ISO 6721-6:2019

Plastics — Determination of dynamic mechanical properties — Part 6: Shear vibration — Non-resonance method

This document describes a forced, non-resonance method for determining the components of the shear complex modulus G* of polymers at frequencies typically in the range 0,01 Hz to 100 Hz. Higher-frequency measurements can be made, but significant errors in the dynamic properties measured are likely to result (see 10.2.2 and 10.2.3). The method is suitable for measuring dynamic storage moduli in the range 0,1 MPa to 50 MPa. NOTE Although materials with moduli greater than 50 MPa can be studied, more accurate measurements of their dynamic shear properties can be made using a torsional mode of deformation (see ISO 6721-2 and ISO 6721-7). This method is particularly suited to the measurement of loss factors greater than 0,02 and can therefore be conveniently used to study the variation of dynamic properties with temperature and frequency through most of the glass-rubber relaxation region (see ISO 6721-1). The availability of data determined over wide ranges of both frequency and temperature enables master plots to be derived, using frequency/temperature shift procedures, which display dynamic properties over an extended frequency range at different temperatures.

Plastiques — Détermination des propriétés mécaniques dynamiques — Partie 6: Vibration en cisaillement — Méthode hors résonance

General Information

• Status: Published
• Publication Date: 16-Apr-2019
• ICS: 83.080.01 - Plastics in general
• Technical Committee: ISO/TC 61/SC 5 - Physical-chemical properties
• Drafting Committee: ISO/TC 61/SC 5/WG 8 - Thermal analysis
• Current Stage: 9020 - International Standard under periodical review
• Start Date: 15-Jan-2024
• Completion Date: 15-Jan-2024

Relations

• Revises: ISO 6721-6:1996 - Plastics — Determination of dynamic mechanical properties — Part 6: Shear vibration — Non-resonance method
• Effective Date: 28-Jan-2017
• Revises: ISO 6721-6:1996/Amd 1:2007 - Plastics — Determination of dynamic mechanical properties — Part 6: Shear vibration — Non-resonance method — Amendment 1
• Effective Date: 28-Jan-2017

Standards Content (Sample)

INTERNATIONAL ISO
STANDARD 6721-6
Second edition
2019-04
Plastics — Determination of dynamic
mechanical properties —
Part 6:
Shear vibration — Non-resonance
method
Plastiques — Détermination des propriétés mécaniques
dynamiques —
Partie 6: Vibration en cisaillement — Méthode hors résonance
Reference number
ISO 6721-6:2019(E)
©
ISO 2019

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ISO 6721-6:2019(E)

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ii © ISO 2019 – All rights reserved

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ISO 6721-6:2019(E)

Contents Page
Foreword .iv
1 Scope . 1
2 Normative references . 1
3 Terms and definitions . 1
4 Principle . 1
5 Apparatus . 2
5.1 Loading assembly . 2
5.1.1 General. 2
5.1.2 Load stage . 2
5.1.3 Transducers. 2
5.2 Electronic data-processing equipment . 3
5.3 Temperature measurement and control . 3
5.4 Devices for measuring test specimen dimensions . 3
6 Test specimens. 3
6.1 General . 3
6.2 Shape and dimensions . 3
6.3 Preparation of polymer specimens . 3
7 Number of test specimens . 3
8 Conditioning .
...