EN ISO 5269-2:2004
(Main)Pulps - Preparation of laboratory sheets for physical testing - Part 2: Rapid-Köthen method (ISO 5269-2:2004)
Pulps - Preparation of laboratory sheets for physical testing - Part 2: Rapid-Köthen method (ISO 5269-2:2004)
ISO 5269-2:2004 specifies a method, using a Rapid-Köthen sheet former, for the preparation of laboratory sheets of pulp for the purpose of carrying out subsequent physical tests on these sheets in order to assess the relevant properties of the pulp itself.
ISO 5269-2:2004 is applicable to most kinds of pulp. It is not suitable for some pulps with very long fibres, such as those made from unshortened cotton, flax and similar materials.
This method is not suitable for the preparation of laboratory sheets for the determination of diffuse blue reflectance factor (ISO brightness) in accordance with ISO 3688.
Faserstoffe - Laborblattbildung für physikalische Prüfungen - Teil 2: Rapid-Köthen-Verfahren (ISO 5269-2:2004)
Dieser Teil der ISO 5269 legt ein Verfahren für die Blattbildung zur Herstellung von Laborblättern auf einer
Rapid-Köthen-Blattbildungseinrichtung fest. Die so hergestellten Laborblätter können anschließend
physikalischen Prüfungen unterzogen werden, um die relevanten Eigenschaften des Faserstoffes zu
bestimmen.
Dieser Teil der ISO 5269 ist auf die Mehrzahl aller Faserstoffe anwendbar, eignet sich jedoch nicht für
besonders langfaserige Faserstoffe, wie sie beispielsweise aus ungekürzter Baumwolle, Flachs und ähnlichen
Rohstoffen hergestellt werden.
Ferner ist dieses Verfahren nicht für die Herstellung von Laborblättern zur Bestimmung des diffusen blauen
Reflexionsfaktors (ISO-Weißgrad) nach ISO 3688 [1] geeignet.
WARNUNG - Wenn langfaseriger Zellstoff in ungekürzter Form verwendet wird, ist die Blattformation
nicht immer zufrieden stellend.
Pâtes - Préparation des feuilles de laboratoire pour essais physiques - Partie 2: Méthode Rapid-Köthen (ISO 5269-2:2004)
Vlaknine - Izdelava laboratorijskih listov za preskušanje fizikalnih lastnost - 2. del: Metoda na Rapid-Köthenovem aparatu (ISO 5269-2:2004)
General Information
Relations
Standards Content (Sample)
SLOVENSKI STANDARD
01-maj-2005
1DGRPHãþD
SIST EN ISO 5269-2:2000
SIST EN ISO 5269-2:2000
Vlaknine - Izdelava laboratorijskih listov za preskušanje fizikalnih lastnost - 2. del:
Metoda na Rapid-Köthenovem aparatu (ISO 5269-2:2004)
Pulps - Preparation of laboratory sheets for physical testing - Part 2: Rapid-Köthen
method (ISO 5269-2:2004)
Faserstoffe - Laborblattbildung für physikalische Prüfungen - Teil 2:
Rapid-Köthen-Verfahren (ISO 5269-2:2004)
Pâtes - Préparation des feuilles de laboratoire pour essais physiques - Partie 2: Méthode
Rapid-Köthen (ISO 5269-2:2004)
Ta slovenski standard je istoveten z: EN ISO 5269-2:2004
ICS:
85.040 Vlaknine Pulps
2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.
EUROPEAN STANDARD
EN ISO 5269-2
NORME EUROPÉENNE
EUROPÄISCHE NORM
December 2004
ICS 85.040 Supersedes EN ISO 5269-2:2000
English version
Pulps - Preparation of laboratory sheets for physical testing -
Part 2: Rapid-Köthen method (ISO 5269-2:2004)
Pâtes - Préparation des feuilles de laboratoire pour essais
physiques - Partie 2: Méthode Rapid-Köthen (ISO 5269-
2:2004)
This European Standard was approved by CEN on 6 December 2004.
CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this European
Standard the status of a national standard without any alteration. Up-to-date lists and bibliographical references concerning such national
standards may be obtained on application to the Central Secretariat or to any CEN member.
This European Standard exists in three official versions (English, French, German). A version in any other language made by translation
under the responsibility of a CEN member into its own language and notified to the Central Secretariat has the same status as the official
versions.
CEN members are the national standards bodies of Austria, Belgium, Cyprus, Czech Republic, Denmark, Estonia, Finland, France,
Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Slovakia,
Slovenia, Spain, Sweden, Switzerland and United Kingdom.
EUROPEAN COMMITTEE FOR STANDARDIZATION
COMITÉ EUROPÉEN DE NORMALISATION
EUROPÄISCHES KOMITEE FÜR NORMUNG
Management Centre: rue de Stassart, 36 B-1050 Brussels
© 2004 CEN All rights of exploitation in any form and by any means reserved Ref. No. EN ISO 5269-2:2004: E
worldwide for CEN national Members.
Foreword
The text of ISO 5269-2:2004 has been prepared by Technical Committee ISO/TC 6 "Paper,
board and pulps” of the International Organization for Standardization (ISO) and has been taken
over as EN ISO 5269-2:2004 by Technical Committee CEN/TC 172 "Pulp, paper and board", the
secretariat of which is held by DIN.
This European Standard shall be given the status of a national standard, either by publication of
an identical text or by endorsement, at the latest by June 2005, and conflicting national
standards shall be withdrawn at the latest by June 2005.
This document supersedes EN ISO 5269-2:2000.
According to the CEN/CENELEC Internal Regulations, the national standards organizations of
the following countries are bound to implement this European Standard: Austria, Belgium,
Cyprus, Czech Republic, Denmark, Estonia, Finland, France, Germany, Greece, Hungary,
Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland,
Portugal, Slovakia, Slovenia, Spain, Sweden, Switzerland and United Kingdom.
Endorsement notice
The text of ISO 5269-2:2004 has been approved by CEN as EN ISO 5269-2:2004 without any
modifications.
INTERNATIONAL ISO
STANDARD 5269-2
Third edition
2004-11-01
Pulps — Preparation of laboratory sheets
for physical testing —
Part 2:
Rapid-Köthen method
Pâtes — Préparation des feuilles de laboratoire pour essais
physiques —
Partie 2: Méthode Rapid-Köthen
Reference number
ISO 5269-2:2004(E)
©
ISO 2004
ISO 5269-2:2004(E)
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ii © ISO 2004 – All rights reserved
ISO 5269-2:2004(E)
Contents Page
Foreword. iv
Introduction . v
1 Scope. 1
2 Normative references. 1
3 Principle. 1
4 Equipment. 2
5 Pretreatment and preparation of sample. 5
5.1 Pretreatment. 5
5.2 Preparation of sample . 6
6 Procedure. 6
6.1 Sheet forming. 6
6.2 Transfer of the sheet. 6
6.3 Drying and conditioning. 7
7 Test report. 7
Bibliography . 8
ISO 5269-2:2004(E)
Foreword
ISO (the International Organization for Standardization) is a worldwide federation of national standards bodies
(ISO member bodies). The work of preparing International Standards is normally carried out through ISO
technical committees. Each member body interested in a subject for which a technical committee has been
established has the right to be represented on that committee. International organizations, governmental and
non-governmental, in liaison with ISO, also take part in the work. ISO collaborates closely with the
International Electrotechnical Commission (IEC) on all matters of electrotechnical standardization.
International Standards are drafted in accordance with the rules given in the ISO/IEC Directives, Part 2.
The main task of technical committees is to prepare International Standards. Draft International Standards
adopted by the technical committees are circulated to the member bodies for voting. Publication as an
International Standard requires approval by at least 75 % of the member bodies casting a vote.
Attention is drawn to the possibility that some of the elements of this document may be the subject of patent
rights. ISO shall not be held responsible for identifying any or all such patent rights.
ISO 5269-2 was prepared by Technical Committee ISO/TC 6, Paper, board and pulps, Subcommittee SC 5,
Test methods and quality specifications for pulps.
This third edition cancels and replaces the second edition (ISO 5269-2:1998), of which the Introduction,
Clauses 1, 2 and 7 and Subclause 5.1 have been revised.
ISO 5269 consists of the following parts, under the general title Pulps — Preparation of laboratory sheets for
physical testing:
Part 1: Conventional sheet-former method
Part 2: Rapid-Köthen method
iv © ISO 2004 – All rights reserved
ISO 5269-2:2004(E)
Introduction
It has been agreed that the ultimate aim of standardization of the preparation of laboratory sheets should be to
develop one method which is internationally acceptable and which, if possible, permits the use of different
types of sheet-making apparatus.
For practical reasons, it has not proved possible to achieve this at present. Therefore, as an interim measure,
in view of the widespread use of equipment described in this part of ISO 5269, it has been decided to provide
agreed guidance on the use of different types of equipment in order to achieve consistency of results with
each method.
To avoid creating too many levels of results, the method specified in this part of ISO 5269 should preferably
be used with the PFI mill method of laboratory beating according to ISO 5264-2. The method specified in
ISO 5269-1 (Conventional sheet-former method) should preferably be used with the Valley beater or PFI mill
[2]
methods of laboratory beating according to ISO 5264-1 and 5264-2, respectively.
INTERNATIONAL STANDARD ISO 5269-2:2004(E)
Pulps — Preparation of laboratory sheets for physical testing —
Part 2:
Rapid-Köthen method
1 Scope
This part of ISO 5269 specifies a method, using a Rapid-Köthen sheet former, for the preparation of laboratory
sheets of pulp for the purpose of carrying out subsequent physical tests on these sheets in order to assess the
relevant properties of the pulp itself.
This part of ISO 5269 is applicable to most kinds of pulp. It is not suitable for some pulps with very long fibres,
such as those made from unshortened cotton, flax and similar materials.
This method is not suitable for the preparation of laboratory sheets for the determination of diffuse blue
[1]
reflectance factor (ISO brightness) in accordance with ISO 3688 .
WARNING — When long-fibred pulp is used in the unshortened form, the sheet formation may not
always be satisfactory.
2 Normative references
The following referenced documents are indispensable for the application of this document. For dated
references, only the edition cited applies. For undated references, the latest edition of the referenced
document (including any amendments) applies.
ISO 187, Paper, board and pulps — Standard atmosphere for conditioning and testing and procedure for
monitoring the atmosphere and conditioning of samples
ISO 4119, Pulps — Determination of stock concentration
ISO 5263-1, Pulps — Laboratory wet disintegration — Part 1: Disintegration of chemical pulps
ISO 5263-2, Pulps — Laboratory wet disintegration — Part 2: Disintegration of mechanical pulps at 20 °C
ISO 5263-3, Pulps — Laboratory wet disintegration — Part 3: Disintegration of mechanical pulps at W 85 °C
ISO 5264-2, Pulps — Laboratory beating — Part 2: PFI mill method
ISO 5269-1, Pulps — Preparation of laboratory sheets for physical testing — Part 1: Conventional sheet-
former method
3 Principle
A circular sheet is formed from a pulp suspension on a wire screen under suction. The sheet is subjected to
pressure and dried in a dryer, with almost complete prevention of shrinkage, in a specified way with respect to
the pressure applied, the suction and the temperature.
ISO 5269-2:2004(E)
4 Equipment
4.1 Rapid-Köthen apparatus, consisting of a sheet former, transfer equipment, one or more dryers and
accessories (see Figure 1). The parts of the instrument which come into contact with stock or water shall be
corrosion resistant.
4.1.1 Sheet former, consisting of a stock container for preparing the pulp suspension, the screen section
on which wet fibre is forwarded, and the suction chamber for drawing off and holding the water after passing
through the screen. The lower part of the stock container, screen section and suction chamber may be sealed
off.
4.1.1.1 Stock container (see Figure 1)
The stock container consists of a transparent cylindrical tube (1) with an internal diameter of
200 mm ± 0,5 mm and a capacity of not less than 10 litres. The container is graduated in litres. Around the
circumference of the lower p
...
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