs métabolites dans les aliments impliquant une extraction avec du
méthanol acidifié et une mesure par LC- ou IC-MS/MS (QuPPe-Methode)
Ta slovenski standard je istoveten z: prEN 18032
ICS:
67.050 Splošne preskusne in General methods of tests and
analizne metode za živilske analysis for food products
proizvode
oSIST prEN 18032:2024 en,fr,de
2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.

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oSIST prEN 18032:2024


DRAFT
EUROPEAN STANDARD
prEN 18032
NORME EUROPÉENNE

EUROPÄISCHE NORM

November 2023
ICS
English Version

Foodstuff - Quick Method for the Analysis of Multiple
Highly Polar Pesticides and their Metabolites in Foodstuff
Involving Extraction with Acidified Methanol and
Measurement by LC- or IC-MS/MS (QuPPe-Method)
Lebensmittel ¿ Schnellmethode zur Bestimmung Produit alimentaire - Méthode rapide pour l'analyse de
mehrerer hochpolarer Pestizide und ihrer Metaboliten plusieurs pesticides hautement polaires et de leurs
in Lebensmitteln nach Extraktion mit angesäuertem métabolites dans les aliments impliquant une
Methanol und Messung mittels LC- oder IC-MS/MS extraction avec du méthanol acidifié et une mesure par
(QuPPe-Methode) LC- ou IC-MS/MS (QuPPe-Methode)
This draft European Standard is submitted to CEN members for enquiry. It has been drawn up by the Technical Committee
CEN/TC 275.

If this draft becomes a European Standard, CEN members are bound to comply with the CEN/CENELEC Internal Regulations
which stipulate the conditions for giving this European Standard the status of a national standard without any alteration.

This draft European Standard was established by CEN in three official versions (English, French, German). A version in any other
language made by translation under the responsibility of a CEN member into its own language and notified to the CEN-CENELEC
Management Centre has the same status as the official versions.

CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia,
Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway,
Poland, Portugal, Republic of North Macedonia, Romania, Serbia, Slovakia, Slovenia, Spain, Sweden, Switzerland, Türkiye and
United Kingdom.

Recipients of this draft are invited to submit, with their comments, notification of any relevant patent rights of which they are
aware and to provide supporting documentation.

Warning : This document is not a European Standard. It is distributed for review and comments. It is subject to change without
notice and shall not be referred to as a European Standard.


EUROPEAN COMMITTEE FOR STANDARDIZATION
COMITÉ EUROPÉEN DE NORMALISATION

EUROPÄISCHES KOMITEE FÜR NORMUNG

CEN-CENELEC Management Centre: Rue de la Science 23, B-1040 Brussels
© 2023 CEN All rights of exploitation in any form and by any means reserved Ref. No. prEN 18032:2023 E
worldwide for CEN national Members.

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oSIST prEN 18032:2024
prEN 18302:2023 (E)
Contents Page
European foreword . 3
1 Scope . 4
2 Normative references . 4
3 Terms and Definitions . 4
4 Principle . 4
5 Preparation and storage of the samples .
...