Fertilizers - Determination of magnesium by complexometry

This Technical Specification specifies a method for the determination of magnesium in fertilizer extracts.
The method is applicable to the following EC fertilizer extracts for which the determination of total magnesium and/or water-soluble magnesium is provided for according to the Regulation (EC) No 2003/2003, Annex I [3]:
-   fertilizers listed in [3], Annex I: straight nitrogenous fertilizers, type 1b + 1c (calcium magnesium nitrate), type 7 (magnesium sulfonitrate), type 8 (nitrogenous fertilizers with magnesium) and straight potassic fertilizers, type 2 (enriched kainite), type 4 (potassium chloride containing magnesium), type 6 (potassium sulfate containing magnesium salt);
-   fertilizers listed in [3], Annex I D relating to secondary nutrients.

Düngemittel - Komplexometrische Bestimmung von Magnesium

Diese Technische Spezifikation legt ein Verfahren zur Bestimmung von Magnesium in Düngemittelextrakten fest. Das Verfahren gilt für die folgenden EG-Düngemittelextrakte, für die die Angabe des Gesamtmagnesiums und/oder des wasserlöslichen Magnesiums entsprechend der Verordnung (EG) Nr. 2003/2003, Anhang I, [3], vorgeschrieben ist:
- in [3], Anhang I, aufgeführte Düngemittel: Einnährstoff-Stickstoffdünger vom Typ 1b + 1c (Calcium-Magnesiumnitrat), Typ 7 (Stickstoff-Magnesiumsulfat), Typ 8 (Stickstoffdünger mit Magnesium) und Einnährstoff-Kalidünger vom Typ 2 (angereichertes Kainit), Typ 4 (Kaliumchlorid mit Magnesium), Typ 6 (Kaliumsulfat mit Magnesium);
- in [3], Anhang I D, aufgeführte Düngemittel mit Bezug auf Sekundärnährstoffe.

Engrais - Dosage du magnésium par complexométrie

La présente Spécification technique spécifie une méthode de dosage du magnésium dans les extraits
d’échantillons d’engrais.
Cette méthode est applicable aux extraits d’échantillons d’engrais CE pour lesquels le dosage du magnésium
total et/ou soluble eau est prévu, conformément au Règlement (CE) n° 2003/2003, Annexe I de la référen ce
bibliographique [3] :
- engrais répertoriés dans l’Annexe I de la référence bibliographique [3] ; engrais azotés simples, type
1b + 1c (nitrate de calcium et de magnésium), type 7 (sulfonitrate de magnésium), type 8 (engrais azotés
contenant du magnésium) et engrais potassiques simples, type 2 (kaïnite enrichie), type 4 (chlorure de
potassium contenant du magnésium), type 6 (sulfate de potassium contenant du sel de magnésium) ;
- engrais répertoriés dans l’Annexe I D de la référence bibliographique [3] relative aux éléments nutritifs
secondaires.

Gnojila - Kompleksometrijsko določevanje magnezija

Ta tehnična specifikacija opredeljuje metodo določevanja magnezija v ekstraktih gnojil. Metoda se uporablja za naslednje ekstrakte gnojil ES, za katere je zagotovljeno določevanje celotne vsebnosti magnezija in/ali vsebnosti v vodi topnega magnezija, v skladu z Uredbo (ES) št. 2003/2003, Priloga I: gnojila, navedena v dodatku I: enostavna dušikova gnojila, tip 1b + 1c (kalcijev magnezijev nitrat), tip 7 (magnezijev sulfonitrat), tip 8 (dušikova gnojila z magnezijem) in enostavna kalijeva gnojila, tip 2 (obogateni kainit), tip 4 (kalijev klorid, ki vsebuje magnezij), tip 6 (kalijev sulfat, ki vsebuje magnezijevo sol); gnojila, navedena v dodatku I D, ki se nanaša na sekundarna hranila.

General Information

Status
Withdrawn
Publication Date
31-May-2011
Withdrawal Date
13-Nov-2012
Current Stage
9960 - Withdrawal effective - Withdrawal
Start Date
14-Nov-2012
Completion Date
14-Nov-2012

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Standards Content (Sample)

SLOVENSKI STANDARD
SIST-TS CEN/TS 16198:2011
01-oktober-2011
*QRMLOD.RPSOHNVRPHWULMVNRGRORþHYDQMHPDJQH]LMD
Fertilizers - Determination of magnesium by complexometry
Düngemittel - Komplexometrische Bestimmung von Magnesium
Engrais - Dosage du magnésium par complexométrie
Ta slovenski standard je istoveten z: CEN/TS 16198:2011
ICS:
65.080 Gnojila Fertilizers
SIST-TS CEN/TS 16198:2011 en,fr,de
2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.

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SIST-TS CEN/TS 16198:2011

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SIST-TS CEN/TS 16198:2011


TECHNICAL SPECIFICATION
CEN/TS 16198

SPÉCIFICATION TECHNIQUE

TECHNISCHE SPEZIFIKATION
June 2011
ICS 65.080
English Version
Fertilizers - Determination of magnesium by complexometry
Engrais - Dosage du magnésium par complexométrie Düngemittel - Komplexometrische Bestimmung von
Magnesium
This Technical Specification (CEN/TS) was approved by CEN on 5 March 2011 for provisional application.

The period of validity of this CEN/TS is limited initially to three years. After two years the members of CEN will be requested to submit their
comments, particularly on the question whether the CEN/TS can be converted into a European Standard.

CEN members are required to announce the existence of this CEN/TS in the same way as for an EN and to make the CEN/TS available
promptly at national level in an appropriate form. It is permissible to keep conflicting national standards in force (in parallel to the CEN/TS)
until the final decision about the possible conversion of the CEN/TS into an EN is reached.

CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia,
Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland,
Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland and United Kingdom.





EUROPEAN COMMITTEE FOR STANDARDIZATION
COMITÉ EUROPÉEN DE NORMALISATION

EUROPÄISCHES KOMITEE FÜR NORMUNG

Management Centre: Avenue Marnix 17, B-1000 Brussels
© 2011 CEN All rights of exploitation in any form and by any means reserved Ref. No. CEN/TS 16198:2011: E
worldwide for CEN national Members.

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SIST-TS CEN/TS 16198:2011
CEN/TS 16198:2011 (E)
Contents Page
Foreword .3
1 Scope .4
2 Normative references .4
3 Terms and definitions .4
4 Principle .4
5 Sampling .4
6 Reagents .5
7 Apparatus .6
8 Preparation of the extraction solution .6
9 Procedure .6
9.1 Control test .6
9.2 Aliquot samples to be taken .7
9.3 Titration in the presence of Eriochrome black-T .7
9.4 Titration in the presence of calcein or of calcon carbonic acid .7
10 Calculation and expression of the result .7
11 Remarks .7
12 Precision .
...

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