Cavity resonator method to measure the complex permittivity of low-loss dielectric plates

Describes the measurement method of dielectric properties in the planer direction of dielectric plate at microwave frequency in order to develop new materials and to design microwave active and passive devices. This method is called a cavity resonator method.

General Information

Status
Replaced
Publication Date
21-Jan-2008
Current Stage
DELPUB - Deleted Publication
Completion Date
18-Feb-2010
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IEC PAS 62562:2008 - Cavity resonator method to measure the complex permittivity of low-loss dielectric plates Released:1/22/2008 Isbn:2831895243
English language
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IEC/PAS 62562
Edition 1.0 2008-01
PUBLICLY AVAILABLE
SPECIFICATION
PRE-STANDARD
Cavity resonator method to measure the complex permittivity of low-loss
dielectric plates
IEC/PAS 62562:2008(E)
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IEC/PAS 62562
Edition 1.0 2008-01
PUBLICLY AVAILABLE
SPECIFICATION
PRE-STANDARD
Cavity resonator method to measure the complex permittivity of low-loss
dielectric plates
INTERNATIONAL
ELECTROTECHNICAL
COMMISSION
PRICE CODE
Q
ICS 17.220 ISBN 2-8318-9524-3
– 2 – PAS 62562 © IEC:2008(E)
CONTENTS
FOREWORD.3

1 Scope.4

2 Measurement parameters .4

3 Theory and calculation equations .5

3.1 Relative permittivity and loss tangent .5

3.2 Temperature dependence of ε′ and tan δ.7

3.3 Cavity parameters .8

4 Measurement equipment and apparatus .9
4.1 Measurement equipment .9
4.2 Measurement apparatus for complex permittivity .9
5 Measurement procedure.10
5.1 Preparation of measurement apparatus .10
5.2 Measurement of reference level .10
5.3 Measurement of cavity parameters: D, H, σ , α , TCρ.10
r c
5.4 Measurement of complex permittivity of test specimen: ε′, tan δ .12
5.5 Temperature dependence of ε′ and tan δ.13
Annex A (informative) Example of measured result and accuracy .14
A.1 Cavity parameters .14
A.2 Relative permittivity ε′ and loss tangent tan δ .15
A.3 Measurement accuracy.16
Bibliography.17

Figure 1 – Resonator structures of two types .5
Figure 2 – Correction term Δε’/ε’ .7
a
Figure 3 – Correction terms ΔA/A and ΔB/B .7
Figure 4 – Schematic diagram of measurement equipments.9
Figure 5 – Cavity resonator used for measurement .10
Figure 6 – Photograph of cavity resonator for measurement around 10 GHz .10
Figure 7 – Mode chart of cavity resonator .11
Figure 8 – Resonance peaks of cavity resonator.11

Figure 9 – Resonance frequency f , insertion attenuation IA and half-power band
0 0
width f .12
BW
Figure 10 – Resonance frequency f of TE mode of cavity resonator with dielectric
0 011
plate (D = 35 mm, H = 25 mm).12
Figure A.1 – Measured temperature dependence of f and Q .14
uc
Figure A.2 – Resonance peaks of cavity resonator clamping sapphire plate.15
Figure A.3 – Measured results of temperature dependence of f , Q , ε′ and tan δ for
0 u
sapphire plate.16

Table A.1 – Measured results of cavity parameters.14
Table A.2 – Measured results of of ε' and tan δ for sapphire plate.15

PAS 62562 © IEC:2008(E) – 3 –
INTERNATIONAL ELECTROTECHNICAL COMMISSION

____________
CAVITY RESONATOR METHOD TO MEASURE THE COMPLEX

PERMITTIVITY OF LOW-LOSS DIELECTRIC PLATES

FOREWORD
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A PAS is a technical specification not fulfilling the requirements for a standard but made
available to the public.
IEC-PAS 62562 has been processed by subcommittee 46F: RF and microwave passive
components, of IEC technical committee 46: Cables, wires, waveguides, r.f. connectors, r.f.
and microwave passive components and accessories.
The text of this PAS is based on the This PAS was approved for
following document: publication by the P-members of the
committee concerned as indicated in
the following document
Draft PAS Report on voting
46F/73/NP 46F/78/RVN
Following publication of this PAS, which is a pre-standard publication, the technical committee
or subcommittee concerned will transform it into an International Standard.
This PAS shall remain valid for an initial maximum period of three years starting from
2008-01. The validity may be extended for a single three-year period, following which it shall
be revised to become another type of normative document or shall be withdrawn.

– 4 – PAS 62562 © IEC:2008(E)
CAVITY RESONATOR METHOD TO MEASURE THE COMPLEX

PERMITTIVITY OF LOW-LOSS DIELECTRIC PLATES

1 Scope
This PAS describes the measurement method of dielectric properties in the planer direction of

dielectric plate at microwave frequency in order to develop new materials and to design

microwave active and passive devices. This method is called a cavity resonator method.

This method has the following characteristics:
• the relative permittivity ε′ and loss tangent tan δ values of a dielectric plate sample can be
measured accurately and non-destructively;
• temperature dependence of complex permittivity can be measured;
-6
• the measurement accuracy is within 0,3% for ε′ and within 5 ×10 for tan δ;
• fringing effect is corrected using correction charts calculated on the basis of rigorous
analysis.
This method is applicable for measurements in the following conditions:
• frequency    : 2 GHz < f < 40 GHz;
• relative permittivity : 2 < ε′ < 100;
–6 –2
• loss tangent    : 10 < tan δ < 10 .

2 Measurement parameters
The measurement parameters are defined as follows.
ε = ε '− jε"= D /(ε E)    (1)
r 0
tan δ = ε" / ε'     (2)
-
ε ε
T ref –6
TC = × 10      (1 × 10 /K)         (3)
ε
T − T
ε
ref
ref
where
D  is the electric flux density;

E  is the electric field strength;
ε  is the permittivity in a vacuum;
ε′ and ε″  are the real and imaginary components of the complex relative permittivity ε ;
r
TCε  is the temperature coefficient of relative permittivity;
ε and ε are the real parts of the complex relative permittivity at temperature T and
T ref
reference temperature T (= 20 °C to 25 °C), respectively.
ref
PAS 62562 © IEC:2008(E) – 5 –
3 Theory and calculation equations

3.1 Relative permittivity and loss tangent

A resonator structure used in the non-destructive measurement of the complex permittivity is

shown in Figure 1a. A cavity having diameter D and length H = 2M is cut into two halves in the

middle of its length. A dielectric plate sample having ε′, tan δ and thickness t is placed

between these two halves. The TE mode, having only the electric field component
tangential to the plane of the sample, is used for the measurement, since air gaps at the

plate-cavity interfaces do not affect the electromagnetic field. Taking account of fringing field
in the plate-region outside diameter of the cavity on the basis of the rigorous mode matching
analysis, we determine ε′ and tan δ from the measured values of the resonant frequency f
and the unloaded Q-factor Q . This numerical calculation, however, is rather tedious.
u
Therefore, we first determine approximate values ε′ and tan δ from the f and Q values by
0 u
a
a
using simple formula for a resonator structure shown in Figure 1b, where the fringing effect
for Figure 1a is neglecte
...

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